CN105112181A - Functional plant essential oil handmade soap and preparation method thereof - Google Patents
Functional plant essential oil handmade soap and preparation method thereof Download PDFInfo
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- CN105112181A CN105112181A CN201510587919.XA CN201510587919A CN105112181A CN 105112181 A CN105112181 A CN 105112181A CN 201510587919 A CN201510587919 A CN 201510587919A CN 105112181 A CN105112181 A CN 105112181A
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Abstract
The invention discloses functional plant essential oil handmade soap, and belongs to the technical field of daily chemical cleaning products. The functional plant essential oil handmade soap is mainly composed of plant polysaccharide, plant superfine powder and sodium aliphatate. The preparation method of the functional plant essential oil handmade soap comprises the steps that essential oil is emulsified through the plant polysaccharide, the plant superfine powder and essential oil emulsified liquid are mixed to prepare essential oil dispersion liquid, and the essential oil dispersion liquid is injected into the sodium aliphatate. The plant polysaccharide has the excellent moisturizing effect; on the one hand, the plant polysaccharide can emulsify the essential oil, enhance the slow release performance of the essential oil, prolong the fragrance holding time and enable the handmade soap to give out fragrance of the essential oil; on the other hand, the plant polysaccharide enables fat soluble and water soluble natural moisturizing, whitening and acne removing active ingredients in the superfine powder to be well dissolved out. The functional plant essential oil handmade soap with different functional ingredients is suitable for different crowds with different requirements.
Description
Technical field
The present invention relates to a kind of functional plants essential oil handmade soap and preparation thereof, belong to daily washing and protect product technical field.
Background technology
The traditional perfumed soap sold in the market all adopts chemical substance to synthesize and makes, and detached by reacted for fat saponification glycerine due to it on the one hand, lose natural glycerin, use procedure can cause skin dry and astringent, coarse; On the other hand because traditional perfumed soap alkalinity is higher, the natural grease on human body skin can be washed away, easily cause multiple skin problem, and also can pollute environment.
Along with the raising of people's living standard, people more and more pay attention to the security of daily necessities, health, and handmade soap enjoys the favor of human consumer.Handmade soap has cold and hot two kinds of soap preparing process: the product after cold soap and grease and caustic soda saponification reaction is rich in the by product-glycerine of saponification reaction, and gentle, foam is fine and smooth abundant, can keep the moistening of skin while deep layer cleaning skin dirt; Namely hot soapmaking add the natural vigour that natural moisturizing factor can keep skin equally while clean skin in natural soap base.
Essential oil is from the flower of plant, leaf, stem, root or fruit, is refined the volatile flavor essential oil of extraction by steam distillation, extrusion process, cold-maceration or solvent-extraction process.Plants essential oil is generally containing the aromatoising substance containing more alkene, ketone, ester class, and under the arrangement of the Nature, these molecules also exist jointly with perfect ratio, make every kind of plant have its singularity.Different aromatic essential oils antisepsis and anti-inflammation, antipyretic-antalgic, tranquilizing and allaying excitement, expelling phlegm for arresting cough, antitumor etc. in there is certain effect, there is stronger practical value.
Essential oil is the Secondary metabolites that molecule amount is less, and volatility is very strong, once ingress of air will volatilize very soon.Conventional method is added essential oil or is treated the slightly cold interpolation essential oil of soap base, because the effect of hydrophile-lipophile balance value (HLB value) the larger emulsification slowly-releasing essential oil of sodium stearate is bad after saponification reaction.Plant ultra-micropowder is by the micro mist of vegetable material after comminution by gas stream, its cell wall rupture, lose complete cellularstructure, specific surface area and porosity strengthens greatly, but do not use organic reagent, general dissolving-out method cannot by contain in plant ultra-micropowder fat-soluble and water-soluble natural moisturizing, whitening, the good stripping of anti-acne active component.In order to solve above-mentioned handmade soap essential oil slowly-releasing and super-fine powder stripping problem, the present invention selects natural plant polyose solution, vegetable polysaccharides has excellent moisture-keeping efficacy, it is energy emulsified refined oil on the one hand, strengthen the sustained release performance of essential oil, extend fragrance remaining time, make handmade soap give out the fragrance of essential oil for a long time, on the other hand vegetable polysaccharides solution can make to contain in super-fine powder fat-soluble and water-soluble natural moisturizing, whitening, the good stripping of anti-acne active component.Functional plants essential oil handmade soap containing difference in functionality composition is suitable for different demand crowd and uses, and has good market outlook.
Summary of the invention
A kind of functional plants essential oil handmade soap and preparation process thereof comprise:
1, vegetable polysaccharides emulsified refined oil
One or more in tremella polysaccharide, bletilla striata mucopolysaccharide, Aloe polysaccharide, Pachymose are made into the aqueous solution of 0.1%-5%, polysaccharide soln is mixed with essential oil with the mass ratio 10:1 ~ 200:1 of essential oil by polysaccharide soln, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 20 ~ 50Mpa, homogenizing time is 5 ~ 30min, and homogenizing temperature is 20 ~ 40 DEG C.
2, essential oil emulsion and plant ultra-micropowder are mixed with essential oil dispersion liquid
By ginseng, the root of Dahurain angelica, white tuckahoe, sunglo, the root of large-flowered skullcap, glossy ganoderma, Herba Dendrobii, aloe comminution by gas stream, controlling its pressure is 0.5 ~ 0.8Mpa, and grading wheel rotating speed is 2000 ~ 4000rpm/min, makes the super-fine powder that particle diameter is 5-50 μm.One or more above-mentioned super-fine powder are selected to be 2:1 ~ 10:1 by super-fine powder and essential oil mass ratio.Super-fine powder is mixed with essential oil emulsion, and with homogeneous method make essential oil emulsion and super-fine powder dispersed, control homogenization pressure is 20-40Mpa, and homogenizing time is 5 ~ 20min, and homogenizing temperature is 20 ~ 40 DEG C.
3, essential oil dispersion liquid injects sodium soap
Controlling the temperature of sodium soap is 40 ~ 60 DEG C, by sodium soap and essential oil dispersion liquid in mass ratio 100:5 ~ 500:5 mix, and slowly to stir.
4, injection molding cooling.
Cooled by above-mentioned mixed solution injection molding after intimate mixing, the temperature controlling soap base during injection molding is 40-60 DEG C, and cooling temperature be-20-20 DEG C, cools 0.5 ~ 2h.
5, the demoulding.
Embodiment
example 1
Ginseng, Herba Dendrobii, aloe are used comminution by gas stream micronizer mill after pressing 4:1:2 mixing, and controlling its pressure is 0.6Mpa, and grading wheel rotating speed is 2000rpm/min, makes the super-fine powder that particle diameter is 5-50 μm.Tremella polysaccharide, Aloe polysaccharide are made into the aqueous solution of 2% by 1:1 mixing, mixed with essential oil by polysaccharide soln with the quality 100:1 of essential oil by polysaccharide soln, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 25Mpa, homogenizing time is 10min, and homogenizing temperature is 30 DEG C.Mixed with essential oil emulsion by super-fine powder with essential oil mass ratio 2.5:1 by super-fine powder, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 35Mpa, and homogenizing time is 30min, and homogenizing temperature is 20 DEG C.Mixed by 250:5 with essential oil dispersion liquid by sodium soap, the temperature controlling sodium soap is 50 DEG C, slowly stirs.Injection molding also cools, and the temperature controlling sodium soap during injection molding is 45 DEG C, and cooling temperature is-20 DEG C, cooling 1h.Finally demould obtains the plants essential oil handmade soap with essential oil slowly-releasing and moisture-keeping functions.
example 2
Ginseng, glossy ganoderma, the root of Dahurain angelica, white tuckahoe are used comminution by gas stream micronizer mill after pressing 2:2:1:1 mixing, and controlling its pressure is 0.7Mpa, and grading wheel rotating speed is 3000rpm/min, makes the super-fine powder that particle diameter is 5-50 μm.Bletilla striata mucopolysaccharide, Aloe polysaccharide are made into the aqueous solution of 2.5% by 3:1 mixing, mixed with essential oil by polysaccharide soln with the quality 150:1 of essential oil by polysaccharide soln, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 30Mpa, homogenizing time is 15min, and homogenizing temperature is 30 DEG C.Mixed with essential oil emulsion by super-fine powder with essential oil mass ratio 4:1 by super-fine powder, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 25Mpa, and homogenizing time is 20min, and homogenizing temperature is 25 DEG C.Mixed by 300:5 with essential oil dispersion liquid by sodium soap, the temperature controlling sodium soap is 45 DEG C, slowly stirs.Injection molding also cools, and the temperature controlling sodium soap during injection molding is 40 DEG C, and cooling temperature is-10 DEG C, cooling 1h.Finally demould obtains the plants essential oil handmade soap with essential oil slowly-releasing and whitening function.
example 3
Ginseng, sunglo, the root of large-flowered skullcap are pressed 2:1:1: use comminution by gas stream micronizer mill after mixing, controlling its pressure is 0.8Mpa, and grading wheel rotating speed is 4000rpm/min, makes the super-fine powder that particle diameter is 5-50 μm.Tremella polysaccharide, bletilla striata mucopolysaccharide, aloe are made into the aqueous solution of 1.5% by 2:1:1, mixed with essential oil by polysaccharide soln with the quality 10:1 of essential oil by polysaccharide soln, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 35Mpa, homogenizing time is 20min, and homogenizing temperature is 30 DEG C.Mixed with essential oil emulsion by super-fine powder with essential oil mass ratio 5:1 by super-fine powder, and adopt homogeneous method to make its Homogeneous phase mixing, control homogenization pressure is 25Mpa, and homogenizing time is 20min, and homogenizing temperature is 25 DEG C.Mixed by 200:5 with essential oil dispersion liquid by sodium soap, the temperature controlling sodium soap is 40 DEG C, slowly stirs.Injection molding also cools, and the temperature controlling sodium soap during injection molding is 40 DEG C, and cooling temperature is-10 DEG C, cooling 2h.Finally demould obtains the plants essential oil handmade soap with essential oil slowly-releasing and acne-removal function.
Claims (9)
1. a plants essential oil handmade soap and preparation thereof is characterized in that: by weight, plant ultra-micropowder 1 ~ 5 part, plants essential oil 0.2 ~ 1 part, vegetable polysaccharides 0.1 ~ 1 part, deionized water 5 ~ 15 parts, sodium soap 100 ~ 200 parts.
2. plant ultra-micropowder is characterized in that according to claim 1: plant ultra-micropowder can be one or more in ginseng submicron powder, root of Dahurain angelica super-fine powder, white tuckahoe super-fine powder, sunglo super-fine powder, root of large-flowered skullcap super-fine powder, glossy ganoderma super-fine powder, dendrobium candidum ultrafine powder, aloe super-fine powder; The broken equipment of plant ultra-micropowder is micronizer mill, and controlling its pressure is 0.5 ~ 0.8Mpa, and grading wheel rotating speed is 2000 ~ 4000rpm/min, and each super-fine powder particle diameter is 5-50 μm.
3. plants essential oil is characterized in that according to claim 1: plants essential oil can be composite for one or more in Herba Lysimachiae foenumgraeci quintessence oil, Flos Rosae Rugosae quintessence oil, chamomile essential oil, lemon quintessence oil, sweet orange oil, litsea cubeba oil.
4. it is characterized in that according to vegetable polysaccharides described in claim 1: vegetable polysaccharides used is one or more in tremella polysaccharide, bletilla striata mucopolysaccharide, Aloe polysaccharide, Pachymose.
5. plants essential oil handmade soap and preparation thereof is characterized in that: its preparation process comprises an a vegetable polysaccharides emulsified refined oil, and b plant ultra-micropowder and essential oil emulsion are mixed with essential oil dispersion liquid, and c essential oil dispersion liquid injects sodium soap, and d reverse mould cools, the e demoulding.
6. it is characterized in that according to the emulsified refined oil of vegetable polysaccharides described in claim 5: with water, polysaccharide is mixed with the aqueous solution of 0.1% ~ 5%, be uniformly mixed by polysaccharide soln and essential oil weight ratio 10:1 ~ 200:1, emulsification method therefor is homogeneous method, and to control homogenization pressure be 20-50Mpa, homogenizing time is 5 ~ 30min, and homogenizing temperature is 20 ~ 40 DEG C.
7. be mixed with essential oil dispersion liquid according to plant ultra-micropowder described in claim 5 and essential oil emulsion it is characterized in that: in essential oil emulsion, add super-fine powder by super-fine powder and essential oil weight ratio 5:1 ~ 100:1 and mix, mixing method therefor is homogeneous method, control homogenization pressure is 20-40Mpa, homogenizing time is 5 ~ 20min, and homogenizing temperature is 20 ~ 40 DEG C.
8. inject sodium soap according to the liquid of essential oil dispersion described in claim 5 it is characterized in that: the weight ratio controlling sodium soap and essential oil dispersion liquid when essential oil dispersion liquid injects sodium soap is 100:5 ~ 500:5, the temperature of sodium soap is 40 ~ 60 DEG C, and slowly stirs.
9. it is characterized in that according to the cooling of injection molding described in claim 5: the temperature controlling soap base during injection molding is 40-60 DEG C, and cooling temperature is-20-20 DEG C, cooling 0.5 ~ 2h.
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105602761A (en) * | 2015-11-23 | 2016-05-25 | 青岛芬芳小镇日化有限公司 | Skin-moistening handmade soap containing plant mucopolysaccharide and hot preparation method thereof |
| CN105999062A (en) * | 2016-05-31 | 2016-10-12 | 安徽皖斛堂生物科技有限公司 | Moisture-preserving acne-curing dendrobium officinale extract medicated soap and preparation method thereof |
| CN106085660A (en) * | 2016-05-31 | 2016-11-09 | 安徽皖斛堂生物科技有限公司 | A kind of Herba Dendrobii extract medicated soap of moisture-keeping crease-shedding and preparation method thereof |
| CN106085656A (en) * | 2016-06-21 | 2016-11-09 | 陆锦满 | A kind of Herba Dendrobii cosmetic perfumed soap |
| CN106281800A (en) * | 2016-08-09 | 2017-01-04 | 宁波圣旺生物科技有限公司 | Herba Dendrobii soap and preparation method thereof |
| CN106398878A (en) * | 2016-08-19 | 2017-02-15 | 跨越生物科技（滁州）有限公司 | Congealed fat essential oil handmade soap with effects of skin soothing and convergence |
| CN106434069A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Moisturizing congealed-fat handmade soap containing essential oil |
| CN106434068A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Ice-cool mint skin-purifying essential oil handmade soap |
| CN106434037A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Repair nourishing creamy essential oil handmade soap |
| CN106833977A (en) * | 2016-12-15 | 2017-06-13 | 湖南利诺生物药业有限公司 | Citral dendrobium candidum perfumed soap and preparation method thereof |
| CN108659998A (en) * | 2018-04-28 | 2018-10-16 | 天津农学院 | A kind of skin makeup handmade soap and preparation method thereof containing compound polysaccharide |
| CN108753497A (en) * | 2018-06-15 | 2018-11-06 | 中华全国供销合作总社南京野生植物综合利用研究所 | A kind of functional plants essential oil handmade soap and its preparation |
| CN110029026A (en) * | 2019-05-28 | 2019-07-19 | 张慧君 | A kind of sterilizing and itch-relieving medicated soap and preparation method thereof |
| CN112342099A (en) * | 2019-08-09 | 2021-02-09 | 南风化工集团股份有限公司 | Production method of plant bacteriostatic mosquito-repellent essential oil soap |
-
2015
- 2015-09-16 CN CN201510587919.XA patent/CN105112181A/en active Pending
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105602761A (en) * | 2015-11-23 | 2016-05-25 | 青岛芬芳小镇日化有限公司 | Skin-moistening handmade soap containing plant mucopolysaccharide and hot preparation method thereof |
| CN105999062A (en) * | 2016-05-31 | 2016-10-12 | 安徽皖斛堂生物科技有限公司 | Moisture-preserving acne-curing dendrobium officinale extract medicated soap and preparation method thereof |
| CN106085660A (en) * | 2016-05-31 | 2016-11-09 | 安徽皖斛堂生物科技有限公司 | A kind of Herba Dendrobii extract medicated soap of moisture-keeping crease-shedding and preparation method thereof |
| CN106085656A (en) * | 2016-06-21 | 2016-11-09 | 陆锦满 | A kind of Herba Dendrobii cosmetic perfumed soap |
| CN106281800A (en) * | 2016-08-09 | 2017-01-04 | 宁波圣旺生物科技有限公司 | Herba Dendrobii soap and preparation method thereof |
| CN106398878A (en) * | 2016-08-19 | 2017-02-15 | 跨越生物科技（滁州）有限公司 | Congealed fat essential oil handmade soap with effects of skin soothing and convergence |
| CN106434069A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Moisturizing congealed-fat handmade soap containing essential oil |
| CN106434068A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Ice-cool mint skin-purifying essential oil handmade soap |
| CN106434037A (en) * | 2016-08-19 | 2017-02-22 | 跨越生物科技（滁州）有限公司 | Repair nourishing creamy essential oil handmade soap |
| CN106833977A (en) * | 2016-12-15 | 2017-06-13 | 湖南利诺生物药业有限公司 | Citral dendrobium candidum perfumed soap and preparation method thereof |
| CN108659998A (en) * | 2018-04-28 | 2018-10-16 | 天津农学院 | A kind of skin makeup handmade soap and preparation method thereof containing compound polysaccharide |
| CN108753497A (en) * | 2018-06-15 | 2018-11-06 | 中华全国供销合作总社南京野生植物综合利用研究所 | A kind of functional plants essential oil handmade soap and its preparation |
| CN110029026A (en) * | 2019-05-28 | 2019-07-19 | 张慧君 | A kind of sterilizing and itch-relieving medicated soap and preparation method thereof |
| CN112342099A (en) * | 2019-08-09 | 2021-02-09 | 南风化工集团股份有限公司 | Production method of plant bacteriostatic mosquito-repellent essential oil soap |
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