CN103548898B - Single matrine and composition pesticide - Google Patents
Single matrine and composition pesticide Download PDFInfo
- Publication number
- CN103548898B CN103548898B CN201310367287.7A CN201310367287A CN103548898B CN 103548898 B CN103548898 B CN 103548898B CN 201310367287 A CN201310367287 A CN 201310367287A CN 103548898 B CN103548898 B CN 103548898B
- Authority
- CN
- China
- Prior art keywords
- matrine
- jervine
- composition pesticide
- agent
- purposes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of single matrine, include following component according to percent by weight：Radix Sophorae Flavescentis extractive liquid 10～20%, Radix Bupleuri extracting solution 2～12%, Fructus Toosendan extracting solution 10～30%, Fructus Piperiss extracting solution 5～15%, Radix seu Caulis Derridis Trifoliatae extracting solution 3～13%, auxiliary agent 15～25%, garlic extract 13～23%, described auxiliary agent is polyoxyethylene nonylphenol ether 10 or methanol.A kind of use matrine and the composition pesticide of jervine preparation, the mass ratio of described matrine and jervine is 0.3: 70～70: 0.3.All components are extracted, are formulated, nuisanceless, noresidue by natural plant raw material, and technique is advanced, and prevention effect is good, does not affect the quality of agricultural product.
Description
Technical field
The present invention relates to insecticide is and in particular to single matrine and composition pesticide.
Background technology
In recent years, people increasingly note the sustainable development of agricultural production and the coordinated development of human and environment.Add generation
After trade tissue, the market competition is fiercer, and green barrier has seriously restricted the outlet of agricultural products in China.Therefore, research and development
Biological pesticide is particularly important, development biological pesticide oneself become ensure human health and agricultural sustainable development important become
Gesture.
Matrine（Matrine), it is to be obtained through organic solvent extraction such as ethanol by the root of Radix Sophorae Flavescentiss, stem, leaf and/or fruit
The main component of alkaloid, is a kind of agricultural chemical of natural plant, has stomach toxicity and action of contace poison.Matrine, to people and animals' low toxicity, is wide
Spectrum insecticide, can be used to prevent and treat rice hoppers, striped rice borer, yellow rice borer, brassicaceous vegetable aphid, Pieris rapae, diamondback moth, fragrant-flowered garlic
Dish fragrant-flowered garlic maggot, Camellia sinensis Euproctis pseudoconspersa, tea chi pot, the harmful organism such as Nicotiana tabacum L. oriental tobacco budworm, cigarette aphid.
However, matrine vegetable pesticide also has some shortcomings, one is that compound structure is complicated, is not easily-synthesized or synthesizes cost
Too high：Two is because the distribution of Radix Sophorae Flavescentiss has region, and the limiting factor being subject in the selection in processing place is many；Three is Radix Sophorae Flavescentiss
Collection there is seasonality, source is restricted.
Content of the invention
The technical problem to be solved in the present invention is to provide single matrine and composition pesticide, and all components are by natural plant
Thing source raw material extracts, is formulated, nuisanceless, noresidue, and technique is advanced, and prevention effect is good, does not affect the quality of agricultural product.
For reaching above-mentioned purpose, technical scheme is as follows：
A kind of single matrine, includes following component according to percent by weight：Radix Sophorae Flavescentis extractive liquid 10～20%, Radix Bupleuri carry
Take liquid 2～12%, Fructus Toosendan extracting solution 10～30%, Fructus Piperiss extracting solution 5～15%, Radix seu Caulis Derridis Trifoliatae extracting solution 3～13%, auxiliary agent 15～25%,
Garlic extract 13～23%,
Described auxiliary agent is emulsifier op-10 or methanol.
A kind of use matrine and the composition pesticide of jervine preparation, the mass ratio of described matrine and jervine is 0.3:
70～70: 0.3.
Preferably, the mass ratio of described matrine and jervine is 1:1.
Preferably, described composition pesticide includes following dosage form：Wettable powder, water dispersible granules and suspending agent.
Preferably, described wettable powder includes following component according to percent by weight：Matrine 0.3～70%, Rhizoma et radix veratri (Radix Rhizoma Veratri)
Alkali 0.3～70%, wetting agent 3～15%, dispersant 3-10%, carrier 8-10%, surplus supplied by filler.
Preferably, described water dispersible granules include following component according to percent by weight：Matrine 0.3～70%, Rhizoma et radix veratri (Radix Rhizoma Veratri)
Alkali 0.3～70%, dispersant 3～12%, wetting agent 2～8%, disintegrating agent 0～8%, binding agent 0～5%, filler 8～84%.
Preferably, described suspending agent includes following component according to percent by weight：Matrine 0.3～40%, jervine
0.3～30%, dispersant 3～12%, wetting agent 2～10%, defoamer 0.1～0.5%, thickening agent 0～2%, antifreeze 0～8%, remaining
Measure as deionized water.
By technique scheme, the invention has the beneficial effects as follows：
Prescription is unique, compatibility science, high-efficiency broad spectrum, nuisanceless, noresidue, and technique is advanced, and prevention effect is good, does not affect agriculture
The quality of product, and the growth of plant can be promoted.Especially for red spider on tea lesser leafhopper on Folium Camelliae sinensis, fruit tree, scale insect
Effect substantially, can comprehensive preventing and treating to insect pest.
Specific embodiment
Fig. 1 prepares the process schematic representation of wettable powder for the present invention.
Fig. 2 prepares the process schematic representation of water dispersible granules for the present invention.
Fig. 3 prepares the process schematic representation of suspending agent for the present invention.
In order that technological means, creation characteristic, reached purpose and effect that the present invention realizes are easy to understand, tie below
Conjunction is specifically illustrating, and the present invention is expanded on further.
1）A kind of single matrine, includes following component according to percent by weight：Radix Sophorae Flavescentis extractive liquid 10～20%, Radix Bupleuri
Extracting solution 2～12%, Fructus Toosendan extracting solution 10～30%, Fructus Piperiss extracting solution 5～15%, Radix seu Caulis Derridis Trifoliatae extracting solution 3～13%, auxiliary agent（Emulsifying
Agent OP-10, methanol）15～25%, garlic extract 13～23%.
Preparation technology：First said herbal medicine is washed, then cut into slices, then extracted, subsequently carried out
The concentration of extracting solution, then compounded, obtain described single matrine product through inspection.
2）A kind of use matrine and the composition pesticide of jervine preparation, the mass ratio of described matrine and jervine is
0.3: 70～70: 0.3.
Preferably, the mass ratio of described matrine and jervine is 1:1.
Preferably, described composition pesticide includes following dosage form：Wettable powder, water dispersible granules and suspending agent.
A kind of use matrine and the wettable powder of jervine preparation, include following component according to percent by weight：Bitter
Ginseng alkali 0.3～70%, jervine 0.3～70%, wetting agent（Sodium lauryl sulphate）3～15%, dispersant（Di-2-ethylhexylphosphine oxide bitter edible plant sulphur
Sour sodium）3-10%, carrier（White carbon）8-10%, filler（Kaolin）Supply surplus.
White carbon is in order to matrine, the uniform absorption of jervine are above it can be understood as dilute to matrine, jervine
Release one time, meanwhile, white carbon can increase mobility, in so whole product, matrine, jervine are uniformly dispersed in each
Inside grain.
With reference to technique Fig. 1, matrine, jervine and dispersant, wetting agent, carrier, filler etc. are mixed stirring
Half an hour, obtain the particle diameter of about 500 mesh through comminution by gas stream, mix half an hour again, it is wettable that prepared matrine, jervine compound
Property powder product.Qualified through analyzing, subpackage completes whole production process.
3）A kind of use matrine and the water dispersible granules of jervine preparation, include following component according to percent by weight：
Matrine 0.3～70%, jervine 0.3～70%, dispersant（Sodium lauryl sulphate）3～12%, wetting agent（The di-2-ethylhexylphosphine oxide bitter edible plant
Sodium sulfonate）2～8%, disintegrating agent（Ammonium sulfate）0～8%, binding agent（Xanthan gum）0～5%, filler（Kaolin）8～84%.
With reference to processing technology Fig. 2, matrine, jervine and dispersant, wetting agent, disintegrating agent, filler etc. are blended in one
Rise, obtain the particle diameter of about 500 mesh through comminution by gas stream, add binding agent mixing, obtain granulation materials.Item is quantitatively sent into stream
Change in bed granulating drier after granulation and drying, the water dispersible granules product that prepared matrine, jervine compound.Through analysis
Qualified, subpackage completes whole production process,
4）A kind of use matrine and the suspending agent of jervine preparation, include following component according to percent by weight：Radix Sophorae Flavescentiss
Alkali 0.3～40%, jervine 0.3～30%, dispersant（Sodium lauryl sulphate）3～12%, wetting agent（Di-2-ethylhexylphosphine oxide bitter edible plant sulfonic acid
Sodium）2～10%, defoamer（Dimethyl polyoxyethylene polysiloxanes）0.1～0.5%, thickening agent（Lignin）0～2%, antifreeze
（Ethylene glycol）0～8%, balance of filler（Deionized water）.
With reference to processing technology Fig. 3, by dispersant, wetting agent, thickening agent, antifreeze in above-mentioned formulation material through high speed shear
Mix homogeneously（30-60min）, add matrine, jervine, ball milling 2～3 hours in ball mill, make diameter of particle all 5
Below μm, prepared suspending agent product, then complete whole production process through analyzing qualified subpackage.
Filler in technique Fig. 3 is to supplement surplus, and such as other compositions add up only 50%, then remaining 50%
Will be supplemented with filler.
Deionized water deficiency surplus inside suspending agent, filler is exactly then deionized water, in this area typically by solid system
Agent is called filler the material of not enough surplus.
Embodiment 1：Prepare 0.6% matrine jervine wettable powder
Matrine 0.3%, jervine 0.3%, lauryl sulphate acid calcium 5%, di-2-ethylhexylphosphine oxide bitter edible plant sodium sulfonate 5%, white carbon 8% are high
Ridge soil is mended to 100%, mixture mix homogeneously in mixed cylinder, and 0.6% matrine jervine water preparation is obtained.
Embodiment 2：Prepare 0.8% matrine jervine water dispersible granules
Matrine 0.3%, jervine 0.5%, di-2-ethylhexylphosphine oxide bitter edible plant sodium sulfonate 6%, sodium lauryl sulphate 4%, ammonium sulfate 2%, Huang
Virgin rubber 5%, balance kaolin is supplied, and is mixed to prepare 0.8% matrine jervine water dispersible granules.
The present invention relates to cosolvent title respectively as follows：
Dispersant：Sodium methylene bis-naphthalene sulfonate
Wetting agent：Sodium lauryl sulphate or dodecyl sodium sulfate
Disintegrating agent：Ammonium sulfate
Binding agent：Xanthan gum
Filler：Kaolin（Water dispersible granules use）, deionized water（Suspending agent uses）
Defoamer：Polysiloxanes, organosilicon
Thickening agent：Lignin
Antifreeze：Ethylene glycol, glycerol
The virulence test of the present invention：Matrine is compounded to toxicity test in Camellia sinensis tea lesser leafhopper with jervine.
Test medicine is provided by Shaanxi Kang He Li Feng biotechnology pharmaceutcal corporation, Ltd.
Determine that through prerun, after each medicament Valid concentration, each medicament is set at 6 dosage respectively by active constituent content
Reason, if clear water comparison.
Reference《Farm-chemical indoor determination test rule insecticide》Carry out, medicament is measured using infusion process little to Camellia sinensis tea
The virulence of greenery Cicadae.Check test worm death condition after 96h, and recorded.Result of the test is as shown in table 1：
Table 1 matrine, jervine and its compounding toxicity test analysis of results table to Camellia sinensis tea lesser leafhopper
As shown in Table 1, matrine, the EC to Camellia sinensis tea lesser leafhopper for the jervine50It is respectively 23.99mg/L and 32.73mg/
L.The virulence of jervine is higher than the virulence of matrine.Matrine and jervine proportioning 1: 1,2: 1,3: 1,1：2 and 1：3 synergic ratio
Value is respectively 6.80,6.90,7.33,7.60 and 8.33mg/L, and both proportionings are 1:Certain potentiation is shown as, from poison when 1
During reason test result visible M: V (1: 1), it spends coefficient together is 148.35, and therefore this proportioning is optimum proportioning
Ultimate principle and principal character and the advantages of the present invention of the present invention have been shown and described above.The technology of the industry
, it should be appreciated that the present invention is not restricted to the described embodiments, the simply explanation described in above-described embodiment and description is originally for personnel
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and its
Equivalent thereof.
Claims (6)
1. a kind of composition pesticide with matrine and jervine preparation is used for preventing and treating the purposes of Camellia sinensis tea lesser leafhopper, its feature
It is, the mass ratio of described matrine and jervine is 3: 1～1: 3.
2. a kind of composition pesticide with matrine and jervine preparation according to claim 1 be used for preventing and treating Camellia sinensis tea little
The purposes of greenery Cicadae it is characterised in that：The mass ratio of described matrine and jervine is 1:1.
3. a kind of composition pesticide with matrine and jervine preparation according to claim 1 be used for preventing and treating Camellia sinensis tea little
The purposes of greenery Cicadae it is characterised in that：Described composition pesticide includes following dosage form：Wettable powder, water dispersible granules and outstanding
Floating agent.
4. a kind of composition pesticide with matrine and jervine preparation according to claim 3 be used for preventing and treating Camellia sinensis tea little
The purposes of greenery Cicadae it is characterised in that：Described wettable powder includes following component according to percent by weight：Matrine 0.3
～70%, jervine 0.3～70%, wetting agent 3～15%, dispersant 3-10%, carrier 8-10%, surplus supplied by filler.
5. a kind of composition pesticide with matrine and jervine preparation according to claim 3 be used for preventing and treating Camellia sinensis tea little
The purposes of greenery Cicadae it is characterised in that：Described water dispersible granules include following component according to percent by weight：Matrine 0.3
～70%, jervine 0.3～70%, dispersant 3～12%, wetting agent 2～8%, disintegrating agent 0～8%, binding agent 0～5%,
Filler 8～84%.
6. a kind of composition pesticide with matrine and jervine preparation according to claim 3 be used for preventing and treating Camellia sinensis tea little
The purposes of greenery Cicadae it is characterised in that：Described suspending agent includes following component according to percent by weight：Matrine 0.3～
40%th, jervine 0.3～30%, dispersant 3～12%, wetting agent 2～10%, defoamer 0.1～0.5%, thickening agent 0～
2%th, antifreeze 0～8%, balance of deionized water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310367287.7A CN103548898B (en) | 2013-08-21 | 2013-08-21 | Single matrine and composition pesticide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310367287.7A CN103548898B (en) | 2013-08-21 | 2013-08-21 | Single matrine and composition pesticide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103548898A CN103548898A (en) | 2014-02-05 |
| CN103548898B true CN103548898B (en) | 2017-03-08 |
Family
ID=50003404
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310367287.7A Active CN103548898B (en) | 2013-08-21 | 2013-08-21 | Single matrine and composition pesticide |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103548898B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105284941A (en) * | 2015-10-26 | 2016-02-03 | 广西农垦国有立新农场 | Novel insecticide, preparation method and application of novel insecticide |
| CN105409656B (en) * | 2015-11-25 | 2018-01-30 | 泰安市农业科学研究院 | A kind of Environment-friendly integrated control method of fragrant-flowered garlic maggot |
| CN105532682B (en) * | 2016-02-17 | 2018-03-23 | 陕西先农生物科技有限公司 | A kind of composition of plant insecticide containing jervine and preparation method |
| CN106172557A (en) * | 2016-07-20 | 2016-12-07 | 广西素安生态农业有限公司 | A kind of Folium Camelliae sinensis common pests herbal control agent and preparation method thereof |
| US20180146676A1 (en) * | 2016-11-30 | 2018-05-31 | Mclaughlin Gormley King Company | Mixtures of sabadilla alkaloids and insect growth regulators and uses thereof |
| CN106973949B (en) * | 2017-04-11 | 2019-06-11 | 四川农业大学 | A kind of Pesticidal combination and application thereof comprising bitter pueraria root extract and matrine |
| CN107624813A (en) * | 2017-10-23 | 2018-01-26 | 罗铭炽 | A kind of ecological agricultural chemical |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106994A (en) * | 1994-09-30 | 1995-08-23 | 袁波 | Ginseng ketone extract solution (pesticide) and preparing method |
| CN1613326A (en) * | 2004-08-30 | 2005-05-11 | 刘起麟 | Preparation for anti-fogery plant insecticide pesticide and use thereof |
| CN102228465A (en) * | 2011-04-26 | 2011-11-02 | 河北一兽药业有限公司 | Plant source insecticidal micron emulsion for aquatic product and preparation method thereof |
-
2013
- 2013-08-21 CN CN201310367287.7A patent/CN103548898B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106994A (en) * | 1994-09-30 | 1995-08-23 | 袁波 | Ginseng ketone extract solution (pesticide) and preparing method |
| CN1613326A (en) * | 2004-08-30 | 2005-05-11 | 刘起麟 | Preparation for anti-fogery plant insecticide pesticide and use thereof |
| CN102228465A (en) * | 2011-04-26 | 2011-11-02 | 河北一兽药业有限公司 | Plant source insecticidal micron emulsion for aquatic product and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103548898A (en) | 2014-02-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103548898B (en) | Single matrine and composition pesticide | |
| CN100384337C (en) | Health-caring highland barley tea and its preparing process | |
| CN105432690A (en) | Special disinfectant for Hu sheep farm | |
| CN102754756B (en) | Natural plant feed additive for improving tear stains of poodles and preparation method thereof | |
| CN101971927B (en) | Compound Chinese herb medicine addictive for culturing sea cucumber seedlings | |
| CN104886576A (en) | Female healthcare food and preparation method thereof | |
| CN105347408A (en) | Fishpond water cleaning agent | |
| CN106070377A (en) | A kind of jervine plant source compound antibacterial and application thereof | |
| CN103656505A (en) | Fish saprolegnia resisting traditional Chinese medicine extractive water aqua and preparation method thereof | |
| CN106539048A (en) | Edible selenium-rich areca-nut brine and method for preparing areca-nuts by using edible selenium-rich areca-nut brine | |
| CN110140808A (en) | Application method of the tea seed cake as aquatic livestock and ruminant additive | |
| CN105816693A (en) | Preparation process of dendrobium superfine powder | |
| CN102396647A (en) | Feed additive for preventing and treating porcine transmissible gastroenteritis | |
| CN104171375A (en) | Traditional Chinese medicine feed additive for preventing necrotic enteritis and preparation method thereof | |
| CN103341091B (en) | Traditional Chinese medicine particle designing powder for promoting growth of livestock and poultry as well as preparation method thereof | |
| CN104522668A (en) | Chinese forest frog particle and preparing method thereof | |
| CN104491708A (en) | External patch for treating mammitis and breast hyperplasia and relieving breast tumor pain and preparation method of patch for external use | |
| CN107353126A (en) | A kind of elm mushroom culture medium and preparation method thereof | |
| CN106667878A (en) | Moisturizing and whitening mask liquid containing herba dendrobii polysaccharides | |
| CN103385933B (en) | Catechu-containing traditional Chinese medicine preparation and preparation method thereof | |
| CN107950756A (en) | A kind of feed addictive for improving livestock and poultry production performance and its preparation method and application | |
| CN104256065A (en) | Traditional Chinese medicine composition for feeding eriocheir sinensis and use method | |
| CN104771477B (en) | Scattered Chinese herbal medicine of a kind of micro mist kidney biography branch and preparation method thereof | |
| CN104367680B (en) | Chinese and western medicine powder for preventing and treating duck serositis, and preparation method and application thereof | |
| CN107875204A (en) | A kind of Chinese herbal medicine for preventing and treating swine fever and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |