CN103610834A - Traditional Chinese medicine composition as well as preparation method and application thereof - Google Patents
Traditional Chinese medicine composition as well as preparation method and application thereof Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine composition as well as a preparation method and an application thereof. The traditional Chinese medicine composition is an extract of a material A and/or water or ethanol aqueous solution of the material A; the material A comprises the following components in parts by weight: 2-10 parts of mulberry, 2-10 parts of balsam pear, 5-20 parts of tea and 1-5 parts of Chinese dates; the mulberry comprises one or more of mulberry leaves, the root bark of white mulberry, ramulus mori, silkworm excrement and mulberry; the tea comprises green tea, oolong tea, black tea and Puer tea. The traditional Chinese medicine composition roots in foodstuff or has homology of medicine and food, has obvious effects of losing weight, lowering lipid and reducing blood sugar and can be taken for a long time.
Description
Technical field
The present invention relates to a kind of Chinese medicine composition and its preparation method and application.
Background technology
In recent years, progressively raising along with people's living standard, the sickness rate of the affluence diseases such as China's hypertension, diabetes and obesity obviously rises, and has become the first killer who threatens middle-aged and elderly people, and hypertension, diabetes, obesity belong to the very close disease of dependency.For to anti-obesity, the mankind have taked various modes, how from keeping on a diet, to set about, also there is health food, also have much from theory of Chinese medical science, the research cause of disease, the Chinese medicine preparation of making by scientific and reasonable composition of prescription, reaches the object for the treatment of both the principal and secondary aspects of a disease, to realize the effect of lowering blood-fat and reducing weight.
The Chinese medicine composition of now a lot of Weight-reducing and lipid-lowerings, although there is the effect of Weight-reducing and lipid-lowering, all contains purgatives medicine in its composition, have the defect that toxic and side effects is large, withdraw rear easy bounce-back, and long-term taking may cause drug dependence and constipation.As contained Semen Cassiae in the Chinese medicine composition of CN201210194739.1 patent application; For another example, in the Chinese medicine composition of CN200910238679.7 patent application, contain Radix Et Rhizoma Rhei; And modern study shows, in Semen Cassiae and Radix Et Rhizoma Rhei, all containing anthraquinone component, the medicine that long-term taking makes with Semen Cassiae or Radix Et Rhizoma Rhei may cause Melanosis coli or claim large intestine Pseudomelanosis.This present situation is urgently to be resolved hurrily.
Summary of the invention
It is large that technical problem to be solved by this invention is to have overcome Weight-reducing and lipid-lowering product toxic and side effects of the prior art, withdraw rear easy bounce-back, formula is indefinite without logos, effective ingredient target, long-term taking may cause and in drug dependence and constipation, composition, contain the defect that purgatives medicine may cause Melanosis coli or claim large intestine Pseudomelanosis etc., and a kind of Chinese medicine composition and its preparation method and application is provided.Chinese medicine composition of the present invention derives from foodstuff or integration of edible and medicinal herbs, and fat-reducing, blood fat reducing, hypoglycemic evident in efficacy, can long-term taking.
The present invention solves above-mentioned technical problem by following technical proposals:
The invention provides a kind of Chinese medicine composition, it is the water of material A and/or material A or the extract of ethanol water, and described material A comprises: in weight portion, and 2-10 part Mulberry, 2-10 part Fructus Momordicae charantiae, 5-20 part Folium Camelliae sinensis, and 1-5 part Fructus Jujubae (having another name called Fructus Jujubae); Wherein, described Mulberry comprises one or more in Folium Mori, Cortex Mori, Ramulus Mori, Bombyx mori L. and Fructus Mori, and described Folium Camelliae sinensis comprises green tea, oolong tea, black tea and Folium camelliae assamicae.
Preferably, described material A comprises: in weight portion, and 3 parts of 5 parts, Folium Mori, 5 parts, Fructus Momordicae charantiae, 10 parts of Folium Camelliae sinensis and Fructus Jujubaes.
In the present invention, in described Folium Camelliae sinensis, the mass ratio of green tea, oolong tea, black tea and Folium camelliae assamicae is preferably (0.8-1.2): (0.8-1.2): (0.8-1.2): (0.8-1.2), be more preferably 1:1:1:1.
In the present invention, one or more in described Folium Mori, Cortex Mori, Ramulus Mori, Bombyx mori L. and Fructus Mori enter the Morus resource material of Chinese crude drug form for this area is conventional said.
In the present invention, described Fructus Momordicae charantiae is the conventional said Fructus Momordicae charantiae that enters Chinese crude drug form in this area.
In the present invention, described Fructus Jujubae is the conventional said Fructus Jujubae that enters Chinese crude drug form in this area.
In the present invention, described Chinese medicine composition is preferably powder type.Wherein, the preparation method of described powder is that this area is conventional, preferably comprising the steps: each component in the extract of the water of material A and/or material A or ethanol water to be dried to respectively containing water quality percentage composition is to be ground into fine powder after 2%-3%, cross 80-120 mesh sieve, or particle diameter is the superfine powder of 0.30-24 μ m, carry out again irradiation sterilization, remix preparation.
Wherein, described dry method is the method for dry Mulberry, Fructus Momordicae charantiae, Folium Camelliae sinensis and the Fructus Jujubae of this area routine.The dry method of described Mulberry, Fructus Momordicae charantiae or Folium Camelliae sinensis is preferably for spraying is dry.Described spray-dired process conditions are that this area is conventional, are preferably: 160 ℃ of inlet temperature, charging rate 9mL/min and atomizing pressure 1.05bar.The dry method of described Fructus Jujubae is preferably vacuum drying.Described vacuum drying process conditions are that this area is conventional, are preferably: 70 ℃ of vacuum-0.08MPa and baking temperatures.
In the present invention, the water of described material A or the extract of ethanol water are that the plant extraction process of this area routine extracts acquisition, preferably it comprises the steps: respectively by the Mulberry in material A, Fructus Momordicae charantiae, Folium Camelliae sinensis or Fructus Jujubae, through water or ethanol water, decoct 2-3 time, filter, remerge and be condensed into extractum.
Wherein, the volumetric concentration of described ethanol water is that this area is conventional, is preferably 45%-75%, is more preferably 65%.Described simmer down to this area routine operation is preferably vacuum concentration.The condition of described vacuum concentration is this area normal condition, and the temperature of described vacuum concentration is preferably 60-100 ℃, is more preferably 60 ℃; The pressure of described vacuum concentration is preferably-0.08MPa.Described concentrating is preferably 1.24-1.26 for being concentrated into the relative density of extractum.
The present invention also provides the preparation method of above-mentioned Chinese medicine composition, and described preparation method is according to this area routine, each composition evenly to be mixed.
Wherein, the preparation method of described material A or the described water of material A or the extract of ethanol water all as previously mentioned.
The present invention also provides the application of above-mentioned Chinese medicine composition in preparation fat-reducing, blood fat reducing or hypoglycemic medicine or health food.
In the present invention, the dosage form of described medicine can be this area routine, is preferably tablet, capsule, granule, pill or oral liquid.
Wherein, described tablet, capsule, granule, pill or oral liquid comprise described Chinese medicine composition and the acceptable adjuvant of pharmacy.
Described adjuvant is pharmaceutically acceptable excipient, is preferably one or more in microcrystalline Cellulose, sodium carboxymethyl cellulose, magnesium stearate and Pulvis Talci.
Meeting on the basis of this area general knowledge, above-mentioned each optimum condition, can combination in any, obtains the preferred embodiments of the invention.
Agents useful for same of the present invention and raw material be commercially available obtaining all.
Positive progressive effect of the present invention is: Chinese medicine composition of the present invention derives from foodstuff or integration of edible and medicinal herbs, has the saccharide of inhibition, stops fatty absorption, accelerates the metabolism of body fat, plays fat-reducing, blood fat reducing, falls the evident in efficacy of blood, can long-term taking.
The specific embodiment
Mode below by embodiment further illustrates the present invention, but does not therefore limit the present invention among described scope of embodiments.The experimental technique of unreceipted actual conditions in the following example, according to conventional method and condition, or selects according to catalogue.
In following embodiment:
Folium Mori are purchased from Hunan Song Lingtang prepared slices of Chinese crude drugs company limited;
Fructus Jujubae is purchased from Hunan Song Lingtang prepared slices of Chinese crude drugs company limited;
Magnesium stearate is purchased from Anhui Shanhe Medical Accessary Material Co., Ltd.;
Sodium carboxymethyl cellulose is purchased from Shandong Chemical Co., Ltd. of Yanggu Hengchang;
All the other medical materials are all to purchase in Hunan Song Lingtang prepared slices of Chinese crude drugs company limited.
In following embodiment, described Folium Camelliae sinensis is comprised of green tea, oolong tea, black tea and Folium camelliae assamicae.In embodiment 1-3, the mass ratio of green tea, oolong tea, black tea and Folium camelliae assamicae is 1:1:1:1.
Embodiment 1
Take the raw material of following weight proportion: 8 parts, Folium Mori, 6 parts, Fructus Momordicae charantiae, 9 parts of Folium Camelliae sinensis, 2 parts of Fructus Jujubaes.Four taste raw materials extract respectively, add the water extraction 2 times that 8-12 doubly measures, and each 1-2h, filters, and remerges and is condensed into extractum.Wherein, described simmer down to vacuum concentration.The temperature of described vacuum concentration is 60 ℃; The pressure of described vacuum concentration is-0.08MPa.The relative density that described simmer down to is concentrated into extractum is 1.25.
Wherein Folium Mori, Fructus Momordicae charantiae, Folium Camelliae sinensis adopt spraying dry (160 ℃ of inlet temperature, charging rate 9mL/min, atomizing pressure 1.05bar), and Fructus Jujubae adopts vacuum drying (0.08MPa, 70 ℃).After above four extract powders are mixed, with one-step-granulating method, granulate, take water as wetting agent, obtain granule, granule is incapsulated, obtain capsule product.
Embodiment 2
Take the raw material of following weight proportion: 5 parts, Folium Mori, 5 parts, Fructus Momordicae charantiae, 10 parts of Folium Camelliae sinensis, 3 parts of Fructus Jujubaes.Press the method granulation of embodiment 1, then add 2% the disintegrating agent carboxymethyl base sodium cellulosate that accounts for 0.05% magnesium stearate lubricant of granule total amount and account for granule total amount, tabletting, every 0.8g-1.3g, subpackage obtains tablet product.
Embodiment 3
Take the raw material of following weight proportion: 4 parts, Folium Mori, 3 parts, Fructus Momordicae charantiae, 15 parts of Folium Camelliae sinensis, 4 parts of Fructus Jujubaes.Press the method granulation of embodiment 1, then add 4% the disintegrating agent carboxymethyl base sodium cellulosate that accounts for 0.05% magnesium stearate lubricant of granule total amount and account for granule total amount, tabletting, every 0.9g-1.5g, subpackage obtains tablet product.
Embodiment 4
Proportioning raw materials in the present embodiment is as follows: 2 parts of Cortex Mori, 2 parts, Fructus Momordicae charantiae, 5 parts of Folium Camelliae sinensis, 1 part of Fructus Jujubae.In the present embodiment, the mass ratio of green tea, oolong tea, black tea and Folium camelliae assamicae is 0.8:0.8:1.2:1.2.And the extract that utilizes the ethanol water of material A makes oral liquid product, the volumetric concentration of the ethanol water adopting is 45%, and remaining process conditions and step are all with embodiment 1.
Embodiment 5
Proportioning raw materials in the present embodiment is as follows: 10 parts of Ramulus Moris, 10 parts, Fructus Momordicae charantiae, 20 parts of Folium Camelliae sinensis, 5 parts of Fructus Jujubaes.In the present embodiment, the mass ratio of green tea, oolong tea, black tea and Folium camelliae assamicae is 1.2:1.2:0.8:0.8.And utilize material A and its extract at ethanol water to make pill product, and the volumetric concentration of the ethanol water adopting is 65%, remaining process conditions and step are all with embodiment 1.
Embodiment 6
Proportioning raw materials in the present embodiment is as follows: 10 parts of Bombyx mori L.s, 10 parts, Fructus Momordicae charantiae, 20 parts of Folium Camelliae sinensis, 5 parts of Fructus Jujubaes, and utilize material A and its extract at ethanol water to make pill product, the volumetric concentration of the ethanol water adopting is 65%.The preparation method of the powder of material A is: it is to be ground into fine powder after 2% that material A is dried to containing water quality percentage composition, crosses 100 mesh sieves, then carries out 60Coradiation sterilizing.Remaining process conditions and step are all with embodiment 1.
Embodiment 7
Proportioning raw materials in the present embodiment is as follows: 10 parts of Fructus Mori, 10 parts, Fructus Momordicae charantiae, 20 parts of Folium Camelliae sinensis, 5 parts of Fructus Jujubaes, and utilize material A to make pill product, the volumetric concentration of the ethanol water adopting is 65%; The preparation method of the powder of material A is: it is to be ground into fine powder after 3% that material A is dried to containing water quality percentage composition, gets the superfine powder that particle diameter is 0.30-24 μ m, then carries out 60Coradiation sterilizing.Remaining process conditions and step are all with embodiment 1.
Effect embodiment 1
In order to confirm that Chinese medicine composition of the present invention has obvious fat-reducing, effect for reducing fat, the mice of high heat food being brought out to animal obesity has carried out pharmacodynamic experiment, tested formula is used Chinese medicine composition of the present invention, is made as respectively group 1, organizes 2, organizes the raw material ratio in the corresponding embodiment 1-3 of 3(difference).Wherein, organizing one composition is: the mixture that 8 parts, Folium Mori, 6 parts, Fructus Momordicae charantiae, 9 parts of Folium Camelliae sinensis and Fructus Jujubae are 2 parts; Group two composition is: the mixture that 5 parts, Folium Mori, 5 parts, Fructus Momordicae charantiae, 10 parts of Folium Camelliae sinensis and Fructus Jujubae are 3 parts; Group three composition is: the mixture that 4 parts, Folium Mori, 3 parts, Fructus Momordicae charantiae, 15 parts of Folium Camelliae sinensis and Fructus Jujubae are 4 parts.
Experimental technique is as follows:
Male ICR mouse is fed under experimental enviroment normal diet 1 week, weighs.Be divided at random 5 groups: Normal group is from on-test to finishing to feed (gavage gives distilled water) with normal diet, all the other animals nutrient fodder (normal feedstuff 80%, Adeps Sus domestica 10%, yolk powder 10%) of all feeding; Model control group gavage gives distilled water.Be subject to continuously reagent 42 days, every day, 0.4g/Kg, weighed weekly 1 time.
Index determining method and result are as follows:
Last is subject to after reagent, mice nose is weighed, measured to each group mice to the length of anus, and calculate Lee ' S index; Meanwhile, mice is plucked to eyeball and get blood, separation of serum, measures TC(serum total cholesterol), TG(triglyceride), HDL-C(HDL-C), LDL-C(low density cholesterol) concentration; Cut open the belly and get body fat (epididymis and perirenal fat pad) and weigh, calculate body fat ratio.Test result is as shown in table 1, table 2 and table 3.
Table 1 is subject to the impact of reagent on Nutritive obesity mice body weight and Lee ' S index
| Group | Starting weight/g | Whole weight/g | Lee ' S index |
| Normal group | 21.45±0.48 | 35.02±2.48 * | 316.12±10.48 * |
| Model control group | 22.05±0.32 | 38.14±2.23 | 327.82±11.47 |
| Group 1 | 22.65±0.41 | 35.25±2.51 * | 314.76±10.62 * |
| Group 2 | 21.90±0.48 | 34.68±2.23 ** | 311.42±10.36 * |
| Group 3 | 21.79±0.42 | 35.72±2.64 * | 314.98±13.25 * |
(note: compare with model control group,
*, p < 0.05,
*, p < 0.01)
The result of table 1 shows: be subject to reagent group all can reduce Lee ' the S index of Nutritive obesity mice, organize 1, organize 2 with model control group comparison, data have significant difference.
Table 2 is subject to the impact of reagent on the fatty weight in wet base of Nutritive obesity mice
(note: compare with model control group,
*, p < 0.05,
*, p < 0.01)
The result of table 2 shows: be subject to the fatty weight in wet base of reagent group lower than model control group, body fat is than higher than model control group, organize 1, organize 2 with model control group comparison, kidney around fatty weight in wet base and body fat compares significant difference.
Table 3 is subject to the impact of reagent on Nutritive obesity mice blood lipid level
(note: compare with model control group,
*, p < 0.05,
*, p < 0.01)
The result of table 3 shows: compare with Normal group, model control group mice serum TC, TG and LDL-C significantly raise, and HDL-C significantly reduces.Group 1, organize 2 and all can significantly reduce mice serum TC, TG and LDL-C concentration, rising HDL-C concentration.
Visible, be subject to reagent all can reduce Lee ' S exponential sum fat index, wherein organize 1, organize 2 and relatively there is significant difference with model control group, and organize 2 effect and be better than organizing 1.Above-mentioned description of test, Folium Mori of the present invention, Fructus Momordicae charantiae, Folium Camelliae sinensis, Fructus Jujubae proportioning are used, and have synergistic function, can be used for again hyperlipemia in the time of fat-reducing.
Comparative example 1
Material in the component of the Chinese medicine composition that employing is not particularly limited in the present invention carries out within 30 days and 42 days, feeding and body weight test to Nutritive obesity mice, and feedstuff kind and method of testing are with effect embodiment 1, and test result is as shown in table 4.
Table 4 is subject to the impact of reagent on Nutritive obesity mice body weight and Lee ' S index
(note: compare with model control group,
*, p < 0.05,
*, p < 0.01)
Owing to buying mice, belong to trophophase, add the weight feed of feedstuff, the body weight increase trend that is inevitable.As can be drawn from Table 4, group 2 is fed mice and is contrasted with nutrient fodder group after 42 days, there is significant differences, other 7 groups of data, except Fructus Jujubae nursing group does not separately have significant difference, remaining 6 groups all have significant difference, best with effect of the present invention, prompting, after combination and compatibility, has the effect of potentiation.
The present invention makes full use of Chinese medical theory and modern medicine study achievement is carried out prescription, for saccharide, fats in absorption of human body metabolic process, from a plurality of links such as decrease uptake, quickening metabolism, act on disease, through animal experiment, confirm to have the effect of obvious Weight-reducing and lipid-lowering.The pharmacology that compositions of the present invention has and health-care effect, can be used as medicine, also can be used as health food.
Claims (10)
1. a Chinese medicine composition, it is characterized in that, described Chinese medicine composition is the water of material A and/or material A or the extract of ethanol water, and described material A comprises: in weight portion, 2-10 part Mulberry, 2-10 part Fructus Momordicae charantiae, 5-20 part Folium Camelliae sinensis, and 1-5 part Fructus Jujubae; Wherein, described Mulberry comprises one or more in Folium Mori, Cortex Mori, Ramulus Mori, Bombyx mori L. and Fructus Mori, and described Folium Camelliae sinensis comprises green tea, oolong tea, black tea and Folium camelliae assamicae.
2. Chinese medicine composition as claimed in claim 1, is characterized in that, described material A comprises: in weight portion, and 3 parts, 5 parts, Folium Mori, 5 parts, Fructus Momordicae charantiae, 10 parts of Folium Camelliae sinensis and Fructus Jujubae; In described Folium Camelliae sinensis, the mass ratio of green tea, oolong tea, black tea and Folium camelliae assamicae is (0.8-1.2): (0.8-1.2): (0.8-1.2): (0.8-1.2), be preferably 1:1:1:1.
3. Chinese medicine composition as claimed in claim 1, is characterized in that, described Chinese medicine composition is powder type; It is to be ground into fine powder after 2%-3% that the preparation method of described powder preferably comprises the steps: each component in the extract of the water of material A and/or material A or ethanol water to be dried to respectively containing water quality percentage composition, cross 80-120 mesh sieve, or particle diameter is the superfine powder of 0.30-24 μ m, carry out again irradiation sterilization, remix preparation.
4. Chinese medicine composition as claimed in claim 3, is characterized in that, the dry method of described Mulberry, Fructus Momordicae charantiae or Folium Camelliae sinensis is dry for spraying; Described spray-dired process conditions are preferably: 160 ℃ of inlet temperature, charging rate 9mL/min and atomizing pressure 1.05bar; The dry method of described Fructus Jujubae is vacuum drying; Described vacuum drying process conditions are preferably: 70 ℃ of vacuum-0.08MPa and baking temperatures.
5. the Chinese medicine composition as described in claim 1-4 any one, is characterized in that, respectively by the Mulberry in material A, Fructus Momordicae charantiae, Folium Camelliae sinensis or Fructus Jujubae, through water or ethanol water, decocts 2-3 time, filters, remerge and be condensed into extractum.
6. Chinese medicine composition as claimed in claim 5, is characterized in that, the volumetric concentration of described ethanol water is 45%-75%, is preferably 65%; Described simmer down to vacuum concentration; The temperature of described vacuum concentration is preferably 60-100 ℃, is more preferably 60 ℃; The pressure of described vacuum concentration is preferably-0.08MPa; The relative density that described simmer down to is concentrated into extractum is 1.24-1.26.
7. a preparation method for the Chinese medicine composition as described in claim 1-6 any one, is characterized in that, described preparation method is that each composition is evenly mixed.
8. the Chinese medicine composition as described in the claim 1-6 any one application in preparation fat-reducing, blood fat reducing or hypoglycemic medicine or health food.
9. application as claimed in claim 8, is characterized in that, the dosage form of described medicine is tablet, capsule, granule, pill or oral liquid.
10. application as claimed in claim 9, is characterized in that, described tablet, capsule, granule, pill or oral liquid comprise described Chinese medicine composition and the acceptable adjuvant of pharmacy; Described adjuvant is preferably one or more in microcrystalline Cellulose, sodium carboxymethyl cellulose, magnesium stearate and Pulvis Talci.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796966A (en) * | 2016-04-14 | 2016-07-27 | 圣原健康产业有限公司 | Traditional Chinese medicine composition for preventing and treating chronic fatigue syndromes and preparation method and application thereof |
| CN106962545A (en) * | 2017-03-31 | 2017-07-21 | 安徽新华学院 | Health care lipid-loweringing worm tea and preparation method thereof |
| CN107333931A (en) * | 2017-07-31 | 2017-11-10 | 季敬洪 | Health tea composition and preparation method thereof |
| CN108125236A (en) * | 2017-12-19 | 2018-06-08 | 重庆海田林业科技有限公司 | Mulberry tree concentrate and its preparation process |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101683161A (en) * | 2008-09-26 | 2010-03-31 | 刘泳宏 | Natural tea drink capable of clearing away heat and production method |
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2013
- 2013-11-25 CN CN201310603197.3A patent/CN103610834B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101683161A (en) * | 2008-09-26 | 2010-03-31 | 刘泳宏 | Natural tea drink capable of clearing away heat and production method |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796966A (en) * | 2016-04-14 | 2016-07-27 | 圣原健康产业有限公司 | Traditional Chinese medicine composition for preventing and treating chronic fatigue syndromes and preparation method and application thereof |
| CN106962545A (en) * | 2017-03-31 | 2017-07-21 | 安徽新华学院 | Health care lipid-loweringing worm tea and preparation method thereof |
| CN107333931A (en) * | 2017-07-31 | 2017-11-10 | 季敬洪 | Health tea composition and preparation method thereof |
| CN108125236A (en) * | 2017-12-19 | 2018-06-08 | 重庆海田林业科技有限公司 | Mulberry tree concentrate and its preparation process |
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