CN103520005B - A kind of mosquito repellent composition microcapsule and preparation method thereof and application - Google Patents
A kind of mosquito repellent composition microcapsule and preparation method thereof and application Download PDFInfo
- Publication number
- CN103520005B CN103520005B CN201310487309.3A CN201310487309A CN103520005B CN 103520005 B CN103520005 B CN 103520005B CN 201310487309 A CN201310487309 A CN 201310487309A CN 103520005 B CN103520005 B CN 103520005B
- Authority
- CN
- China
- Prior art keywords
- extract
- mosquito repellent
- weight portion
- oil
- repellent composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a kind of mosquito repellent composition microcapsule and preparation method thereof and application, described microcapsule prepares in accordance with the following methods: will have the plant extract of repelling effect, mix with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil and water, spraying dry obtains powder, is described mosquito repellent composition microcapsule.Mosquito repellent composition microcapsule of the present invention can directly act on human body or act on human body for the production of cosmetics, reaches the effect of long period mosquito repellent, and has anti-miliaria antipruritic effect simultaneously.
Description
Technical field
The invention relates to a kind of mosquito repellent composition microcapsule and preparation method thereof and application, particularly about a kind of be applied to cosmetics have anophelifuge concurrently, the compositions microcapsule and preparation method thereof of the effect such as antipruritic preparing the application in cosmetics with it, belongs to cosmetic technical field.
Background technology
Anophelifuge technology is a kind of technology of extensive use at China's cosmetic field; traditional has the repellant such as diethyltoluamide (DEET), mosquitofugal oil (DMP) or the citronellal etc. that mainly with the addition of chemosynthesis in the cosmetics of repelling effect; spread upon on skin; form protecting film, make mosquito dare not be close.But the repellant of this interpolation chemical composition may cause skin allergy.
Traditional has the repellant such as diethyltoluamide (DEET), mosquitofugal oil (DMP) or the citronellal etc. that mainly with the addition of chemosynthesis in the cosmetics of repelling effect, spreads upon on skin, forms protecting film, makes mosquito dare not be close.But the repellant of this interpolation chemical composition may cause allergy and stimulation to skin.
Also have in recent years and the research of plant extract as human body mosquito-repellent is reported, such as, utilize lemon scented gum extract, citronella oil, Oleum Pelargonii Graveolentis, Essential lavender oil, oil of rosemary, Oleum Caryophylli, Juniperus oxycedrus wet goods, but this is that the mosquito-repellent of main component is short for action time, generally at 1 ~ 2 hour with plant volatile oil.
CN101884608A discloses a kind of mosquito repellent composition, said composition is the early-stage Study of applicant in this case, it is made up of Semen Vitis viniferae extract, Flos Lonicerae extract, Flos Chrysanthemi Indici extract, Radix Glycyrrhizae extract, Herba Pogostemonis extract, Rhizoma Atractylodis extract, Flos Caryophylli extract, Radix Scutellariae extract and black tea extract, said composition can be used for preparing floral water, has anophelifuge, sterilization, anti-miliaria, the effect such as antipruritic concurrently.But find when practical application, the floral water be prepared into said composition, its anophelifuge persistency is not very good, and this product meets B level to Aedes albopictus repellent effect, and effective mosquito repellent time reaches 4 hours.
In addition, the cosmetics with repelling effect of prior art mostly are the liquid of spraying use, such as floral water etc., body surface liquid amount retained will be increased when health is perspired, although and some mosquito components are extracted form natural plant composition, because it is and human body skin Full connected, retain in human skin in a large number for a long time, how much can bring certain damage to skin.Separately, experiment and practical situations show, the usual color and luster of mosquito-driving liquid of existing extracted form natural plant composition is darker, will not easy cleaning and pollution clothes if to be sprayed onto on some medicated clothings, such as mosquito repellent composition disclosed in CN101884608A, itself be brown liquid, in the points for attention of commercially available back, clearly mark " be sure not to be sprayed on light medicated clothing, avoid painted ".
Summary of the invention
One object of the present invention is to provide a kind of mosquito repellent composition microcapsule, and said composition microcapsule can directly act on human body or act on human body for the production of cosmetics, reaches the effect of long period mosquito repellent, and has anti-miliaria antipruritic effect simultaneously.
One object of the present invention is to provide the preparation method of described mosquito repellent composition microcapsule.
One object of the present invention is to provide described mosquito repellent composition microcapsule preparing the application in cosmetics.
First, the invention provides a kind of mosquito repellent composition microcapsule, this microcapsule prepares in accordance with the following methods:
The plant extract of repelling effect will be had, mix with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil and water, spraying dry obtains powder, is described mosquito repellent composition microcapsule.
Present invention also offers a kind of method preparing described mosquito repellent composition microcapsule, the method comprises: will have the plant extract of repelling effect, to add water mixed preparing mixed liquor with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil, this mixed liquor is spray-dried makes powder, obtains described mosquito repellent composition microcapsule.
According to specific embodiment of the invention scheme, in the preparation process of mosquito repellent composition microcapsule of the present invention, the described plant extract with repelling effect can be any extract with repelling effect of the prior art, can be such as be selected from Flos Pelargonii Hortori, menthyl lactate, Chinese mugwort oil, eucalyptus citriodora oil, citronella oil, Cupressus funebris oil, pinke needle oil, Semen Vitis viniferae extract, Flos Lonicerae extract, Flos Chrysanthemi Indici extract, Radix Glycyrrhizae extract, Herba Pogostemonis extract, Rhizoma Atractylodis extract, Flos Caryophylli extract, Radix Scutellariae extract, and one or more the mixture in black tea extract.The all commercially available acquisition of each extract, also can record conventionally prepare voluntarily, each extract should meet related quality criterion requirement.
According to preferred specific embodiments of the present invention, the plant extract with repelling effect of the present invention can be adopt the mosquito repellent composition prepared by Semen Vitis viniferae, Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and black tea nine kind of plant in CN101884608A, also can be the mixture of at least two kinds in Flos Pelargonii Hortori, menthyl lactate, Chinese mugwort oil, eucalyptus citriodora oil, citronella oil, Cupressus funebris oil, pinke needle oil.
According to specific embodiment of the invention scheme, in the preparation process of mosquito repellent composition microcapsule of the present invention, the described plant extract with repelling effect, with the mixed proportion of starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil is:
There is plant extract 100 ~ 110 weight portion of repelling effect, starch ocentyl succinic aluminum 60 ~ 100 weight portion, maltodextrin 10 ~ 20 weight portion, beta-schardinger dextrin-10 ~ 20 weight portion, gelatin 4 ~ 15 weight portion, chitosan 0.4 ~ 1.6 weight portion, sodium alginate 0.5 ~ 1 weight portion, soybean lecithin 1 ~ 3 weight portion, Jojoba oil 10 ~ 20 weight portion.
According to specific embodiment of the invention scheme, for ensureing the concentration of anophelifuge effective ingredient in mosquito repellent composition microcapsule, just repelling effect can be reached to use suitable amount, in the preparation process of mosquito repellent composition microcapsule of the present invention, the described consumption with the plant extract of repelling effect is in wherein total solids content >=0.7%, is preferably 0.7% ~ 1.0%.
According to specific embodiment of the invention scheme, in the preparation process of mosquito repellent composition microcapsule of the present invention, described water is in order to each raw material mix homogeneously is coordinated mixed liquor, to utilize the carrying out of subsequent spray drying.One of ordinary skill in the art suitably can control the consumption of water as required.Usually, in the present invention, the consumption of water is 150 ~ 350 weight portions (be 100 ~ 110 parts by weight with the described consumptions with the plant extract of repelling effect).
According to specific embodiment of the invention scheme, in the preparation process of mosquito repellent composition microcapsule of the present invention, described spray-dired carrying out can according to the existing operation in affiliated field.The spray drying condition preferably controlled in the present invention is: inlet temperature 160 ~ 180 DEG C, leaving air temp 80 ~ 100 DEG C.To other conditions of drying process with atomizing without particular requirement.
In addition, according to specific embodiment of the invention scheme, there is the plant extract of repelling effect and starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil and add water the mixed liquor of mixed preparing before carrying out spraying dry, homogenizing process can be carried out, preferred homogenization pressure is 15 ~ 35MPa, conventional homogenizing temperature substantially without impact, for room temperature or can suitably be heated to 50 ~ 75 DEG C to repelling effect of the present invention.Mixed liquor before homogenizing also can some insoluble large particulate matters of filtering (such as, can cross 100 mesh screen) as required.
By analysis, mosquito repellent composition microcapsule of the present invention, mainly provides the kernel of anophelifuge microcapsule with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-; Using gelatin, chitosan, sodium alginate as attachment adhesive, anophelifuge substance is attached on kernel, and anophelifuge substance rate of release is slowed down; Described soybean lecithin, Jojoba oil can, as liposome, make anophelifuge substance rate of release slow down further.
Mosquito repellent composition microcapsule of the present invention, use natural anophelifuge composition to drive away mosquito, to human-body safety nonhazardous effect, and the present invention is by making a kind of microcapsule to the particular procedure of natural anophelifuge composition, its steady quality, anophelifuge persistency (mosquito repellent time is more than 6 hours) can be extended, and Aedes albopictus repellent effect not reduced along with the prolongation of time.Mosquito repellent composition microcapsule of the present invention has anophelifuge, anti-miliaria, the effect such as antipruritic concurrently, directly can use, is applied in skin surface, also can be further used for preparing cosmetics, such as, be prepared into talcum powder or emulsion etc.
On the other hand, present invention also offers described mosquito repellent composition microcapsule as the application had in the cosmetics of anophelifuge, anti-miliaria and/or antipruritic effect.
On the other hand, present invention also offers a kind of cosmetics, wherein containing mosquito repellent composition microcapsule of the present invention.Described cosmetics can be such as talcum powder, or moisturizer etc.
Experiment proves, technical scheme of the present invention, through mosquito component and suitable component being carried out after process is prepared into powder, can obtain following useful technique effect:
The first, anophelifuge microcapsule of the present invention can delay the release time of mosquito component, meets A level to Aedes albopictus repellent effect, and effective mosquito repellent time reaches 6 hours.
The second, human body owing to there being the existence of sweat gland, therefore has the phenomenon of perspire, especially when summer more very, and anophelifuge microcapsule of the present invention this as pressed powder, soft, dry and comfortable, lubricious, there is the effect of talcum powder, meet QB/T1859 XIANGFEN, talcum powder, prickly-heat powder standard-required.
3rd, anophelifuge microcapsule of the present invention is pressed powder and has the existence of liposome layer, although when smearing and contact with clothing, anophelifuge microcapsule only adheres at clothing surface, medicated clothing can make anophelifuge microcapsule and clothing surface depart from when firmly shaking, not pollution clothes.
Detailed description of the invention
Describe the beneficial effect of implementation process of the present invention and generation below by way of specific embodiment in detail, be intended to help reader to understand essence of the present invention and feature better, not as can the restriction of practical range to this case.
Following scheme of the present invention describes and in formula:
The plant extract of repelling effect used is self-control, brown liquid, total solids content >=0.7%.
Semen Vitis viniferae extract used is commercial products, is the extract of the seed from vitaceae Fructus Vitis viniferae (Vitis vinifera L.), red-brown powder, there is no foreign odor taste, absworption peak 280nm, 256nm, total number of bacteria≤1000/g, procyanidin content >=96%.
Flos Pelargonii Hortori used is commercial products, is the extract from Flos Pelargonii seed, brownish-yellow powder, and specification is 10%, total number of bacteria≤1000/g.
Embodiment 1
Mix being purchased Chinese herbal medicine Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and the black tea ratio according to Flos Lonicerae 0.5 weight portion, Flos Chrysanthemi Indici 1 weight portion, Radix Glycyrrhizae 0.5 weight portion, Herba Pogostemonis 0.2 weight portion, Rhizoma Atractylodis 0.1 weight portion, Flos Caryophylli 0.05 weight portion, Radix Scutellariae 0.1 weight portion, black tea 0.05 weight portion, pulverizer is utilized to grind, then be dipped in the ethanol of 30 times of weight, room temperature (18 DEG C ~ 25 DEG C) soaks 72 hours, by medicinal residues filtering, obtain mixing Chinese medicine extraction liquid.It is brown liquid, and after testing, wherein total solids content is about 0.8%.
Get the mixing Chinese medicine extraction liquid 100g extracted according to the method described above, with Flos Pelargonii Hortori 5g, 80 grams, starch ocentyl succinic aluminum, maltodextrin 10 grams, beta-schardinger dextrin-10 grams, 14 grams, gelatin, chitosan 0.4 gram, sodium alginate 0.6 gram, soybean lecithin 1.2 grams, Semen Vitis viniferae extract 0.1 gram, Jojoba oil 20 grams and water 250 grams of mixing and stirring.Cross 100 mesh sieves, obtain filtrate.Filtrate carries out spraying dry after homogenizing under 30MPa pressure, spray drying condition: inlet temperature 175 DEG C, leaving air temp 90 DEG C.Obtain light brown powder after spraying dry, be the mosquito repellent composition microcapsule of the present embodiment.
Embodiment 2
Mix being purchased Chinese herbal medicine Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and the black tea ratio according to Flos Lonicerae 0.55 weight portion, Flos Chrysanthemi Indici 0.9 weight portion, Radix Glycyrrhizae 0.4 weight portion, Herba Pogostemonis 0.2 weight portion, Rhizoma Atractylodis 0.08 weight portion, Flos Caryophylli 0.04 weight portion, Radix Scutellariae 0.08 weight portion, black tea 0.04 weight portion, pulverizer is utilized to grind, then be dipped in the ethanol of 33 times of weight, room temperature (18 DEG C ~ 25 DEG C) soaks 78 hours, by medicinal residues filtering, obtain mixing Chinese medicine extraction liquid.It is brown liquid, and after testing, wherein total solids content is about 0.7%.
Get the mixing Chinese medicine extraction liquid 100g extracted according to the method described above, with Flos Pelargonii Hortori 0.2g, menthyl lactate 0.1g, the oily 0.2g that ends, eucalyptus citriodora oil 0.3g, Semen Vitis viniferae extract 0.1 gram, 80 grams, starch ocentyl succinic aluminum, maltodextrin 20 grams, beta-schardinger dextrin-20 grams, 4 grams, gelatin, chitosan 1.2 grams, sodium alginate 1 gram, soybean lecithin 2 grams, Jojoba oil 15 grams and water 280 grams of mixing and stirring.Cross 100 mesh sieves, obtain filtrate.Filtrate carries out spraying dry after homogenizing under 30MPa pressure, spray drying condition: inlet temperature 175 DEG C, leaving air temp 99 DEG C.Obtain light brown powder after spraying dry, be the mosquito repellent composition microcapsule of the present embodiment.
Embodiment 3
Mix being purchased Chinese herbal medicine Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and the black tea ratio according to Flos Lonicerae 0.45 weight portion, Flos Chrysanthemi Indici 1.1. weight portion, Radix Glycyrrhizae 0.6 weight portion, Herba Pogostemonis 0.15 weight portion, Rhizoma Atractylodis 0.13 weight portion, Flos Caryophylli 0.06 weight portion, Radix Scutellariae 0.12 weight portion, black tea 0.06 weight portion, pulverizer is utilized to grind, then be dipped in the ethanol of 30 times of weight, room temperature (18 DEG C ~ 25 DEG C) soaks 78 hours, by medicinal residues filtering, obtain mixing Chinese medicine extraction liquid.It is brown liquid, and after testing, wherein total solids content is about 0.85%.
Get the mixing Chinese medicine extraction liquid 100g extracted according to the method described above, with Chinese mugwort oily 0.1g, citronella oil 0.3g, Cupressus funebris oil 0.1g, pinke needle oil 0.5g, 80 grams, starch ocentyl succinic aluminum, maltodextrin 12 grams, beta-schardinger dextrin-18 grams, 10 grams, gelatin, chitosan 1.6 grams, sodium alginate 0.8 gram, soybean lecithin 3 grams, Semen Vitis viniferae extract 0.1 gram, Jojoba oil 10 grams and water 220 grams of mixing and stirring.Cross 100 mesh sieves, obtain filtrate.Filtrate carries out spraying dry after homogenizing under 30MPa pressure, spray drying condition: inlet temperature 175 DEG C, leaving air temp 99 DEG C.Obtain light brown powder after spraying dry, be the mosquito repellent composition microcapsule of the present embodiment.
Comparative example 1
Mix being purchased Chinese herbal medicine Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and the black tea ratio according to Flos Lonicerae 0.5 weight portion, Flos Chrysanthemi Indici 1 weight portion, Radix Glycyrrhizae 0.5 weight portion, Herba Pogostemonis 0.2 weight portion, Rhizoma Atractylodis 0.1 weight portion, Flos Caryophylli 0.05 weight portion, Radix Scutellariae 0.1 weight portion, black tea 0.05 weight portion, pulverizer is utilized to grind, then be dipped in the ethanol of 30 times of weight, room temperature (18 DEG C ~ 25 DEG C) soaks 72 hours, by medicinal residues filtering, obtain mixing Chinese medicine extraction liquid.
Get the mixing Chinese medicine extraction liquid 100g extracted according to the method described above, with Flos Pelargonii Hortori 5g, 80 grams, starch ocentyl succinic aluminum, maltodextrin 10 grams, beta-schardinger dextrin-10 grams, soybean lecithin 2.5 grams, Semen Vitis viniferae extract 0.1 gram, Jojoba oil 20 grams and water 250 grams of mixing and stirring.Cross 100 mesh sieves, obtain filtrate.Filtrate carries out spraying dry after homogenizing under 30MPa pressure, spray drying condition: inlet temperature 175 DEG C, leaving air temp 90 DEG C.Obtain light brown powder after spraying dry, be the mosquito repellent composition microcapsule of the present embodiment.
Comparative example 2
Mix being purchased Chinese herbal medicine Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and the black tea ratio according to Flos Lonicerae 0.5 weight portion, Flos Chrysanthemi Indici 1 weight portion, Radix Glycyrrhizae 0.5 weight portion, Herba Pogostemonis 0.2 weight portion, Rhizoma Atractylodis 0.1 weight portion, Flos Caryophylli 0.05 weight portion, Radix Scutellariae 0.1 weight portion, black tea 0.05 weight portion, pulverizer is utilized to grind, then be dipped in the ethanol of 30 times of weight, room temperature (18 DEG C ~ 25 DEG C) soaks 72 hours, by medicinal residues filtering, obtain mixing Chinese medicine extraction liquid.
Get the mixing Chinese medicine extraction liquid 100g extracted according to the method described above, with Flos Pelargonii Hortori 5g, 50 grams, starch ocentyl succinic aluminum, beta-schardinger dextrin-20 grams, 2.5 grams, gelatin 10 parts by weight of soybean lecithin, Semen Vitis viniferae extract 0.1 gram, Jojoba oil 20 grams and water 250 grams of mixing and stirring.Cross 100 mesh sieves, obtain filtrate.Filtrate carries out spraying dry after homogenizing under 30MPa pressure, spray drying condition: inlet temperature 175 DEG C, leaving air temp 90 DEG C.Obtain light brown powder after spraying dry, be the mosquito repellent composition microcapsule of the present embodiment.
Anophelifuge is tested:
Carry out according to GB/T17322.10-1998.Experimenter is 45 people, is divided into three groups, often organizes 15 people, tests respectively to the anophelifuge microcapsule of the embodiment of the present invention 1,2,3.Everyone is blank on the other hand, and another hands presses 1.5mg/cm
2dose uniformity smear 5cm × 5cm the back of the hand region, expose wherein 4cm × 4cm position, remainder tightly covers.Spread product 2 hours, starts to test.Test result sees table.
Experimental result shows, the anophelifuge microcapsule of the embodiment of the present invention 1,2,3 all meets A level to Aedes albopictus repellent effect, and effective mosquito repellent time reaches 6 hours.And the anophelifuge microcapsule of comparative example 1 meets B level to Aedes albopictus repellent effect, effective mosquito repellent time reaches 4 hours; Be do not add gelatin, chitosan, sodium alginate through the reason that the effective mosquito repellent time of relative analysis is short, do not make anophelifuge substance rate of release slow down.Although the anophelifuge microcapsule of comparative example 2 with the addition of some starch ocentyl succinic aluminum, beta-schardinger dextrin-and gelatin in preparation process, gained dry powder also just reaches Aedes albopictus repellent effect and meets B level, and effective mosquito repellent time reaches 4 hours; Its repelling effect is not as good as the anophelifuge microcapsule prepared according to formula of the present invention.
The antipruritic test of anti-miliaria:
Select 450 volunteers to participate in free trial activity in summer, be divided into three groups, often organize 150 people, respectively the microcapsule of the embodiment of the present invention 1,2,3 is tested.The using method of microcapsule of the present invention: be (1) applied in skin desired area with appropriate powder; (2) be applied in mosquito bite rear in right amount by this product.
Test after 60 days, to the evaluation result record of result of use as following table:
As can be seen from the above table, consumer is to the situation using the anti-miliaria of cosmetics of the present invention antipruritic, and satisfaction rate can reach more than 90%, Be very effective.And in using, it is easy to use that cosmetics of the present invention generally react in consumer, health, pollution-free medicated clothing situation occurs, and soft, dry and comfortable, lubricious, and skinfeel is better, fragrant, makes us taking like a shot.
Claims (8)
1. a mosquito repellent composition microcapsule, this microcapsule prepares in accordance with the following methods:
The plant extract of repelling effect will be had, mix with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil and water, spraying dry obtains powder, is described mosquito repellent composition microcapsule;
Wherein, described in there is the plant extract of repelling effect, with the mixed proportion of starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil be:
There is plant extract 100 ~ 110 weight portion of repelling effect, starch ocentyl succinic aluminum 60 ~ 100 weight portion, maltodextrin 10 ~ 20 weight portion, beta-schardinger dextrin-10 ~ 20 weight portion, gelatin 4 ~ 15 weight portion, chitosan 0.4 ~ 1.6 weight portion, sodium alginate 0.5 ~ 1 weight portion, soybean lecithin 1 ~ 3 weight portion, Jojoba oil 10 ~ 20 weight portion;
Wherein, the plant extract described in repelling effect is selected from one or more the mixture in Flos Pelargonii Hortori, menthyl lactate, Chinese mugwort oil, eucalyptus citriodora oil, citronella oil, Cupressus funebris oil, pinke needle oil, Semen Vitis viniferae extract, Flos Lonicerae extract, Flos Chrysanthemi Indici extract, Radix Glycyrrhizae extract, Herba Pogostemonis extract, Rhizoma Atractylodis extract, Flos Caryophylli extract, Radix Scutellariae extract and black tea extract; Described have total solids content >=0.7% in the plant extract of repelling effect.
2. mosquito repellent composition microcapsule according to claim 1, wherein having total solids content in the plant extract of repelling effect is 0.7% ~ 1.0%.
3. mosquito repellent composition microcapsule according to claim 1, wherein, the described plant extract with repelling effect is the mosquito repellent composition prepared by Semen Vitis viniferae, Flos Lonicerae, Flos Chrysanthemi Indici, Radix Glycyrrhizae, Herba Pogostemonis, Rhizoma Atractylodis, Flos Caryophylli, Radix Scutellariae and black tea nine kind of plant, or is selected from the mixture of at least two kinds in Flos Pelargonii Hortori, menthyl lactate, Chinese mugwort oil, eucalyptus citriodora oil, citronella oil, Cupressus funebris oil, pinke needle oil.
4. the preparation method of the mosquito repellent composition microcapsule described in any one of claims 1 to 3, the method comprises:
The plant extract of repelling effect will be had, to add water mixed preparing mixed liquor with starch ocentyl succinic aluminum, maltodextrin, beta-schardinger dextrin-, gelatin, chitosan, sodium alginate, soybean lecithin, Jojoba oil, this mixed liquor is spray-dried makes powder, obtains described mosquito repellent composition microcapsule.
5. preparation method according to claim 4, wherein, described spray drying condition is: inlet temperature 160 ~ 180 DEG C, leaving air temp 80 ~ 100 DEG C.
6. the mosquito repellent composition microcapsule described in any one of claims 1 to 3 is preparing the application had in the cosmetics of anophelifuge, anti-miliaria and/or antipruritic effect.
7. cosmetics, wherein containing the mosquito repellent composition microcapsule described in any one of claims 1 to 3.
8. cosmetics according to claim 7, it is moisturizer or talcum powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310487309.3A CN103520005B (en) | 2013-10-17 | 2013-10-17 | A kind of mosquito repellent composition microcapsule and preparation method thereof and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310487309.3A CN103520005B (en) | 2013-10-17 | 2013-10-17 | A kind of mosquito repellent composition microcapsule and preparation method thereof and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103520005A CN103520005A (en) | 2014-01-22 |
| CN103520005B true CN103520005B (en) | 2015-09-02 |
Family
ID=49922598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310487309.3A Active CN103520005B (en) | 2013-10-17 | 2013-10-17 | A kind of mosquito repellent composition microcapsule and preparation method thereof and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103520005B (en) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103655245B (en) * | 2012-08-31 | 2015-03-11 | 郭心仪 | Mosquito repelling flora water |
| CN103931670B (en) * | 2014-04-08 | 2015-09-09 | 许银亚 | Jojoba oil vaporizer mosquito liquid |
| CN104288051A (en) * | 2014-10-16 | 2015-01-21 | 武汉嘉润天合信息科技有限公司 | Compound traditional Chinese medicine mosquito repellent |
| CN104480724A (en) * | 2014-12-05 | 2015-04-01 | 南通大学 | Functional natural plant mosquito repelling ecological home textile product |
| CN104873419B (en) * | 2015-05-19 | 2018-02-02 | 天津郁美净集团有限公司 | The preparation and application of one kind of multiple plant compositions and its extract, microcapsules |
| BE1023579B1 (en) * | 2015-11-05 | 2017-05-09 | LOëN HOLDING S.A.R.L. | REPULSIVE ACCESSORIES AGAINST CHIPS, MITES AND INSECTS |
| CN105926287A (en) * | 2016-06-16 | 2016-09-07 | 东莞市联洲知识产权运营管理有限公司 | Purely-natural and mosquito-repelling fabric for infants and production method of purely-natural and mosquito-repelling fabric |
| CN106361618B (en) * | 2016-09-12 | 2019-06-18 | 华南理工大学 | A kind of sustained release mosquito-repellent essential oil microcapsules children's talcum powder and preparation method thereof |
| CN106491432A (en) * | 2016-11-25 | 2017-03-15 | 江苏爱西施科技服务咨询股份有限公司 | A kind of fibroin prickly-heat powder with removing dampness to relieve itching effect and preparation method thereof |
| CN106491374B (en) * | 2016-12-06 | 2020-01-10 | 广州睿森生物科技有限公司 | Nepetalactone microcapsule, preparation method thereof and application of nepetalactone microcapsule in preparation of mosquito repellent product |
| CN106580776A (en) * | 2016-12-11 | 2017-04-26 | 东莞小猕猴户外用品有限公司 | Preparation method of long-acting mosquito repellent liquid and long-acting mosquito repellent liquid |
| CN107996619A (en) * | 2017-11-20 | 2018-05-08 | 徐纳川 | A kind of natural anophelifuge agent and preparation method |
| CN109260056A (en) * | 2018-11-06 | 2019-01-25 | 北京爸爸的选择科技有限公司 | A kind of mosquito-proof sting bath foam of infant's draft and preparation method thereof |
| CN111903717A (en) * | 2020-09-01 | 2020-11-10 | 张增香 | Mosquito-repelling microcapsule and application thereof |
| CN113273571A (en) * | 2021-06-07 | 2021-08-20 | 山东安然纳米实业发展有限公司 | Mosquito-repelling cool-feeling dual-functional cross-linked microcapsule and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101444495A (en) * | 2008-12-31 | 2009-06-03 | 江南大学 | Vitamin E microcapsule preparation method |
| CN101884608A (en) * | 2010-07-09 | 2010-11-17 | 天津郁美净集团有限公司 | Mosquito repelling composition |
| CN102835925A (en) * | 2012-09-18 | 2012-12-26 | 铜陵洁雅生物科技股份有限公司 | Plant type mosquito repelling wet tissue |
-
2013
- 2013-10-17 CN CN201310487309.3A patent/CN103520005B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101444495A (en) * | 2008-12-31 | 2009-06-03 | 江南大学 | Vitamin E microcapsule preparation method |
| CN101884608A (en) * | 2010-07-09 | 2010-11-17 | 天津郁美净集团有限公司 | Mosquito repelling composition |
| CN102835925A (en) * | 2012-09-18 | 2012-12-26 | 铜陵洁雅生物科技股份有限公司 | Plant type mosquito repelling wet tissue |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103520005A (en) | 2014-01-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103520005B (en) | A kind of mosquito repellent composition microcapsule and preparation method thereof and application | |
| CN103735468B (en) | A kind of cosmetics containing mosquito repellent composition microcapsule | |
| CN105594755B (en) | A kind of plant mosquito-repellent and the preparation method with repelling effect fabric | |
| CN101884608B (en) | Mosquito repelling composition | |
| CN101146513B (en) | Cosmetic material containing sweet pea extract | |
| CN105112181A (en) | Functional plant essential oil handmade soap and preparation method thereof | |
| CN104771353A (en) | Cream used for deep cleaning and caring of face skin | |
| CN106176332A (en) | The disposable hair-washing composition of foam type | |
| CN106236624A (en) | A kind of hydrogel facial film with whitening effect and preparation method thereof | |
| CN106344437A (en) | Folium artemisiae argyi anti-mosquito lotion and preparation method thereof | |
| CN102440937A (en) | Healthcare wet tissue with antimicrobial and anti-acne functions | |
| CN105816362A (en) | Repellent lotion for infants | |
| CN108158918A (en) | Wrap up microcapsules of natural extract and preparation method thereof and microcapsule-type lipstick | |
| CN102335103A (en) | Essential oil with mosquito-dispelling function | |
| CN103340798A (en) | Natural plant sun cream and preparation process thereof | |
| CN105326737A (en) | Traditional Chinese medicine acne removing mask creme | |
| CN109512764A (en) | Natural plants ferment essence hydrosol and the preparation method and application thereof | |
| CN104013554A (en) | Traditional Chinese medicine-based whitening freckle-removing emulsion mask of W/O/W system and preparation method thereof | |
| CN104188872A (en) | Environmental protection moisture type water-based nail polish and preparation method thereof | |
| CN107823004A (en) | Plant composition with anti-sunlight function and its application in sunscreen product | |
| CN112680279A (en) | Natural medicinal fragrant plant composite essential oil and essential oil soap with sterilizing and anti-inflammation functions and preparation method thereof | |
| CN102793640B (en) | Vitiligo covering composition and preparation method thereof | |
| CN106176516A (en) | One is calmed the nerves perfume | |
| CN106635527A (en) | Young-keeping and skin-whitening soap and preparation method thereof | |
| CN106074276A (en) | A kind of nanometer Deacne pack containing Chinese medicine ingredients and its preparation method and application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |