CN103432043B - Face mask containing plant material residues - Google Patents
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- CN103432043B CN103432043B CN201310389135.7A CN201310389135A CN103432043B CN 103432043 B CN103432043 B CN 103432043B CN 201310389135 A CN201310389135 A CN 201310389135A CN 103432043 B CN103432043 B CN 103432043B
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Abstract
The invention provides a face mask containing plant material residues. A formula of the face mask comprises the following components in percentage by weight: 1%-2% of span 60, 1%-2% of PEG-60 (polyethylene glycol-60) sorbitan stearate, 2%-3% of stearic acid, 1%-2.5% of monoglyceride, 1%-3% of 16/18 alcohol, 3%-6% of 26# white mineral oil, 2%-6% of isopropyl myristate, 2%-6% of isooctyl palmitate, 1%-3% of polydimethylsiloxane, 3%-5% of glycerinum, 0.05-0.15% of xanthan gum, 0.1-10% of the plant material residues, 0.1%-0.2% of polyacrylate-13 (and) polyisobutene (and) polysorbate-20, 0.2%-0.4% of preservative and the balance of water. According to the face mask provided by the invention, the material residues after plant materials are extracted and utilized are turned into wealth, the production cost is reduced, and the utilization rate of the plant materials is increased.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of washing-off type facial film utilizing the waste residue of plant material after extracting to prepare.
Background technology
In recent years; the trend (" green century ") of one back to nature has been started in the whole world; " the natural cosmetics heat " that parallels with wholefood trend is progressively formed, and consumer more focuses on environmental conservation and ecological balance, the requirement of cosmetics is more prone to its actual effect.Many cosmetics manufacturers greatly develop the cosmetics that animals and plants composition is batching, and some cosmetic material production firms also utilize various Method and Technology, and preparation and each Plant Extracts of purification, isolate effective ingredient wherein.As Chinese patent 201110441416.3 discloses a kind of for suppressing the plant extraction liquid of acne cosmetics, various plants raw material is prepared compound plant extract by alcohol extracting method by it.Current cosmetic field, when preparing plant extraction liquid, adopts following several extraction process: alcohol extraction, water extraction, immersion method and supercritical CO usually
2extraction, some also comprises some supplementary meanss, as cellulose treatment, ultrasonic Treatment, resin absorption purification etc.As everyone knows, the plant extraction liquid that alcohol extracting method and water extraction are produced is water miscible, the water solublity that what it mainly extracted is in plant material and alcohol soluble component; And the plant extraction liquid that immersion method and supercritical carbon dioxide fluid extraction are produced is oil-soluble, the oil-soluble ingredients that what it mainly extracted is in plant.There is the single problem of extraction component in alcohol extracting method, water extraction, immersion method and supercritical carbon dioxide fluid extraction as can be seen here.In addition, also there is the not high problem of extraction ratio in these four kinds of processing technique.As " pharmaceutical raw material and intermediate information " is just recorded in the 8th phase 25-26 page for 2007: the flavone compound yield adopting " ultrasound wave-ol puies forward-ol extraction " method to obtain in " extracting pyrite compounds in Herba Lophatheri " this section of document is 2.27%; The extraction ratio adopting CO_2 supercritical technology to produce first product diosgenin in " extracting diosgenin from Rhizoma Dioscoreae Nipponicae " this section of document is 4.44%.Visible, the plant material after extraction and application, must also containing abundant effective ingredient in its residue.There is a plant material and utilize insufficient problem in existing plant extract technique, and usually ignores the potential value of the plant residue after being extracted in prior art.
As everyone knows, plant has carried out a series of metabolism biochemical process in growth course, formed and have accumulated various chemical substance, these chemical substances constitute the chemical composition of plant, usually there is containing some in plant the composition of certain skin-care effect, as: alkaloid, glycoside, organic acid, resin (comprises resinic acid, resinol and resin hydro carbons), volatile oil, saccharide (comprises cellulose, starch, inulin, natural gum and phlegmatic temperament etc.), aminoacid, protein and enzyme, tannin, plant pigment (comprises chlorophyll, carotene, flavonoid, beet red bases and quinones etc.), oils and fats and wax and inorganic constituents (trace element) etc.These compositions plant material carry out extraction prepare plant extraction liquid time, can not be utilized fully.The plant residue of plant material after modern extraction process is extracted still has very high recycle value, containing a large amount of nutritional labelings, as contained most oil-soluble ingredients and water soluble ingredient greatly through the plant residue of alcohol extraction water extraction; The plant residue produced through immersion method and SCF-CO 2 contains most water soluble ingredient and oil-soluble ingredients greatly, and being abandoned by these plant residues and doing garbage disposal is the huge wasting of resources really.
Summary of the invention
The object of the invention is to make up the deficiencies in the prior art, provide a kind of facial film, the powder that residue after it contains plant material extraction is made, obtained its steady quality of facial film, and there is certain skin-care effect, make plant material better be fully utilized simultaneously, plant material is extracted and utilizes rear remaining raw material residue to turn waste into wealth, and reduce production cost, improve the utilization rate of plant material.
It is as follows that the present invention reaches the technical scheme that its object adopts: a kind of facial film containing plant material residue, and its formula of described facial film comprises each component of following mass percentage:
Described plant material residue is the mixing of a kind of dusty raw materials residue of plant material or the dusty raw materials residue of multiple different plant material;
Described dusty raw materials residue is prepared as follows: the residue that plant material is left after extraction and application carries out drying, is ground into 10 ~ 20 orders afterwards.The compatibility of each component of face pack prescription of the present invention is good, and formula system is stablized.Residue after plant material extracts is processed into the dusty raw materials residue of certain particle diameter, and add in specific proportions in face pack prescription, well can coexist with other components, formulation stable, facial film is not easy to occur quality problems.The raw material residue powder of plant material after extraction and application is usually containing a large amount of ions; and in cosmetics series, add this raw material residue containing a large amount of ion, usually can bring considerable influence to the stability of cosmetics series especially emulsifying agent and thickening agent.Face pack prescription system of the present invention, using Arlacel-60, PEG-60 Span60 as emulsifying agent, polyacrylate-13 (with) polyisobutylene (with) polysorbate-20 and HANSHENGJIAO be as thickening agent, the face pack prescription system complemented each other to form in specific proportions with other components in formula, residue after plant material extracts is processed into the dusty raw materials residue of certain particle diameter, add in specific proportions in face pack prescription, well can coexist with other components.The facial film that the present invention makes meets " cosmetics health specification " requirement completely, by heat-resisting cold-resistant stability test, can guarantee within 3 year effect duration, kept stable.
Water used in formula is deionized water, the antiseptic that antiseptic can adopt the art conventional.
Preferably, the mass percentage of plant material residue that its formula of facial film comprises is 1 ~ 5%.
In the present invention, the residue of described plant material left by after extraction and application refers to the residue that plant material is left after one or more extraction processes in alcohol extraction, water extraction, immersion method, supercritical carbon dioxide extraction method are extracted, and said extracted technique is all the technique being prepared plant extraction liquid by plant material that cosmetic field is commonly used.The art, alcohol extraction refers to a kind of method using polyhydric alcohol (as glycerol, sorbitol, propylene glycol, ethanol) and extraction with aqueous solution effective ingredients in plant thereof, and conventional 30%-90% ethanol water extracts.Water extraction refers to a kind of method of direct water extraction effective ingredients in plant, conventional decocting method.Immersion method refers to that one oils and fats (as mineral oil, vegetable oil) extracts the method for effective ingredients in plant, conventional white mineral oil, Oleum Cocois, olive oil soak extraction.Supercritical carbon dioxide extraction method refers to the dissolution utilizing supercritical carbon dioxide to part effective ingredient in natural product, extract effective ingredient selectively, then the method by decompression, intensification makes supercritical fluid become common gases, be extracted material then to separate out completely or substantially, thus reach the object of separating-purifying.Current the used extraction process preparing plant extraction liquid by plant material of cosmetic industry is adopt ethanol extraction method to extract mostly.When the present invention carries out extraction and application (alcohol extraction, water extraction, immersion method, supercritical carbon dioxide extraction method) for plant material, there is no particular restriction for its Extraction technique, the residue that plant material stays after extracting (alcohol extraction, water extraction, immersion method, supercritical carbon dioxide extraction method), these residues can use to prepare facial film of the present invention by the present invention.
Described plant material refer to cosmetic field can plant material, described plant material is preferably from Aesculus hippocastanum L., Aloe, Althaea officinalis L., Radix Angelicae Sinensis, Anthemis nobilis, large Fructus Arctii, arnica montana, silver birch, Flos Inulae, Fructus Capsici, Radix Carpesii, Centaurea cyanus, Herba Centellae, Lobaria islandica, golden pheasant sodium, Flos Chrysanthemi, cola, Crataegus Oxyacantha, Gherkin, Semen Cuscutae, corn radish, Fructus Forsythiae, Radix Gentianae, Radix Glycyrrhizae, Radix Hamamelidis Mollis, ocean Caulis Hederae Sinensis, Helichrysum, SONGGUOJU, hop, Herba Hyperici perforati, Semen Juglandis, Flos Impatientis, Herba Leonuri, Rhizoma Chuanxiong, Radix Arnebiae (Radix Lithospermi), Radix Malvae sylvestris, Flos Matricariae chamomillae, Herba Menthae, the bark of Fructus Myricae rubrae, Fructus oleae europaeae, Radix Ginseng, Cortex Phellodendri, Big Semen Plantaginis, Radix Et Rhizoma Rhei, Flos Rosae Multiflorae, Herba Rosmarini Officinalis, Salvia japonica Thunb., Flos Matricariae chamomillae, Flos Rosae Rugosae, Herba Lophatheri, Fructus Phyllanthi fruit, Radix Scutellariae, Galla Chinensis, Ganoderma, Radix Puerariae, Radix Polygoni Multiflori, Radix Sophorae Flavescentis, Flos Lonicerae, Flos Carthami, Rhizoma Zingiberis Recens, Herba Portulacae, Folium Artemisiae Argyi, Semen Ginkgo, Ramulus et Folium Spiraeae Salicifolia, Fructus Lycopersici esculenti, Radix Dauci Sativae, pollen, Herba bromi japonici, Folium olive, Herba Equiseti Arvinsis, Testa oryzae, Herba Passiflorae Caeruleae.In the present invention, for plant material cited above, wherein Section Plant Material specifically utilizes position for raw material with it, is specially: the seed of Aesculus hippocastanum L. and bark, the leaf juice of Aloe, the root of Althaea officinalis L., the root of Radix Angelicae Sinensis, the flower of Anthemis nobilis, the root of large Fructus Arctii and leaf, the Hua Heye of arnica montana, the bark of silver birch, the flower of Flos Inulae, the fruit of Fructus Capsici, the fruit of Radix Carpesii, the flower of Centaurea cyanus, the bark of golden pheasant sodium, the flower of Flos Chrysanthemi, the seed of cola, the seed of Crataegus Oxyacantha, the fruit of Gherkin, the seed of Semen Cuscutae, the root of corn radish, the fruit of Fructus Forsythiae, the root of Radix Gentianae, the root of Radix Glycyrrhizae, the leaf of Radix Hamamelidis Mollis and Pi Hegen, the leaf of ocean Caulis Hederae Sinensis, the Flowers of Helichrysum bracteatum, the flower of SONGGUOJU, the flower of Herba Hyperici perforati, the sarcocarp of Semen Juglandis and peel, the leaf of Flos Impatientis, the root of Rhizoma Chuanxiong, the Ye Hehua of Radix Malvae sylvestris, the flower of Flos Matricariae chamomillae, mentha leave, leaf of Fructus oleae europaeae, the root of Radix Ginseng, the bark of Cortex Phellodendri, the leaf of Big Semen Plantaginis, the root of Radix Et Rhizoma Rhei or stem, the flower of Flos Rosae Multiflorae, Herba Rosmarini Officinalis leaf, the leaf of Salvia japonica Thunb., the flower of Flos Matricariae chamomillae, the root of Radix Scutellariae, gallic insect gall, the tuber of Ganoderma, the root of Radix Puerariae, the tuber of Radix Polygoni Multiflori, the root of Radix Sophorae Flavescentis, the flower of Flos Lonicerae, the flower of Flos Carthami, the tuber of Rhizoma Zingiberis Recens, the leaf of Folium Artemisiae Argyi, Semen Ginkgo fruit, the flower of Ramulus et Folium Spiraeae Salicifolia, the fruit of Fructus Lycopersici esculenti, the tuber of Radix Dauci Sativae, the seed of Herba bromi japonici, the seed of Herba Passiflorae Caeruleae.If Section Plant Material is not specified, then utilize the specific requirement in position to it, this kind of plant material is as Herba Centellae, Lobaria islandica, hop, Herba Leonuri, Radix Arnebiae (Radix Lithospermi), Herba Lophatheri, Herba Portulacae, Herba Equiseti Arvinsis etc.
Preferably, described plant material is selected from Radix Angelicae Sinensis, arnica montana, Radix Puerariae, Radix Glycyrrhizae, plant material residue is Radix Angelicae Sinensis, arnica montana, Radix Puerariae, Radix Glycyrrhizae dusty raw materials residue mix according to mass ratio 1:1:2:3.Adopt this preferred plant material residue, the facial film of preparation has good white-skinned face function.
Preferably, described plant material is selected from Aesculus hippocastanum L., large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia, Radix Scutellariae, and plant material residue is Aesculus hippocastanum L., the dusty raw materials residue of large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia, Radix Scutellariae mixes according to mass ratio 1:1:1:3.Adopt this preferred plant material residue, the facial film of preparation has good antiinflammatory anti-acne effect.
Preferably, described plant material is selected from Centaurea cyanus, Herba Centellae, Radix Ginseng, Flos Inulae, plant material residue be Centaurea cyanus, Herba Centellae, Radix Ginseng, Flos Inulae dusty raw materials residue according to the mixing of mass ratio 1:1:3:1, adopt this preferred plant material residue, the facial film of preparation has good wrinkle removing effect.
Preferably, described plant material is selected from Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae, Herba Passiflorae Caeruleae, plant residue be Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae, Herba Passiflorae Caeruleae dusty raw materials residue according to the mixing of mass ratio 1:1:1:1, adopt this preferred plant material residue, its facial film prepared has good replenishing water and preserving moisture effect.
Technical scheme of the present invention has following beneficial effect:
Beneficial effect of the present invention is the utilization rate substantially increasing plant material, and the residue nutrient substance after plant material is extracted is fully used, thus reaches the maximum using of resource, also reduces cost of material simultaneously.By adding plant material residue in facial film of the present invention, also can to a certain degree reach the similar effect of the corresponding plant material extracting solution of interpolation.
The compatibility of each component of face pack prescription of the present invention is good, and formula system is stablized.Residue after plant material extracts is processed into the powdered plant material residue of certain particle diameter, add in specific proportions in face pack prescription, be able to well coexist with other components, formulation stable, facial film is not easy to occur quality problems, and the present invention is the formula system that the utilization of plant material residue provides a kind of reasonably stability.
Detailed description of the invention
The invention provides a kind of face pack prescription system, the powder stock residue that residue after it contains plant material extraction is made, obtained its steady quality of facial film, and there is certain skin-care effect, make plant material better be fully utilized simultaneously, plant material is extracted and utilizes rear remaining raw material residue to turn waste into wealth, and reduce production cost, improve the utilization rate of plant material.
For preferred embodiment, technical scheme of the present invention is introduced below.
Embodiment 1 ~ 3(mono-kind has the facial film containing plant material residue of white-skinned face function)
The facial film of embodiment 1 ~ 3 adopts formula as shown in table 1 below, the plant material residue added in embodiment 1 ~ 3 formula be Radix Angelicae Sinensis, arnica montana, Radix Puerariae, Radix Glycyrrhizae dusty raw materials residue mix according to mass ratio 1:1:2:3.Wherein, Radix Angelicae Sinensis refers to the root of Radix Angelicae Sinensis, and arnica montana refers to the Hua Heye of arnica montana, and Radix Puerariae refers to its root.
Wherein,
the dusty raw materials residue of Radix Angelicae Sinensis, arnica montana, Radix Puerariae, Radix Glycyrrhizae is prepared in accordance with the following steps:
1) plant material Radix Angelicae Sinensis, arnica montana, Radix Puerariae or the residue of Radix Glycyrrhizae after extraction and application is collected, the present embodiment is remaining residue after ethanol extraction, concrete Extraction technique can be: extraction temperature 60 DEG C, extraction time 6 hours, the volume fraction of solvent for use ethanol is 80%, and solid-liquid ratio (mass ratio of plant material and ethanol) is 1:8.
2) Radix Angelicae Sinensis, arnica montana, Radix Puerariae or Glycyrrhiza uralensisFisch residue left after extraction and application in step 1 are carried out drying, pulverize the dusty raw materials residue of formation 10 ~ 20 object Radix Angelicae Sinensis, arnica montana, Radix Puerariae or Radix Glycyrrhizae afterwards.
its preparation technology of the facial film of embodiment 1 ~ 3 adopts existing technique, and following technique can be adopted to prepare:
1, Arlacel-60, PEG-60 Span60, stearic acid, monoglyceride, 16/18 alcohol, No. 26 white mineral oils, isopropyl myristate, iso-octyl palmitate, polydimethylsiloxane are dropped into oil phase pot, be heated to 50-60 DEG C, as oil phase heat preservation for standby use after dissolving;
2, Jiang Shui, glycerol, HANSHENGJIAO drop into emulsifying pot, are heated to 85-90 DEG C, and insulation 20-30 minute, is cooled to 55-60 DEG C, as aqueous phase.
3, by oil phase suction emulsifying pot, homogenizing (3000rpm) 2-3 minute, insulated and stirred (30rpm) 20-25 minute.
4, be uniformly dispersed by plant material residue deionized water, for subsequent use, wherein the mass ratio of plant material residue and deionized water is 1:1.
5, pot temperature to be emulsified is cooled to 42-45 DEG C, successively by the step 4 uniform plant material residue of aqueous dispersion, polyacrylate-13 (with) polyisobutylene (with) polysorbate-20, antiseptic add in pot, homogenizing 2-3 minute, stirs, and gets final product discharging.
Table 1 embodiment 1 ~ 3 formula table (each component is mass percentage)
embodiment 1 ~ 3 effect:
Facial film prepared by embodiment 1 ~ 3 through 100 personnel 4 weeks on probation continuously, while commercially available declare to there is the washing facial film of good white-skinned face function for comparative example 1 with a.Tested object: each experimental group is 100 women (20-30 year).Test zone and method: get 2-3g facial film uniform application in face, both hands finger to be looped massage gently in face, cleans up after 5 minutes with water.Use: twice daily, continue use 4 weeks; Test event: whitening.Result on trial sees the following form 2.
Table 2
Facial film prepared by embodiment 1 ~ 3 is tried out 4 weeks continuously through 100 personnel, and the trier of more than 90% all represents that whitening effect is obvious, does not all find the phenomenon such as chafe, allergy after on probation.
Embodiment 4 ~ 6(mono-kind has the facial film containing plant material residue of antiinflammatory anti-acne effect)
The face pack prescription of embodiment 4,5,6 is substantially identical with the formula of the embodiment 1,2,3 shown in table 1 successively respectively, its difference is that plant material residue is different, and the plant material residue added in embodiment 4 ~ 6 formula is Aesculus hippocastanum L., greatly the dusty raw materials residue of Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia, Radix Scutellariae and mixes according to mass ratio 1:1:1:3.Wherein, Aesculus hippocastanum L. refers to its seed and bark, and large Fructus Arctii refers to its root and leaf, and Ramulus et Folium Spiraeae Salicifolia is its flower, and Radix Scutellariae is its root.
Wherein,
the dusty raw materials residue of Aesculus hippocastanum L., large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia, Radix Scutellariae is prepared in accordance with the following steps:
1) plant material Aesculus hippocastanum L., large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia or the Radix Scutellariae residue after extraction and application is collected, the present embodiment is remaining residue after ethanol extraction, concrete Extraction technique can be: extraction temperature 60 DEG C, extraction time 6 hours, volume fraction of ethanol is 80%, and solid-liquid ratio (mass ratio of plant material and ethanol) is 1:8.
2) Aesculus hippocastanum L. in step 1 after extraction and application, large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia or Radix Scutellariae residue are carried out drying, pulverize the dusty raw materials residue of formation 10 ~ 20 object Aesculus hippocastanum L., large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia or Radix Scutellariae afterwards.
its preparation technology of the facial film of embodiment 4 ~ 6 is substantially identical with the preparation technology of embodiment 1 ~ 3, does not repeat them here.
embodiment 4 ~ 6 effect:
Facial film prepared by embodiment 4 ~ 6 through 100 personnel 4 weeks on probation continuously, while with a commercially available declare to have well go the washing facial film of acne effect for comparative example 2.Tested object: each experimental group is 100 women (in 15-25 year, face has acne).Test zone and method: get 2-3g facial film uniform application in face, both hands finger to be looped massage gently in face, cleans up after 5 minutes with water.Use: twice daily, continue use 4 weeks.Test event: antiinflammatory anti-acne.Result on trial sees the following form 3.
Table 3
Facial film prepared by embodiment 4 ~ 6 is tried out 4 weeks continuously through 100 personnel, and the trier of more than 85% all feeds back acne and reduces, and does not all find the phenomenon such as chafe, allergy after on probation.
Embodiment 7 ~ 9(mono-kind has the facial film containing plant material residue of wrinkle removing effect)
The face pack prescription of embodiment 7,8,9 is substantially identical with the formula of the embodiment 1,2,3 shown in table 1 successively respectively, its difference is that plant material residue is different, the plant material residue added in embodiment 7 ~ 9 formula be Centaurea cyanus, Herba Centellae, Radix Ginseng, Flos Inulae dusty raw materials residue mix according to mass ratio 1:1:3:1.Wherein, Centaurea cyanus refers to the flower of its Centaurea cyanus, and Radix Ginseng is its root, and Flos Inulae is its flower.
Wherein,
the dusty raw materials residue of Centaurea cyanus, Herba Centellae, Radix Ginseng, Flos Inulae is prepared in accordance with the following steps:
1) plant material Centaurea cyanus, Herba Centellae, Radix Ginseng or the residue of Flos Inulae after extraction and application is collected, the present embodiment is remaining residue after ethanol extraction, concrete Extraction technique can be: extraction temperature 60 DEG C, extraction time 6 hours, volume fraction of ethanol is 80%, and solid-liquid ratio (mass ratio of plant material and ethanol) is 1:8.
2) residue of Centaurea cyanus left after extraction and application in step 1, Herba Centellae, Radix Ginseng or Flos Inulae is carried out drying, pulverize the dusty raw materials residue of formation 10 ~ 20 object Centaurea cyanus, Herba Centellae, Radix Ginseng or Flos Inulae afterwards.
its preparation technology of the facial film of embodiment 7 ~ 9 is substantially identical with the preparation technology of embodiment 1 ~ 3, does not repeat them here.
embodiment 7 ~ 9 effect:
Facial film prepared by embodiment 7 ~ 9 through 100 personnel 4 weeks on probation continuously, while commercially available declare to there is the washing facial film of good wrinkle removing effect for comparative example 3 with a.Tested object: each experimental group is 100 women (40-50 year).Test zone and method: get 2-3g uniform application in face, both hands finger to be looped massage gently in face, cleans up after 5 minutes with water.Use: twice daily, continue use 4 weeks.Test event: wrinkle removing.Result on trial sees the following form 4.
Table 4
Facial film prepared by embodiment 7 ~ 9 is tried out 4 weeks continuously through 100 personnel, and the trier of more than 85% all feeds back wrinkle and reduces, and does not all find the phenomenon such as chafe, allergy after on probation.
Embodiment 10 ~ 12(mono-kind has the facial film containing plant material residue of replenishing water and preserving moisture effect)
The face pack prescription of embodiment 10,11,12 is substantially identical with the formula of the embodiment 1,2,3 shown in table 1 successively respectively, its difference is that plant material residue is different, the plant material residue added in embodiment 10 ~ 12 formula be Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae, Herba Passiflorae Caeruleae dusty raw materials residue mix according to mass ratio 1:1:1:1.Wherein, Althaea officinalis L. refers to the root of Althaea officinalis L., and SONGGUOJU refers to the flower of SONGGUOJU, and Herba Passiflorae Caeruleae refers to its seed.
Wherein,
the dusty raw materials residue of Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae or Herba Passiflorae Caeruleae is prepared in accordance with the following steps:
1) plant material Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae or the residue of Herba Passiflorae Caeruleae after extraction and application is collected, the present embodiment is remaining residue after ethanol extraction, concrete Extraction technique can be: extraction temperature 60 DEG C, extraction time 6 hours, volume fraction of ethanol is 80%, and solid-liquid ratio (mass ratio of plant material and ethanol) is 1:8.
2) residue of Althaea officinalis L. left after extraction and application in step 1, SONGGUOJU, Flos Rosae Rugosae or Herba Passiflorae Caeruleae is carried out drying, pulverize the dusty raw materials residue of formation 10 ~ 20 object Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae or Herba Passiflorae Caeruleae afterwards.
its preparation technology of the facial film of embodiment 10 ~ 12 is substantially identical with the preparation technology of embodiment 1 ~ 3, does not repeat them here.
embodiment 10 ~ 12 effect:
Facial film prepared by embodiment 10 ~ 12 through 100 personnel 4 weeks on probation continuously, while commercially available declare to there is the washing facial film of good replenishing water and preserving moisture effect for comparative example 3 with a.Tested object: each experimental group is 100 women (20-30 year).Test zone and method: get 2-3g uniform application in face, both hands finger to be looped massage gently in face, cleans up after 5 minutes with water.Use: twice daily, continue use 4 weeks.Test event: replenishing water and preserving moisture.Result on trial sees the following form 5.
Table 5
Facial film prepared by embodiment 10 ~ 12 is tried out 4 weeks continuously through 100 personnel, and the trier of more than 92% all feeds back skin moisture-keeping well, and gloss is flexible, does not all find the phenomenon such as chafe, allergy after on probation.
Production practices prove, the compatibility of each component of face pack prescription of the present invention is good, and formula system is stablized.Facial film of the present invention wherein adds a certain amount of plant material residue, and prepared facial film zest is little, has certain skin care effect.After the present invention makes plant material be extracted utilization, remaining raw material residue can be turned waste into wealth, and plant material is better fully utilized, greatly reduces cost of material, also improve the utilization rate of plant material simultaneously.
Embodiment is above only the example set forth technical solution of the present invention, should not be understood to that the utilization of the present invention to plant material residue is confined to these concrete extraction processes about the description of the concrete extraction process of plant material being carried out to extraction and application in embodiment, in facial film of the present invention, the residue that plant material stays after extracting through alcohol extraction, water extraction, immersion method, supercritical carbon dioxide extraction method can be utilized, these residues are turned waste into wealth, also can play certain skin care effect simultaneously.
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore all contents not departing from technical solution of the present invention, according to technical spirit of the present invention to any simple modification made for any of the above embodiments, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.
Claims (6)
1. the facial film containing plant material residue, it is characterized in that, its formula of described facial film comprises each component of following mass percentage:
Described plant material residue is Radix Angelicae Sinensis, arnica montana, Radix Puerariae, Radix Glycyrrhizae dusty raw materials residue mix according to mass ratio 1:1:2:3;
Described dusty raw materials residue is prepared as follows: the residue that plant material is left after extraction and application carries out drying, is ground into 10 ~ 20 orders afterwards.
2., containing the facial film of plant material residue, it is characterized in that, described facial film its join
Side comprises each component of following mass percentage:
Described plant material residue is Aesculus hippocastanum L., the dusty raw materials residue of large Fructus Arctii, Ramulus et Folium Spiraeae Salicifolia, Radix Scutellariae mixes according to mass ratio 1:1:1:3; Described dusty raw materials residue is prepared as follows: the residue that plant material is left after extraction and application carries out drying, is ground into 10 ~ 20 orders afterwards.
3. the facial film containing plant material residue, it is characterized in that, its formula of described facial film comprises each component of following mass percentage:
Described plant material residue be Centaurea cyanus, Herba Centellae, Radix Ginseng, Flos Inulae dusty raw materials residue according to the mixing of mass ratio 1:1:3:1; Described dusty raw materials residue is prepared as follows: the residue that plant material is left after extraction and application carries out drying, is ground into 10 ~ 20 orders afterwards.
4. the facial film containing plant material residue, it is characterized in that, its formula of described facial film comprises each of following mass percentage
Described plant material residue be Althaea officinalis L., SONGGUOJU, Flos Rosae Rugosae, Herba Passiflorae Caeruleae dusty raw materials residue according to the mixing of mass ratio 1:1:1:1; Described dusty raw materials residue is prepared as follows: the residue that plant material is left after extraction and application carries out drying, is ground into 10 ~ 20 orders afterwards.
5. the facial film containing plant material residue according to any one of Claims 1 to 4, is characterized in that, the mass percentage of plant material residue contained in face pack prescription is 1-5%.
6. the facial film containing plant material residue according to any one of Claims 1 to 4, it is characterized in that, the residue of described plant material left by after extraction and application refers to the residue that plant material is left after one or more extraction processes in alcohol extraction, water extraction, immersion method, supercritical carbon dioxide extraction method are extracted.
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| CN201310389135.7A CN103432043B (en) | 2013-08-30 | 2013-08-30 | Face mask containing plant material residues |
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| CN201310389135.7A CN103432043B (en) | 2013-08-30 | 2013-08-30 | Face mask containing plant material residues |
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| CN102871883B (en) * | 2012-10-22 | 2013-12-18 | 上海韬鸿投资管理咨询有限公司 | Elastic activated skin care compound essential oil |
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| CN106860068A (en) * | 2017-01-17 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment moisturizing essence |
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Inventor after: Zhao Guang Inventor before: Cai Yiwen |
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Effective date of registration: 20170220 Address after: Baiyun District of Guangzhou City, Guangdong province 510442 Yong Ping Jie Dongping Cun Ma Shi Ling Dongfeng West Road No. 31-4 Patentee after: Guangzhou City, a thousand grass grass Cosmetics Co., Ltd. Address before: 510370 Guangdong province Guangzhou City Creek Road in Panlong industrial zone of Liwan District dragon two friends of a 6 storey industrial building Patentee before: Guangzhou Danqi Daily Chemical Factory Co., Ltd. |