CN103665037A - 一种2,2′-双[(3,5-二甲苯基)磷]联萘的制备方法 - Google Patents
一种2,2′-双[(3,5-二甲苯基)磷]联萘的制备方法 Download PDFInfo
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6018081A (en) * | 1996-03-15 | 2000-01-25 | Dsm N.V. | Process to prepare a terminal aldehyde |
US20050288257A1 (en) * | 2004-06-25 | 2005-12-29 | Taber Douglass F | Novel stable compositions of water and oxygen sensitive compounds and their method of preparation |
CN1746179A (zh) * | 2004-09-09 | 2006-03-15 | 中国科学院成都有机化学有限公司 | 光学纯7,7′-二取代-2,2′-双二苯基膦-1,1′-联萘配体及其合成方法 |
CN101501099A (zh) * | 2006-08-09 | 2009-08-05 | 共荣社化学株式会社 | 含双(二苯基膦基)联萘基团的聚合物 |
CN101830930A (zh) * | 2009-03-11 | 2010-09-15 | 中国科学院大连化学物理研究所 | 手性联萘二苯基磷功能化的介孔材料及其制备和应用 |
CN101885741A (zh) * | 2010-07-13 | 2010-11-17 | 成都理工大学 | 手性单膦配体的合成方法 |
CN103059064A (zh) * | 2012-09-08 | 2013-04-24 | 青岛科技大学 | 手性双膦配体与手性催化剂及制备、应用方法 |
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- 2013-12-06 CN CN201310646748.4A patent/CN103665037B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6018081A (en) * | 1996-03-15 | 2000-01-25 | Dsm N.V. | Process to prepare a terminal aldehyde |
US20050288257A1 (en) * | 2004-06-25 | 2005-12-29 | Taber Douglass F | Novel stable compositions of water and oxygen sensitive compounds and their method of preparation |
CN1746179A (zh) * | 2004-09-09 | 2006-03-15 | 中国科学院成都有机化学有限公司 | 光学纯7,7′-二取代-2,2′-双二苯基膦-1,1′-联萘配体及其合成方法 |
CN101501099A (zh) * | 2006-08-09 | 2009-08-05 | 共荣社化学株式会社 | 含双(二苯基膦基)联萘基团的聚合物 |
CN101830930A (zh) * | 2009-03-11 | 2010-09-15 | 中国科学院大连化学物理研究所 | 手性联萘二苯基磷功能化的介孔材料及其制备和应用 |
CN101885741A (zh) * | 2010-07-13 | 2010-11-17 | 成都理工大学 | 手性单膦配体的合成方法 |
CN103059064A (zh) * | 2012-09-08 | 2013-04-24 | 青岛科技大学 | 手性双膦配体与手性催化剂及制备、应用方法 |
Non-Patent Citations (4)
Title |
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LEI LIU等: "Improved Syntheses of Phosphine Ligands by Direct Coupling of Diarylbromophosphine with Organometallic Reagents", 《CHEM. EUR. J.》, vol. 17, no. 39, 30 September 2011 (2011-09-30), pages 10828 - 10831 * |
李栋等: "3,3′-取代联苯和联萘骨架亚磷酰胺配体的合成", 《合成化学》, vol. 16, no. 06, 20 December 2008 (2008-12-20), pages 656 - 659 * |
王俊: "光学活性2,2"-双二苯基膦基-1,1"-联萘(BINAP)的合成", 《武汉科技大学硕士学位论文》, 15 May 2007 (2007-05-15), pages 10 * |
龚成斌等: "氯化二苯基膦制备方法的改进", 《西南师范大学学报(自然科学版)》, vol. 24, no. 01, 20 February 1999 (1999-02-20), pages 120 - 122 * |
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Address after: 516081 No. 5, science and technology innovation road, west science and Technology Park, Dayawan, Guangdong, Huizhou Patentee after: Raffles Guangdong Pharmaceutical Technology Co. Ltd. Address before: 516081 No. 5, science and technology innovation road, west science and Technology Park, Dayawan, Guangdong, Huizhou Patentee before: Raffles PharmaTech Co., Ltd. |
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Effective date of registration: 20200810 Address after: No.3, Binhai 10th Road North, Dayawan Petrochemical District, Huizhou City, Guangdong Province Co-patentee after: GUANGDONG XIANQIANG PHARMACEUTICAL Co.,Ltd. Patentee after: GUANGDONG RAFFLES PHARMATECH Co.,Ltd. Address before: 516081 No. 5, science and technology innovation road, west science and Technology Park, Dayawan, Guangdong, Huizhou Patentee before: GUANGDONG RAFFLES PHARMATECH Co.,Ltd. |
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Effective date of registration: 20210705 Address after: 516081 No.3, North Binhai 10th Road, Dayawan Petrochemical District, Huizhou City, Guangdong Province Patentee after: GUANGDONG RAFFLES PHARMATECH Co.,Ltd. Address before: 516081 No.3, North Binhai 10th Road, Dayawan Petrochemical District, Huizhou City, Guangdong Province Patentee before: GUANGDONG RAFFLES PHARMATECH Co.,Ltd. Patentee before: GUANGDONG XIANQIANG PHARMACEUTICAL Co.,Ltd. |
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