CN104188872A - Environmental protection moisture type water-based nail polish and preparation method thereof - Google Patents
Environmental protection moisture type water-based nail polish and preparation method thereof Download PDFInfo
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Abstract
The invention discloses environmental protection moisture type water-based nail polish and a preparation method of the environmental protection moisture type water-based nail polish. The preparation comprises the following substances: povidone, polyvinyl alcohol, bletilla extract, sodium carboxymethyl cellulose, glycerin, 75% ethanol, vitamin B1, vitamin C, lavender extract, angelica extract, lily extract, essence, distilled water, pearl pigment or pigment, nipagin esters and a 3% ethylenediamine tetraacetic acid disodium salt solution. The environmental protection moisture type water-based nail polish prepared by the invention is transparent and crystal, appropriate in consistency, good in stability, harmless, non-irritating and fragrant in smell; when the environmental protection moisture type water-based nail polish is smeared on nails, not only the aesthetic feeling is enhanced, but also a moisturizing effect on the nails is realized, so that the nails are kept ruddy and shining.
Description
Technical field
The present invention relates to a kind of environmental protection and moisten type water-based nail polish and preparation method thereof, particularly type water-based nail polish and preparation method thereof is moistened in a kind of environmental protection containing natural component extract.
Background technology
Traditional nial polish claims again " nail varuish ".Its main component is the volatile organic solvent of 60%-70%, the nitrocellulose of 20% left and right, a small amount of oil-based solvent, Camphora, titanium dioxide and oil colour etc.
Acetone in the raw material of traditional nial polish, ethyl acetate, nitrocellulose etc. have certain bio-toxicity, inflammable and explosive, when volatilization, produce the penetrating odor of giddy, room air is polluted to (volume after organic solvent volatilization will expand 1,000 times), the in the situation that of long-term suction, not only human body respiration mucous membrane is had to strong zest, and nervous system is also had to harm.The principle that nial polish is attached to nail surface is first by fingernail surface damage, produces many coarse duck eyes on surface, and nial polish infiltrates in pothole, and under life-time service, pigment easily precipitates, and fingernail is easily yellow, dry and cracked, and many women of liking to be beautiful have sacrificed health for this reason.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of environmental protection and moisten type water-based nail polish with pure water, the filmogen of environmental protection is main component, green, environmental protection, nontoxic.
The present invention also provides a kind of environmental protection to moisten the preparation method of type water-based nail polish.
Type water-based nail polish is moistened in a kind of environmental protection provided by the invention, by the raw material of following content, is prepared from:
Described Radix Angelicae Dahuricae extracting solution is prepared by the following method:
Take the Radix Angelicae Dahuricae appropriate, soak 0.15-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and obtain Radix Angelicae Dahuricae extracting solution.
Described Rhizoma Bletillae extraction solution is prepared by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.15-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and obtain Rhizoma Bletillae extraction solution.
Described lavandula angustifolia extracting solution is prepared by the following method:
Take lavandula angustifolia appropriate, in 90-100 ℃ of extraction 2 times, add the 5-25 times of water yield the 1st time, extract 0.5-2h, the 2nd time by the 5-20 times of water yield, extracts 0.5-2h, at every turn with 3 layers of gauzes filtration, merging filtrate, heating is concentrated into 5-20 times of g/ml of lavandula angustifolia weight, obtains lavandula angustifolia extracting solution.
Described Bulbus Lilii extracting solution is prepared by the following method:
Take Bulbus Lilii appropriate, soak 0.5-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 10-15 times of water gaging the 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 4-7 times of g/ml of Bulbus Lilii weight, adds liquid weight 1%-5% active carbon, and 80-100 ℃ of heating in water bath stirs, sucking filtration, gets filtrate, obtains Bulbus Lilii extracting solution.
Described pearlescent pigment or the color of pigment are bright cherry-red, crocus, rose-red, grass green, turquoise.
The preparation method of type water-based nail polish is moistened in a kind of environmental protection provided by the invention, comprises the following steps:
A) weighing polyvinyl alcohol 10-15g, polyvidon 1-10g, be dissolved in 50-80ml distilled water, stir, within standing 24 hours, treat its natural swelling, dissolving, be warming up to 80-90 ℃, insulation 10-30 minute, adds sodium carboxymethyl cellulose 0.1-1g, until swelling is complete, form the substrate of clear;
B) take glycerol 1-5g, Rhizoma Bletillae extraction solution 1-5g, lavandula angustifolia extracting solution 0.1-1g, Radix Angelicae Dahuricae extracting solution 0.1-1g, Bulbus Lilii extracting solution 0.1-1g, vitamin B
10.1-0.5g, vitamin C 0.1-0.5g, stir 1-5min, mix homogeneously;
C) by step b) gained mixed solution adds step a) in gained substrate, is uniformly mixed;
D) with 75% ethanol 1-5g, dissolve ethyl hydroxybenzoate 0.1-0.3g, be mixed with antiseptic solution, add step c) in gained solution, be uniformly mixed;
E) get 3% disodium ethylene diamine tetra-acetic acid solution 0.01-0.05g, pearlescent pigment or pigment 0.05-0.1g, essence 0.1-1.3ml, add steps d) in mixed solution, heat while stirring it is dissolved, mix homogeneously, obtains environmental protection and moistens type water-based nail polish.
Various compositions in the present invention are as follows:
Lavandula angustifolia is to generally acknowledge to have calmness most, releives, and the plant of syngignoscism.It can releive intense strain, calm mind, calms down pneumostatic, and Jiu You hospital is extracting the volatile oil that comes for improving old people's sleep from lavandula angustifolia abroad.In Xinjiang, neurasthenia and insomnia are also treated with lavandula angustifolia herb preparation by a lot of Uygur medicine hospitals.Research discovery, lavandula angustifolia has obvious antibacterial action, and the linalool containing in lavandula angustifolia is the antibacterial main component of lavandula angustifolia, and it can suppress the growth of 17 kinds of antibacterials (comprising gram-negative bacteria and gram-positive bacteria), 10 kinds of funguses.
The Pseudobulbus Bletillae (Rhizoma Bletillae), Bulbus Lilii, Radix Angelicae Dahuricae extracting solution extract from natural plants, nontoxic, to skin without anaphylaxis and carcinogenecity.These natural botanical extraction liquids have the effect of moistening maintenance fingernail, can make more satin of fingernail.Rhizoma Bletillae extraction solution is good filmogen, can form thin film at nail surface.
B is deficient in vitamin
1, easily make fingernail fragile; The tissue inflammation of agnail and fingernail surrounding is relevant with the C that is deficient in vitamin.
Glycerol is pleasantly sweet, is water white transparency viscous liquid, is the most ancient wetting agent, before more than ten years, a lot of people directly add water nursing skin with glycerol, safe and cheap, are the maximum prevailing wetting agents of content in cosmetics, there is good water absorption, be commonly used to do the interpolation raw material of cosmetics.The glycerol that purity is higher is watered rear use, and moisturizing effect is very good, with rear soft skin, touches up very comfortable.Glycerol is a kind of non-irritating and the natural plants wetting agent that can lock moisture, can be used as personal care product's softening agent, moisturizing agent and emollient.
The object of the invention is to develop a kind of environmental protection and moisten type water-based nail polish and using pure water as solvent, environment-friendly materials are as filmogen, and have added plant component and comprise the Pseudobulbus Bletillae (Rhizoma Bletillae), Bulbus Lilii, the Radix Angelicae Dahuricae, vitamin B
1, vitamin C, lavandula angustifolia etc. be to fingernail Yellow Gentian Extract.The present invention has abandoned traditional oiliness nial polish take the preparation that a large amount of poisonous, harmful organic solvents is main component, develops environmental protection, nontoxic nial polish product.
The specific embodiment
Below in conjunction with embodiment, the present invention will be further described.
Glycerol of the present invention, essence, vitamin B
1, vitamin C is commercially available.
Embodiment 1
The preparation of 1.1 Radix Angelicae Dahuricae extracting solution:
Take Radix Angelicae Dahuricae 30g, soak 0.45h, be heated to 100 ℃, decoct and extract 3 times, add 12 times of water gagings the 1st time, extract 1.5h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time, extract 0.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filter, obtain Radix Angelicae Dahuricae extracting solution.
The preparation of 1.2 Rhizoma Bletillae extraction solution:
Take Pseudobulbus Bletillae (Rhizoma Bletillae) 40g, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 8 times of water gagings the 1st time, extract 1h, add 6 times of water gagings the 2nd time, extract 1h, add 5 times of water gagings the 3rd time, extract 0.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 4 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and get final product.
The preparation of 1.3 lavandula angustifolia extracting solution:
Take lavandula angustifolia 25g, be heated to 100 ℃, decoct and extract 2 times, add 10 times of water yields the 1st time, extract 1h, 8 times of water yields of the 2nd use, extract 1h, with 3 layers of gauze, filter at every turn, and merging filtrate, heating is concentrated into 5 times of g/ml of lavandula angustifolia weight, standby.
The preparation of 1.4 Bulbus Lilii extracting solution:
Take Bulbus Lilii 20g, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 10 times of water gagings the 1st time, extract 1h, add 8 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings the 3rd time, extract 1h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 5 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, adds amount of liquid 4% active carbon, and 80 ℃ of heating in water bath stir, sucking filtration, gets filtrate, standby.
The preparation of type water-based nail polish is moistened in 1.5 1 kinds of environmental protection:
A) weighing polyvinyl alcohol 15g and polyvidon 10g, be dissolved in 70ml water, stirs, within standing 24 hours, treat its natural swelling dissolving, be warming up to 90 ℃, be incubated 25 minutes, add sodium carboxymethyl cellulose 0.1g, until swelling is complete, form the substrate of clear.
B) take glycerol 3g, Rhizoma Bletillae extraction solution 5g, lavandula angustifolia extracting solution 0.5g, Radix Angelicae Dahuricae extracting solution 0.5g, Bulbus Lilii extracting solution 0.5g, vitamin B
10.1g, vitamin C 0.1g, stir 5min, mix homogeneously.
C) by step b) gained mixed solution adds step a) in gained substrate, is uniformly mixed;
D) with 75% ethanol 5g, dissolve ethyl hydroxybenzoate 0.1g and be mixed with antiseptic solution, add step c) in gained solution, be uniformly mixed;
E) take 3% disodium ethylene diamine tetra-acetic acid solution 0.03g, bright cherry-red pearlescent pigment 0.1g, essence 0.2ml, add steps d) in mixed solution, heat while stirring it is dissolved, mix homogeneously, obtains environmental protection and moistens type water-based nail polish.
Embodiment 2
The preparation of 2.1 Radix Angelicae Dahuricae extracting solution:
Take Radix Angelicae Dahuricae 40g, soak 1h, be heated to 100 ℃, decoct and extract 3 times, add 10 times of water gagings the 1st time, extract 1.5h, add 10 times of water gagings the 2nd time, extract 1.5h, add 7 times of water gagings the 3rd time, extract 1h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filter, obtain Radix Angelicae Dahuricae extracting solution.
The preparation of 2.2 Rhizoma Bletillae extraction solution:
Take Pseudobulbus Bletillae (Rhizoma Bletillae) 50g appropriate, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 10 times of water gagings the 1st time, extract 1.5h, add 6 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings the 3rd time, extract 0.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 5 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and get final product.
The preparation of 2.3 lavandula angustifolia extracting solution:
Take lavandula angustifolia 20g, be heated to 100 ℃, decoct and extract 2 times, add 5 times of water yields the 1st time, extract 0.5h, 5 times of water yields of the 2nd use, extract 0.5h, with 3 layers of gauze, filter at every turn, and merging filtrate, heating is concentrated into 5 times of g/ml of lavandula angustifolia weight, standby.
The preparation of 2.4 Bulbus Lilii extracting solution:
Take Bulbus Lilii 20g, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 10 times of water gagings the 1st time, extract 1h, add 8 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings the 3rd time, extract 1h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 4 times of g/ml of Bulbus Lilii weight, adds amount of liquid 4% active carbon, and 90 ℃ of heating in water bath stir, sucking filtration, gets filtrate, standby.
The preparation of type water-based nail polish is moistened in 2.5 1 kinds of environmental protection:
A) weighing polyvinyl alcohol 15g and polyvidon 5g, be dissolved in 70ml water, stirs, within standing 24 hours, treat its natural swelling dissolving, be warming up to 90 ℃, be incubated 25 minutes, add sodium carboxymethyl cellulose 0.05g, until swelling is complete, form the substrate of clear.
B) take glycerol 2g, Rhizoma Bletillae extraction solution 4g, lavandula angustifolia extracting solution 0.4g, Radix Angelicae Dahuricae extracting solution 0.4g, Bulbus Lilii extracting solution 0.4g, vitamin B
10.05g, vitamin C 0.05g, stir 5min, mix homogeneously.
C) by step b) gained mixed solution adds step a) in gained substrate, is uniformly mixed;
D) with 75% ethanol 4g, dissolve ethyl hydroxybenzoate 0.2g and be mixed with antiseptic solution, add c step, mix homogeneously.
E) take 3% disodium ethylene diamine tetra-acetic acid solution 0.02g, crocus pigment 0.05g, essence 0.5ml, add in d step mixed solution, heat while stirring it is dissolved, mix homogeneously.
Embodiment 3
The physical and chemical index of embodiment 1,2 is as follows
3.1 character
This product color and luster is full, transparent, light, and denseness is suitable, has moist feeling, abnormal smells from the patient fragrance, good stability.
3.2pH value checks
Get this product, with pH meter, measure, recording pH value is 5-7.
3.3 caloric test
Nial polish is packaged in transparent dressing product bottle, in the refrigerator cold-storages of 4 ℃, within one month, observes without lamination.24h in the calorstat of 55 ℃, nial polish is without layering, the phenomenon such as spoiled.
3.4 centrifugal test
Nial polish is packaged in to 3000r/min in tool plug test tube, and centrifugal 20min, without lamination.
3.5 room temperatures are placed experiment
Embodiment 1,2 made nial polishs are placed in to bottle for cosmetics, the standing investigation of room temperature 6 months, without lamination, use aftersensation is unchanged, abnormal smells from the patient is unchanged.
3.6 irritation tests, anaphylaxis experiment
Get embodiment 1,2 and be applied in right amount on volunteer (20-60 year, 40 people) fingernail, observe after spending 10 minutes, all do not occur allergic phenomena.
3.7 appearance of films: smooth smooth, there is special pearl effect.
3.8 VOCs (V0C): get 10ml product and carry out VOC detection, test result is almost nil.
3.9 drying times: coat nail surface <3min drying time nial polish bone dry time <10min after nial polish
Embodiment 4:
This nial polish resultant effect is investigated
By experiment on probation, carry out the effect of the nial polish that Evaluation operation example 1,2 produces.Adopt public-opinion poll point system, the women who chooses 80 20-60 year age bracket is object on probation, is divided into arbitrarily two groups, smears on fingernail respectively with the moist type water-based nail polish of environmental protection of embodiment 1,2 preparations.Every result of use total points is 5 minutes: five are divided into best result, represents fine, very satisfied; 4 are divided into better; 3 are divided into and can accept; 3 minutes is bad below, can not accept.It is below every average.The results are shown in Table 1:
Table 1 resultant effect is investigated
| Result of use | The every average of embodiment 1 | The every average of embodiment 2 |
| Abnormal smells from the patient | 4.8 | 4.9 |
| Ductility | 4.8 | 4.8 |
| Tack | 4.6 | 4.5 |
| Glossiness | 4.5 | 4.6 |
| Aesthetics | 4.8 | 4.9 |
Claims (7)
1. a type water-based nail polish is moistened in environmental protection, it is characterized in that, by the raw material of following content, is prepared from:
2. type water-based nail polish is moistened in environmental protection according to claim 1, it is characterized in that, described Radix Angelicae Dahuricae extracting solution is prepared by the following method:
Take the Radix Angelicae Dahuricae appropriate, soak 0.15-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and obtain Radix Angelicae Dahuricae extracting solution.
3. type water-based nail polish is moistened in environmental protection according to claim 1, it is characterized in that, described Rhizoma Bletillae extraction solution is prepared by the following method:
Take the Pseudobulbus Bletillae (Rhizoma Bletillae) appropriate, soak 0.15-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times of g/ml of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filters and obtain Rhizoma Bletillae extraction solution.
4. type water-based nail polish is moistened in environmental protection according to claim 1, it is characterized in that, described lavandula angustifolia extracting solution is prepared by the following method:
Take lavandula angustifolia appropriate, in 90-100 ℃ of extraction 2 times, add the 5-25 times of water yield the 1st time, extract 0.5-2h, the 2nd time by the 5-20 times of water yield, extracts 0.5-2h, at every turn with 3 layers of gauzes filtration, merging filtrate, heating is concentrated into 5-20 times of g/ml of lavandula angustifolia weight, obtains lavandula angustifolia extracting solution.
5. type water-based nail polish is moistened in environmental protection according to claim 1, it is characterized in that, described Bulbus Lilii extracting solution is prepared by the following method:
Take Bulbus Lilii appropriate, soak 0.5-1h, be heated to 90-100 ℃, decoct and extract 3 times, add 10-15 times of water gaging the 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 4-7 times of g/ml of Bulbus Lilii weight, adds liquid weight 1%-5% active carbon, and 80-100 ℃ of heating in water bath stirs, sucking filtration, gets filtrate, obtains Bulbus Lilii extracting solution.
6. type water-based nail polish is moistened in environmental protection according to claim 1, it is characterized in that, described pearlescent pigment or the color of pigment are bright cherry-red, crocus, rose-red, grass green, turquoise.
7. a preparation method for type water-based nail polish is moistened in environmental protection claimed in claim 1, and its feature exists, and described preparation method comprises the following steps:
A) weighing polyvinyl alcohol 10-15g, polyvidon 1-10g, be dissolved in 50-80ml water, stir, within standing 24 hours, treat its natural swelling, dissolving, be warming up to 80-90 ℃, insulation 10-30 minute, adds sodium carboxymethyl cellulose 0.1-1g, until swelling is complete, form the substrate of clear;
B) take glycerol 1-5g, Rhizoma Bletillae extraction solution 1-5g, lavandula angustifolia extracting solution 0.1-1g, Radix Angelicae Dahuricae extracting solution 0.1-1g, Bulbus Lilii extracting solution 0.1-1g, vitamin B
10.1-0.5g, vitamin C 0.1-0.5g, stir 1-5min, mix homogeneously;
C) by step b) gained mixed solution adds step a) in gained substrate, is uniformly mixed;
D) with 75% ethanol 1-5g, dissolve ethyl hydroxybenzoate 0.1-0.3g, be mixed with antiseptic solution, add step c) in gained solution, be uniformly mixed;
E) get 3% disodium ethylene diamine tetra-acetic acid solution 0.01-0.05g, pearlescent pigment or pigment 0.05-0.1g, essence 0.1-1.3ml, add steps d) in mixed solution, heat while stirring it is dissolved, mix homogeneously, obtains environmental protection and moistens type water-based nail polish.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410466168.1A CN104188872A (en) | 2014-09-12 | 2014-09-12 | Environmental protection moisture type water-based nail polish and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410466168.1A CN104188872A (en) | 2014-09-12 | 2014-09-12 | Environmental protection moisture type water-based nail polish and preparation method thereof |
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| CN104188872A true CN104188872A (en) | 2014-12-10 |
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ID=52074358
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104940080A (en) * | 2015-07-03 | 2015-09-30 | 福建农林大学 | Konjac glucomannan aqueous nail polish and preparation method thereof |
| CN106619188A (en) * | 2017-01-24 | 2017-05-10 | 山西大学 | Fluorescent nail polish and preparation method thereof |
| CN107661269A (en) * | 2017-11-20 | 2018-02-06 | 皖南医学院 | A kind of nontoxic nail saver for repairing nail and preparation method thereof |
| CN105726419B (en) * | 2016-04-19 | 2019-01-11 | 中国农业科学院农产品加工研究所 | A kind of edible nail polish |
-
2014
- 2014-09-12 CN CN201410466168.1A patent/CN104188872A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 中华人民共和国卫生部: "《表2（2）化妆品禁用组分》", 《化妆品卫生规范》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104940080A (en) * | 2015-07-03 | 2015-09-30 | 福建农林大学 | Konjac glucomannan aqueous nail polish and preparation method thereof |
| CN105726419B (en) * | 2016-04-19 | 2019-01-11 | 中国农业科学院农产品加工研究所 | A kind of edible nail polish |
| CN106619188A (en) * | 2017-01-24 | 2017-05-10 | 山西大学 | Fluorescent nail polish and preparation method thereof |
| CN107661269A (en) * | 2017-11-20 | 2018-02-06 | 皖南医学院 | A kind of nontoxic nail saver for repairing nail and preparation method thereof |
| CN107661269B (en) * | 2017-11-20 | 2020-04-17 | 皖南医学院 | Non-toxic nail-protecting oil capable of repairing nails and preparation method thereof |
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Application publication date: 20141210 |
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