CN104800126A - Plant extraction solution composite with skin care and conditioning effects, preparation method and application - Google Patents
Plant extraction solution composite with skin care and conditioning effects, preparation method and application Download PDFInfo
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Abstract
The invention relates to the technical field of plant extraction solution composites, in particular to a plant extraction solution composite with skin care and conditioning effects, a preparation method and an application of the composite. The plant extraction solution composite with the skin care and conditioning effects comprises the following plants: herbal selaginellae, seaweed, rhodiola rosea, centella asiatica, honeysuckle, ginger, chamomile and purslane. The plant extraction solution composite with the skin care and conditioning effects is low in formula cost, good in skin care and conditioning effects and high in oxidation resistance and moisture retention, can obviously improve water absorption and locking capacity of skin, has effects of inflammation resistance, irritation resistance, skin soothing and the like, and is applicable to sensitive skin and anti-acne and after-sun repair products.
Description
Technical field
The present invention relates to plant extraction liquid technical field of compositions, more specifically, relate to a kind of plant extraction liquid composition and method of making the same and the application with skin protection opsonic action.
Background technology
Herba Selaginellae is a kind of desert plant, because it can when almost being dried " resurrection " and well-known completely.When extreme drought, its branch and leaf can tightly be shrunk to spherical, firmly pin precious last in body to drip, even if lose self moisture up to 98%, still can indomitable existence many decades, contain abundant glycosyl trehalose this is because bring back to life in cursive script, powerful lock water moisture-keeping functions can be played, then the water containing vitality is imported in body in each cell, and pin the moisture being equivalent to cell own wt 450 times.Be in this most magical in all plants found at present, the most effectively lock water mode.At present, the domestic research to this plant and extracting method are also very limited; Lang De company of Korea S hundred is the company that a Specialty Graduate produces plant extraction liquid, the Herba Selaginellae extracting solution content that company produces is higher, about 10%, but because it adopts alcohol extraction process, also unsatisfactory in preserving moisture and protecting skin effect, need interpolation more than 5% just can reach the moistening effect that can detect, formulation cost is higher.
Summary of the invention
The present invention is intended to solve the problems of the technologies described above at least to a certain extent.
Primary and foremost purpose of the present invention is to provide a kind of plant extract fluid composition with skin protection opsonic action, and the cost of its formula is low, and skin protection opsonic action is effective.
A further object of the present invention is to provide a kind of preparation method with the plant extract fluid composition of skin protection opsonic action.
3rd object of the present invention provides the application of above-mentioned plant extract fluid composition in skin protection conditioning further.
For solving the problems of the technologies described above, the technical solution used in the present invention is:
There is provided a kind of plant extract fluid composition with skin protection opsonic action, described plant is composed of the following components: Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Flos Lonicerae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae and Herba Portulacae.
The plant extract fluid composition that the present invention has skin protection opsonic action is made up of following parts by weight: Herba Selaginellae extracting solution 1 ~ 3 part, seaweed extracted liquor 2 ~ 4 parts, Radix Rhodiolae extracting solution 1 ~ 3 part, Herba Centellae extracting solution 1 ~ 3 part, Flos Lonicerae extractive solution 2 ~ 4 parts, ginger extract 1 ~ 2 part, Flos Matricariae chamomillae extracting solution 1 ~ 3 part, Herba Portulacae extract 2 ~ 4 parts.
Wherein, Herba Selaginellae can recover cell viability, has well lock water moisture-keeping function; Sargassum has antibacterial, antiviral, antiinflammatory, antioxidation, radioprotective, anti-ageing effect of waiting for a long time; Radix Rhodiolae has whitening, antioxidation, radiation-resistant effect; Herba Centellae can effectively promote fibroblast and collagen, accelerates the injured skin even reparation of tendon, reaches effect of scar eliminating, anti-acne print, reparation; Flos Lonicerae has antibacterial, effect such as antiviral, antiinflammatory, immunity moderation; Rhizoma Zingiberis Recens has and promotes the effect such as cutaneous circulation, comfortable, antipruritic, antiinflammatory, antibacterial, antioxidation; Flos Matricariae chamomillae can strengthen and extend epidermal stem cells (TA) vigor, promotes new Hemapoiesis; The effect such as Herba Portulacae has antiinflammatory, antipruritic, antiallergic, free radical resisting, calmness are releived.
Such scheme preferably, is made up of following parts by weight: Herba Selaginellae extracting solution 1 part, seaweed extracted liquor 2 parts, Radix Rhodiolae extracting solution 1 part, Herba Centellae extracting solution 1 part, Flos Lonicerae extractive solution 2 parts, ginger extract 1 part, Flos Matricariae chamomillae extracting solution 1 part, Herba Portulacae extract 2 parts.
In such scheme, the extracting solution of described Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae, Herba Portulacae adopts alcohol extracting method to extract.
Preferably, described alcohol extracting method adopts 75% alcoholic solution as solvent, and Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae or Herba Portulacae are soaked in 4h in described 75% alcoholic solution, and under the condition of 80 DEG C reflux, extract.The follow-up extraction completing extracting solution respectively through the operation such as concentrating under reduced pressure, spraying dry.
In such scheme, described Flos Lonicerae extractive solution adopts supercritical carbon dioxide extraction, using supercritical carbon dioxide as solvent, extracts chlorogenic acid active component from solid honeysuckle plant.
The present invention also provides a kind of as the above-mentioned preparation method with the plant extract fluid composition of skin protection opsonic action, comprises the following steps:
S1. be soaked in 75% alcoholic solution respectively by 1 ~ 3 weight portion Herba Selaginellae, 2 ~ 4 weight portion Sargassums, 1 ~ 3 weight portion Radix Rhodiolae, 1 ~ 3 weight portion Herba Centellae, 1 ~ 2 weight portion Rhizoma Zingiberis Recens, 1 ~ 3 weight portion Flos Matricariae chamomillae, 2 ~ 4 weight portion Herba Portulacaes, after soaking 4h, under the condition of 80 DEG C, reflux, extract, obtains the extracting solution of each raw material; 2 ~ 4 weight portion Flos Lonicerae extractive solutions are adopted supercritical carbon dioxide extraction;
S2. by Radix Rhodiolae extracting solution and Herba Centellae extracting solution respectively with water dissolution to transparent, obtain lysate one, lysate two;
S3. seaweed extracted liquor is even with water dissolution, obtain lysate three;
S4. Herba Selaginellae extracting solution, Flos Lonicerae extractive solution, ginger extract, Flos Matricariae chamomillae extracting solution, Herba Portulacae extract are added water, be warming up to 55 ~ 60 DEG C, stirring and evenly mixing together with the lysate three that the lysate one obtained with step S2 and lysate two, step S3 obtain, has the plant extract fluid composition of skin protection opsonic action described in obtaining.
In such scheme, preferably, in described step S1, be soaked in 75% alcoholic solution respectively by 1 weight portion Herba Selaginellae, 2 weight portion Sargassums, 1 weight portion Radix Rhodiolae, 1 weight portion Herba Centellae, 1 weight portion Rhizoma Zingiberis Recens, 1 weight portion Flos Matricariae chamomillae, 2 weight portion Herba Portulacaes, after soaking 4h, under the condition of 80 DEG C, reflux, extract, obtains the extracting solution of each raw material; 2 weight portion Flos Lonicerae extractive solutions are adopted supercritical carbon dioxide extraction.
The present invention still further provides the above-mentioned application of plant extract fluid composition in skin protection conditioning.
Compared with prior art, the invention has the beneficial effects as follows:
The formulation cost that the present invention has the plant extract fluid composition of skin protection opsonic action is low, and skin protection opsonic action is effective, the Herba Selaginellae extracting solution collocation of being rich in glycosyl trehalose is rich in the seaweed extracted liquor of Sargassum polysaccharides by it, improve the absorption of moisture and the ability of water conservation, improve lock outlet capacity, the elasticity of skin is increased; Radix Rhodiolae contains rhodioside, higher to the scavenging action of OH, has good antioxidation; Flos Lonicerae contains active chlorogenic acid, has good inhibitory action to common antibacterial; And Herba Centellae contains active asiaticoside, saponin, all there is certain inhibitory action to staphylococcus aureus, Propiobacterium, effectively can also promote the synthesis of fibroblast and collagen protein I and III, collocation Rhizoma Zingiberis Recens, play the effect of invigorating blood circulation, accelerate the reparation of injured skin; Meanwhile, in order to alleviate responsive skin, impaired skin to the tolerance degree of plant extraction liquid, adding Flos Matricariae chamomillae, Herba Portulacae, reaching effect of antiallergic, antiinflammatory.
Above-mentioned eight kind of plant book on Chinese herbal medicine compositions combine with a certain proportion of parts by weight by the present invention, be rich in the non-oxidizability that high activity antioxidant content (as flavonoid, unsaturated fatty acids, vitamins) carrys out supplementary skin, to improve the activity of skin endogenous anti-oxidative enzyme, prevent the formation of free radical, block the snperoxiaized process of body lipid, thus Cell protection is from peroxide injury, maintain the normal physiological function of cell; On the other hand, for damaged skin, by the mutual cooperative effect before each composition of various plants extracting solution, the current potential drop of direct reduction redox reaction, increase antioxidant effect, by detecting, the clearance rate of DPPH free radical significantly being improved, better can prevent skin injury.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is further illustrated, but specific embodiment does not do any restriction to the present invention, and protection scope of the present invention should be as the criterion with claim.
The each embodiment of table 1 proportioning parameter by weight
Contrast test is carried out below respectively by four kinds of method of testings.
(1) to the scavenging action of DPPH free radical
Method of testing: 2, bitter diazanyl free radical (DPPH) analytic process of 2-diphenyl-1-has single electron according to DPPH free radical and have the characteristic of strong absorption (in darkviolet) at 517nm place, with spectrophotography, quantitative analysis is carried out to free radical scavenging degree, in order to the oxidation resistance of evaluation experimental sample.
Test result: in the reaction system of 0.025mg/mlDPPH free radical, eight kinds of natural botanical extraction liquid compositionss of the embodiment of the present invention, to the Scavenging activity of DPPH free radical, are far longer than independent plant extract (Radix Rhodiolae).Wherein, the scavenging action of plant extract fluid composition to DPPH free radical become according to embodiment one each ingredients weight parts array is better, and embodiment two, three is taken second place.
(2) skin surface water content test
Method of testing: choose 14 voluntary testers, in the position of right hand inner forearm 5 square centimeters, draw test difference, test respectively with water tester and use the water content of front skin and use the moisture content of skin after latter 2 hours, compare group with untreated skin simultaneously, calculate the percentage rate % that water content increases.
Test result: the eight kinds of natural botanical extraction liquid compositionss adopting the embodiment of the present invention, added 12 ~ 15% relative to the skin of matched group containing water gaging after 2 hours.Wherein, the moisture content of skin of the plant extract fluid composition test become according to each ingredients weight parts array of embodiment one adds 15%, best results, and embodiment two, three is taken second place.
(3) raw material irritant test is reduced
Method of testing: adopt zein method (zein), zein is almost completely water insoluble, but after its and surfactant interact, water solublity increase; Sodium laureth sulfate (AES) aqueous solution easily makes zein dissolve, therefore by detecting the situation of change of nitrogen content before and after in AES aqueous solution, and the ammon amount situation of change after interpolation plant extraction liquid, zein and the dissolubility tested after sample effect can be determined, and the nitrogen content in the zein dissolved is directly proportional to the skin irritation that surfactant causes, irritating size can be judged thus.
Test result:
1%AES active matter aqueous solution zest: Zein value/mgNL
-1=5100.
The plant extraction liquid zest of 1%AES active matter aqueous solution+1%: Zein value/mgNL
-1=1520.
Test result illustrates that embodiment of the present invention plant extract fluid composition obviously can reduce the stimulation of surfactant base, and ideal according to the test result of the plant extract fluid composition of embodiment one each ingredients weight parts array one-tenth.
(4) toxicology test
Method of testing: carry out dermoreaction scoring by " cosmetics health specification " (version in 2007) skin irritation/corrosion test, carry out overall merit with the meansigma methods of tested material animal integration, and observe other toxic action except zest.
Show through toxicology test:
Acute skin irritation result of the test is: nonirritant.
In the embodiment of the present invention, the preparation method step with the plant extract fluid composition of skin protection opsonic action is as follows:
S1. be soaked in 75% alcoholic solution respectively by the Herba Selaginellae of formulation weight number, Sargassum, Radix Rhodiolae, Herba Centellae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae and Herba Portulacae, after soaking 4h, under the condition of 80 DEG C, reflux, extract, obtains the extracting solution of each raw material; The Flos Lonicerae extractive solution of formulation weight number is adopted supercritical carbon dioxide extraction simultaneously;
S2. by Radix Rhodiolae extracting solution and Herba Centellae extracting solution respectively with water dissolution to transparent, obtain lysate one, lysate two;
S3. seaweed extracted liquor is even with water dissolution, obtain lysate three;
S4. Herba Selaginellae extracting solution, Flos Lonicerae extractive solution, ginger extract, Flos Matricariae chamomillae extracting solution, Herba Portulacae extract are added water, be warming up to 55 ~ 60 DEG C, stirring and evenly mixing together with the lysate three that the lysate one obtained with step S2 and lysate two, step S3 obtain, has the plant extract fluid composition of skin protection opsonic action described in obtaining.
In actual use, this effect acquired by the application of plant extract fluid composition in skin protection conditioning is ideal, oxidation resistance and moisture retention are comparatively strong, can significantly improve skin to the absorption of moisture and lock outlet capacity, and there is antiinflammatory, irritation, effects such as skin of releiving.Be applicable to sensitivity skin and anti-pox, shine the products such as rear reparation.
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and is not the restriction to embodiments of the present invention.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.All any amendments done within the spirit and principles in the present invention, equivalent to replace and improvement etc., within the protection domain that all should be included in the claims in the present invention.
Claims (9)
1. have a plant extract fluid composition for skin protection opsonic action, it is characterized in that, described plant is composed of the following components: Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Flos Lonicerae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae and Herba Portulacae.
2. the plant extract fluid composition with skin protection opsonic action according to claim 1, it is characterized in that, be made up of following parts by weight: Herba Selaginellae extracting solution 1 ~ 3 part, seaweed extracted liquor 2 ~ 4 parts, Radix Rhodiolae extracting solution 1 ~ 3 part, Herba Centellae extracting solution 1 ~ 3 part, Flos Lonicerae extractive solution 2 ~ 4 parts, ginger extract 1 ~ 2 part, Flos Matricariae chamomillae extracting solution 1 ~ 3 part and Herba Portulacae extract 2 ~ 4 parts.
3. the plant extract fluid composition with skin protection opsonic action according to claim 2, it is characterized in that, be made up of following parts by weight: Herba Selaginellae extracting solution 1 part, seaweed extracted liquor 2 parts, Radix Rhodiolae extracting solution 1 part, Herba Centellae extracting solution 1 part, Flos Lonicerae extractive solution 2 parts, ginger extract 1 part, Flos Matricariae chamomillae extracting solution 1 part and Herba Portulacae extract 2 parts.
4. the plant extract fluid composition with skin protection opsonic action according to claim 2, is characterized in that, the extracting solution of described Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae and Herba Portulacae adopts alcohol extracting method to extract.
5. the plant extract fluid composition with skin protection opsonic action according to claim 4, it is characterized in that, described alcohol extracting method adopts 75% alcoholic solution as solvent, Herba Selaginellae, Sargassum, Radix Rhodiolae, Herba Centellae, Rhizoma Zingiberis Recens, Flos Matricariae chamomillae or Herba Portulacae are soaked in 4h in described 75% alcoholic solution, and under the condition of 80 DEG C reflux, extract.
6. the plant extract fluid composition with skin protection opsonic action according to claim 2, is characterized in that, described Flos Lonicerae extractive solution adopts supercritical carbon dioxide extraction.
7. the preparation method with the plant extract fluid composition of skin protection opsonic action as described in any one of claim 1 to 6, is characterized in that, comprise the following steps:
S1. be soaked in 75% alcoholic solution respectively by 1 ~ 3 weight portion Herba Selaginellae, 2 ~ 4 weight portion Sargassums, 1 ~ 3 weight portion Radix Rhodiolae, 1 ~ 3 weight portion Herba Centellae, 1 ~ 2 weight portion Rhizoma Zingiberis Recens, 1 ~ 3 weight portion Flos Matricariae chamomillae and 2 ~ 4 weight portion Herba Portulacaes, after soaking 4h, under the condition of 80 DEG C, reflux, extract, obtains the extracting solution of each raw material; 2 ~ 4 weight portion Flos Lonicerae extractive solutions are adopted supercritical carbon dioxide extraction;
S2. by Radix Rhodiolae extracting solution and Herba Centellae extracting solution respectively with water dissolution to transparent, obtain lysate one, lysate two;
S3. seaweed extracted liquor is even with water dissolution, obtain lysate three;
S4. Herba Selaginellae extracting solution, Flos Lonicerae extractive solution, ginger extract, Flos Matricariae chamomillae extracting solution, Herba Portulacae extract are added water, be warming up to 55 ~ 60 DEG C, stirring and evenly mixing together with the lysate three that the lysate one obtained with step S2 and lysate two, step S3 obtain, has the plant extract fluid composition of skin protection opsonic action described in obtaining.
8. the preparation method with the plant extract fluid composition of skin protection opsonic action according to claim 7, it is characterized in that, in described step S1, be soaked in 75% alcoholic solution respectively by 1 weight portion Herba Selaginellae, 2 weight portion Sargassums, 1 weight portion Radix Rhodiolae, 1 weight portion Herba Centellae, 1 weight portion Rhizoma Zingiberis Recens, 1 weight portion Flos Matricariae chamomillae and 2 weight portion Herba Portulacaes, after soaking 4h, under the condition of 80 DEG C, reflux, extract, obtains the extracting solution of each raw material; 2 weight portion Flos Lonicerae extractive solutions are adopted supercritical carbon dioxide extraction.
9. the application of plant extract fluid composition in skin protection conditioning according to any one of claim 1 to 6.
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Cited By (7)
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CN105055253A (en) * | 2015-08-29 | 2015-11-18 | 广州煜明生物科技有限公司 | Natural moisturizing composition, preparation method thereof and application to cosmetics |
CN105176702A (en) * | 2015-09-10 | 2015-12-23 | 潘福昆 | Kitchen cleaner |
CN106420530A (en) * | 2016-11-21 | 2017-02-22 | 威莱(广州)日用品有限公司 | Plant extract liquid composition with skin protecting and conditioning functions and method for preparing plant extract liquid composition |
CN107115232A (en) * | 2017-04-25 | 2017-09-01 | 广州雅纯化妆品制造有限公司 | A kind of liquid of releiving of refreshing oneself applied to cosmetics |
CN107811895A (en) * | 2017-12-28 | 2018-03-20 | 广东医科大学 | Marine alga repair hydrosol and preparation method thereof |
CN110123953A (en) * | 2019-05-09 | 2019-08-16 | 中山卡丝生物科技有限公司 | Cold compress patch for promoting postoperative skin repair and preparation method thereof |
CN110279511A (en) * | 2019-07-30 | 2019-09-27 | 湖南优感觉生物科技有限公司 | It is a kind of to facilitate the sheath that environment maintains in vagina |
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Cited By (8)
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CN105055253A (en) * | 2015-08-29 | 2015-11-18 | 广州煜明生物科技有限公司 | Natural moisturizing composition, preparation method thereof and application to cosmetics |
CN105055253B (en) * | 2015-08-29 | 2018-02-23 | 广州煜明生物科技有限公司 | A kind of natural moisture preserving composition and preparation method thereof and the application in cosmetics |
CN105176702A (en) * | 2015-09-10 | 2015-12-23 | 潘福昆 | Kitchen cleaner |
CN106420530A (en) * | 2016-11-21 | 2017-02-22 | 威莱(广州)日用品有限公司 | Plant extract liquid composition with skin protecting and conditioning functions and method for preparing plant extract liquid composition |
CN107115232A (en) * | 2017-04-25 | 2017-09-01 | 广州雅纯化妆品制造有限公司 | A kind of liquid of releiving of refreshing oneself applied to cosmetics |
CN107811895A (en) * | 2017-12-28 | 2018-03-20 | 广东医科大学 | Marine alga repair hydrosol and preparation method thereof |
CN110123953A (en) * | 2019-05-09 | 2019-08-16 | 中山卡丝生物科技有限公司 | Cold compress patch for promoting postoperative skin repair and preparation method thereof |
CN110279511A (en) * | 2019-07-30 | 2019-09-27 | 湖南优感觉生物科技有限公司 | It is a kind of to facilitate the sheath that environment maintains in vagina |
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Application publication date: 20150729 |