CN105395442A - Natural plant long-lasting moisturizing composition and use thereof - Google Patents
Natural plant long-lasting moisturizing composition and use thereof Download PDFInfo
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- CN105395442A CN105395442A CN201610015806.7A CN201610015806A CN105395442A CN 105395442 A CN105395442 A CN 105395442A CN 201610015806 A CN201610015806 A CN 201610015806A CN 105395442 A CN105395442 A CN 105395442A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a natural plant long-lasting moisturizing composition prepared from shiny-leaved yellowhorn oil, a synergist and a solvent. By fully playing the role of synergetic moisturizing of the synergist in the composition, the problem of dry skin can be solved fundamentally, moisture needed by the inside of the skin can be supplemented, water loss of the skin surface can be successfully avoided, the wetness of the skin can be kept for a long time, addition of an aseptic is not needed, irritation of other raw materials in a cosmetic to the skin is greatly reduced, and the natural plant long-lasting moisturizing composition is excellent in moisturizing effect, longer in moisturizing time, easy to use, safe, effective, and harmless to a human body.
Description
Technical field
The present invention relates to the long-acting moisture-keeping composition of a kind of natural plants, particularly relate to by long-acting moisture-keeping composition of the natural plants of shinyleaf yellowhorn oil, synergetic effect additive and solvent composition and uses thereof.
Background technology
Although existing wetting agent has many advantages, but still may there are some defects, and often interpolation kind is more, moistening effect does not play long-acting moisturizing.
As polyalcohols wetting agent, this constituents is cheap, and safety is higher.Shortcoming is then: moistening effect is easier to the humidity effect by environment, and when the relative humidity of environment is too low, the effect retaining hydrone can decline, and in addition, reach the object of efficient moisture-retention, is limited to the mechanism of itself, more difficultly reaches.Long-time moistening effect is also undesirable, such as glycerol, have another name called glycerol, its good water absorption is two-way, and both can absorb moisture from air is skin moisture-keeping, also moisture can be absorbed from skin, and make skin drier, cutaneous normal function, the words that especially use amount is large, can be too greasy, likely can blocked pore and cause acne and acne.
Fatty acid is the fat-soluble skin moistening moisturizing ingredient of a class.Fatty acid molecule varies in size, and has saturated and unsaturated dividing.Unsaturated fatty acid is the important component part of sebum film, and the composition such as NMF, ceramide together forms intercellular substance important between horn cell, conducts other active component, forms complete skin barrier.Casual injury, may will destroy skin barrier, allow it more be difficult to resist environmental stimuli, easy rubescent sensitivity.Equally, if suitably these nutrition can be supplemented when skin is problematic, barrier will be helped to recover, but undersaturated fatty acid, such as linolenic acid, linoleic acid, oleic acid etc., because these fatty acid nutritives enrich, likely small pox inducement on the contrary---the hair follicle of some people is extremely responsive to free fatty, inflammation can be stimulated by it, and unsaturated fatty acid is easily oxidized, there is situations such as going bad, become sour, even have antibacterial at amount reproduction, so when adding above-mentioned nutritional labeling, also can corresponding interpolation or increase antiseptic consumption.
Lignum Xanthoceratis belongs to Sapindaceae Lignum Xanthoceratis and belongs to, and being also referred to as civil official fruit, xanthoceras sobifolia bunge etc., is the woody seeds of the distinctive preciousness of China.
Chinese patent CN102784089A, mention shinyleaf yellowhorn shell very high containing Saponin amount, colorimetric determination reaches 4%, and shinyleaf yellowhorn shell Saponin has the effect of anti-hypoxia, antioxidation, resisting fatigue; Chinese patent CN102823873A shinyleaf yellowhorn shell is very high containing flavone amount, and has the effect of anti-hypoxia, antioxidation, resisting fatigue.
Nutritional labeling in shinyleaf yellowhorn oil: unsaturated fatty acid content accounts for 94%, and (linoleic acid accounts for 36.9%, oleic acid accounts for 57.1%), saponin of Lignum Xanthoceratis accounts for 0.5%, and other are 18 kinds of trace element and the VB such as 19 seed amino acids, potassium, sodium, calcium, magnesium, ferrum, zinc of needed by human body
1, VB
2, VC, VE, VA, the multivitamin such as carotene.
The processing technique that the preparation of shinyleaf yellowhorn oil generally takes milling process and carbon dioxide supercritical extraction method to combine at present.
Production technology: wait physical method to produce through selected Lignum Xanthoceratis seed → mistake sieve classification → cleaning → shelling → sorting → kernel parch → pulverize → add water steaming and decocting → removal bitterness → cake → carbon dioxide supercritical fluid extraction processed → complete purification → shinyleaf yellowhorn oil → packaging → warehouse-in, do not add any spice or additive, and Lignum Xanthoceratis is wild or dry crop, there is no pesticide, chemical fertilizer and other pollutions.
Mention in " preliminary study of Lignum Xanthoceratis study on chemical compositions of leaves " (Shenyang Inst. of Applied Ecology, Chinese Academy of Sciences Zhu Dan etc.) literary composition: containing soaping agents, tannin, sugar, polysaccharide etc. in experiment Lignum Xanthoceratis leaf, analyze from threpsology and medicine and pharmacology aspect, the value of Lignum Xanthoceratis leaf is very considerable.
Lignum Xanthoceratis all has certain curative effect to hypertension, sclerosis of blood vessels, cellulitis stone disease, rheumatism, nerve enuresis and anti-inflammatory analgetic etc., is also to manufacture the first-class raw material of paint, machinery oil, lubricating oil and soap, but application in cosmetics is considerably less.
The present invention is according to above-mentioned prior art, and provide a kind of based on shinyleaf yellowhorn oil, additional synergetic effect additive, solvent, without the need to adding antiseptic, does not increase expensive cosmetic material, the natural long-acting moisture-keeping composition that use cost is lower and purposes.
Summary of the invention
The invention provides a kind of containing shinyleaf yellowhorn oil, the long-acting moisture-keeping composition of natural plants of additional synergetic effect additive and solvent composition, by giving full play to the collaborative moisture-keeping function of synergist in compositions, can fundamentally solve xerodermatic problem, moisture needed for skin inside can be supplemented, successfully can pin again the loss of skin surface moisture, the water of skin is kept to moisten for a long time, and without the need to adding antiseptic, to greatly reduce in cosmetics other raw materials to the zest of skin, moistening effect is excellent, and moisture preserving time is longer, easy use, and it is safe and effective, harmless.
The long-acting moisture-keeping composition of natural plants of the present invention, containing shinyleaf yellowhorn oil, synergetic effect additive and solvent, this moisture-keeping composition enhances the moistening effect of skin moisturizing, lock water, and without the need to adding antiseptic, antioxygenic property is good, and effect stability is easy to use.
In described natural plants moisture-keeping composition, shinyleaf yellowhorn oil weight percentage is 1.0-40%; Be preferably 5.0-15%;
Synergetic effect additive weight percentage is 1.0-50%; Be preferably 20-45%;
Weight of solvent percentage composition is 20-80%, is preferably 40-70%.
Described synergetic effect additive is the mixture of at least one in sorbitol, Polyethylene Glycol, 1,2-decanediol, Sensiva SC50.
Described solvent is one or both the mixture in water, shinyleaf yellowhorn shell aqueous extract, Lignum Xanthoceratis branch aqueous extract, Lignum Xanthoceratis leaf aqueous extract;
Described shinyleaf yellowhorn fruit shell aqueous extract is make to be soaked in water the solution of shinyleaf yellowhorn shell gained, preparation method: by 100%, take the shinyleaf yellowhorn shell of 10%-50%, be cut into small pieces or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described shinyleaf yellowhorn shell aqueous extract;
Described Lignum Xanthoceratis branch aqueous extract is make to be soaked in water the solution of Lignum Xanthoceratis branch gained, preparation method: by 100%, take the Lignum Xanthoceratis branch of 10%-50%, be cut into segment or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described Lignum Xanthoceratis branch aqueous extract;
Described Lignum Xanthoceratis leaf aqueous extract is make to be soaked in water the solution of Lignum Xanthoceratis fruit leaf gained, preparation method: by 100%, take the Lignum Xanthoceratis leaf of 10%-50%, be cut into small pieces or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described Lignum Xanthoceratis leaf aqueous extract.
Described natural plants moisture-keeping composition can be used in the product such as personal care articles, wet tissue.The present composition can adopt this area conventional method preparation; Or preparation method is: stir after shinyleaf yellowhorn oil and solvent are added container, then add synergetic effect additive, be warming up to 40-60 DEG C, be stirred to entirely molten after be down to room temperature and get final product; Or continue to filter, subpackage.This compositions can play the effect of long-acting moisturizing at lower addition (2% ~ 5%).
The present invention also comprises the product such as personal care articles, wet tissue containing above-mentioned natural plants moisture-keeping composition.The products such as described personal care articles, wet tissue, comprise all products in this area, as cream frost, emulsion, cleansing milk, shampoo, bath gel, handwashing liquid, toothpaste, cosmetic water, facial mask essence, wet tissue series products etc.
Wetting agent is in order to simulate the natural moisture preserving system be made up of oil, water, NMF in human body skin, and effect is that delaying moisture content loses, increases the infiltration of dermal-epidermal moisture content.For skin temporarily provides protection, reduces damage, promotes repair process.Skin moisturizer is made up of main component and other auxiliary elements.Main component comprises sealer, hygroscopic agent, hydrophilic matrix etc., and auxiliary element has emulsifying agent, antiseptic etc.
Natural safe, nontoxic, the environmental protection of natural plants wetting agent raw material of the present invention, harmless, simulate natural moisture preserving system completely, skin is served to the effect of long-acting moisturizing.Shinyleaf yellowhorn oil not only provides abundant oleic acid, linoleic acid, and comprises other multivitamins such as the 18 kinds of trace element such as 19 seed amino acids, potassium, sodium, calcium, magnesium, ferrum, zinc being needed by human body and VB1, VB2, VC, VE, VA, carotene.
Solvent is all the raw material that is easy to get of Lignum Xanthoceratis: branch, shell, fruit leaf, without the need to deep processing, without extractant extractions such as toluene, ether, chloroforms, avoid the injury of chemical reagent, no solvent residue, raw material is easy to get, cost is low, directly uses water extraction, gets the supernatant.And containing Multiple components in above raw material:
1. as Saponin, can scavenging free radicals, antioxidation, can increase the non-oxidizability of compositions, ensures the steady quality of compositions, and antiseptic effect is good, and itself has good protective effect to skin.
2., as sugar, polysaccharide, be applied in compositions, moisturizing can be produced, stablize, improve the colour of skin, the function such as antibacterial, better with other conventional cosmetics compatibility; Can form the uniform thin film of one deck at skin surface, reduce the moisture evaporation of skin surface, make moisture permeate into horny layer from substrate microstructure, the further aquation of induction horny layer, preserves the moisture of skin self, and completes skin moistening effect.
The synergetic effect additive used is alcohols, can have again soft and smooth skinfeel, and have the effect of antisepsis and sterilization while raising compositions moisturizing effect.
No matter be traditional glycerol, or now advanced hyaluronic acid, the too low moisturizing poor effect of concentration, moisture in skin corium can be drawn out when concentration is too high, belong to the phenomenon of " suck-back ": namely moisture absorbing component is too high, make related solution not only from air, also absorb moisture from skin, make originally to wish that moistening skin is done all the better.
And natural plants moisture-keeping composition of the present invention, concentration is high and low, all can not affect its moisture-keeping efficacy, also there will not be " suck-back " phenomenon, three's Synergistic, serve the function of natural moisture preserving system: as the fatty acid contained in composition each in compositions, successfully pin moisture, prevent moisture from evaporating; Each seed amino acid, draws outside moisture, and can penetrate into horny layer and play a role; Needed by human vitamin, can repair corneocyte, nourishes rough skin; Sugar, polysaccharide etc., can get up free water molecules.Common raising skin defencive function, doubles to promote skin water content and storage capacity, careful skin pattern; and Saponin, the sterols in alcohols or solvent, while moisturizing, the skin problem that may can also cause nutritious fatty acid; play antiinflammatory, the effect of calming down.
Natural plants moisture-keeping composition of the present invention, not only effectively improves shinyleaf yellowhorn oil effect to skin moisture-keeping, but also has stronger antioxidation, can directly use, without the need to adding antiseptic.The natural plants moisture-keeping composition of the present invention suitability is wide, and use amount is little, and alternative conventional wetting agent adds in the cosmetics such as emulsion, cream frost, facial mask essence.
Accompanying drawing explanation
Fig. 1 is moisture-keeping composition of the present invention and hyaluronic acid water content curve comparison figure.
Fig. 2 to be moisture-keeping composition of the present invention with the moisture of skin containing single moisturizing ingredient emulsion, composition emulsion scatter and disappear test value curve comparison figure.
Fig. 3 is that moisture-keeping composition of the present invention is to DPPH free radical scavenging activity.
Detailed description of the invention
The following examples contribute to the present invention of those skilled in the art's comprehend, but do not limit the present invention in any way.
Embodiment 1
The each formula inventory (% by weight) of table 1. natural plants moisture-keeping composition
Compound method: in the appropriate size there-necked flask (as 250mL) of being with stirring and thermometer, according to the inventory of each formula of table 1, first add shinyleaf yellowhorn oil and stirring solvent, add synergetic effect additive again, be warming up to 60 DEG C, be stirred to entirely molten after be down to room temperature, stable natural plants moisture-keeping composition can be obtained.
Embodiment 2
Moistening effect is evaluated.
For studying the moisture retention of moisture-keeping composition, moisture-keeping composition 1#-2#, 5%4# of prepared by embodiment 1 2% under (61% (envionmental humidity of potassium sulfate saturated solution exsiccator is 61%)), are measured its moisturizing rate from 10% glycerol, 3% saturating trehalose respectively under different relative humidity.Assay method is according to the ex vivo assessment method-weight method of wetting agent moisture-keeping efficacy.The results are shown in Table 2.
Equipment: exsiccator, calorstat, analytical balance, thermometer;
Determine to measure environment: 61% (envionmental humidity of potassium sulfate saturated solution exsiccator is 61%);
Moisturizing rate measures: the sample taking a certain amount of moisture content, be placed in room temperature respectively, in the exsiccator of moisture constant (61%), place the minimizing that different time (4h, 8h, 24h) claims its quality afterwards, calculate the water retention of sample, by relative analysis, compare the size of different sample moisture retention.
Computing formula is as follows:
Moisturizing rate (%)=(M
t-n-m
t-0)/M
t-0* 100%
M in formula
t-n-place sample quality after n hour;
M
t-0sample quality before-placement.
Rate of descent %=(the B of moisturizing rate
t2-B
t1)/B
t1* 100%
B in formula
t1-under identical relative humidity conditions, the moisturizing rate after t1 hour placed by sample;
B
t2-under identical relative humidity conditions, the moisturizing rate after t2 hour placed by sample.
Table 2.2% natural plants moisture-keeping composition 1#-2#, 5%4# and 10% glycerol, 3% the moisturizing rate of trehalose
As can be seen from Table 2: under the humidity of 61%, each sample was the moisturizing rate of 4 hours, 8 hours, 24 hours, and the order of each sample moisturizing rate is: 5%4#>2%2#>10% glycerol >0.5%1#>3% trehalose.
After 8 hours, each sample moisturizing rate rate of descent is respectively: 13.3%, 24.1%, 21.8%, 14.0%, 12.5%; After 24 hours, each sample moisturizing rate rate of descent is respectively: 65.4%, 30.6%, 30.0%, 21.3%, 17.4%, so can find out, each sample moisturizing rate all declines along with the prolongation of standing time, but the decline degree of different sample is different, if although 10% glycerol is in placement after 8 hours, moisturizing rate decline degree will lower than 2%2#, 5%4#, but place after 24 hours, compositions moisturizing rate decline degree of the present invention slows down, even if illustrate after sample is placed 24 hours, compositions of the present invention still keeps higher moisturizing rate.
For 2%2# compositions, and one pack system 2% hyaluronic acid, utilize digital moisture of skin tester to carry out the mensuration of moisture.Principle: mainly adopt capacitance principle, namely carries out the mensuration of moisture content of skin according to water and the difference of the dielectric constant of other materials.Test environment: 20 DEG C, relative humidity is under the condition of 40%-60%, selects lossless, without chaeta, without cosmetics position.The results are shown in Figure 1.
By using skin moisture tester, before above-mentioned two component tests are used, using the skin moisture value after 1 hour, 3 hours, 8 hours, showing whether compositions of the present invention has long-acting moistening effect by data.
As can be seen from Figure 1, before using 2%2# compositions of the present invention, one pack system 2% hyaluronic acid respectively, scaly dry skin hydropenia, the moistening effect using latter 1 hour is all fine, after use 2%2# compositions one hour, and the moisture value of skin is 75.6; Use latter 3 hours, although skin moisture value declines to some extent, still remain on the state of relatively moistening, the moisture value of latter 8 hours is used to decline slow, well below hyaluronic acid rate of descent, therefore can find out the present composition, moistening effect as long-acting in 2%2# is very significant.
Data show, and use hyaluronic acid after 1 hour, clearly, moisture value is 82.4% to moistening effect, but is just reduced to 42.7% after three hours, has even dropped to 26.7% after eight hours.Reason is likely: be used alone the hyaluronic acid stock solution that concentration is higher, not direct moistening effect, because hyaluronic acid can absorb large quantity of moisture from skin, make skin drier and more astringent after using on the contrary, but concentration is low, do not play long-acting moisture retention effect that the present composition can play as emulsion B data in embodiment 3 yet.
Embodiment 3
Effect by the numerical Evaluation moisture-keeping composition of test skin moisture loss TEWL: utilize German CK company skin moisture loss (TEWL) tester TM300 to measure.
By the latex A that formula (water appropriate, glycerol 5%, cetearyl alcohol acid alcohol 1.6%, glyceryl stearate 0.5%, stereth-250.5%, poly-dimethicone 0.3%, allantoin 0.2%, carbomer 0.1%, Cremophor RH40 0.1%, Methylisothiazolinone is appropriate, iodine alkynol butyl mephenesin Carbamate is appropriate) is prepared, wherein moisturizing ingredient is: glycerol 5%.
By the emulsion B that formula (water appropriate, cetearyl alcohol acid alcohol 1.6%, hyaluronate sodium 0.8%, glyceryl stearate 0.5%, stereth-250.5%, poly-dimethicone 0.3%, allantoin 0.2%, carbomer 0.1%, Cremophor RH40 0.1%, Methylisothiazolinone is appropriate, iodine alkynol butyl mephenesin Carbamate is appropriate) is prepared, wherein moisturizing ingredient is: hyaluronate sodium 0.8%.
By the emulsion C that formula (water appropriate, glycerol 3%, Jojoba seed oil 2%, cetearyl alcohol acid alcohol 1.6%, glyceryl stearate 0.5%, stereth-250.5%, poly-dimethicone 0.3%, allantoin 0.2%, hyaluronate sodium 0.1%, betanin 0.1%, carbomer 0.1%, Cremophor RH40 0.1%, Methylisothiazolinone is appropriate, iodine alkynol butyl mephenesin Carbamate is appropriate) is prepared, wherein moisturizing ingredient is: glycerol 3%, Jojoba seed oil 2%, hyaluronate sodium 0.1%, betanin 0.1%.
By formula (water appropriate, moisture-keeping composition 2%, cetearyl alcohol acid alcohol 1.6%, glyceryl stearate 0.5%, stereth-250.5%, poly-dimethicone 0.3%, allantoin 0.2%, carbomer 0.1%, Cremophor RH40 0.1%) preparation moisturizing emulsion, wherein moisture-keeping composition is respectively with 1#, 2#, 3#, 4# in embodiment, and prepared moisturizing emulsion is numbered D, E, F, G respectively.
Above formula, A, B, C emulsion all needs to add appropriate antiseptic, and D, E, F, G all can ensure its antiseptic effect without the need to adding antiseptic.
Test instrunment: German CK company skin moisture loss (TEWL) tester TM300
Test condition: 1. select healthy volunteer, experimenter is without any dermatopathy, and recipient site skin is without exception;
2. before experiment, experimenter needs with unified gentle cleaning agent cleaning inner forearm face, in constant environment (20-22 DEG C, relative humidity is 40%-60%) sit quietly 30min.At test period, experimenter does not arbitrarily leave test environment, and will keep being emotionally stable; Between age 29-38 year, women.
Test result as shown in Figure 2.Can learn from figure, the emulsion D of natural moisture preserving compositions composition of the present invention, E, F, the numerical value that G scatters and disappears to moisture of skin, will well below single component (A arbitrary than other emulsions, B) the lost numerical value measured by, also lower than the moisture loss numerical value measured by emulsion C, illustrate further natural moisture preserving compositions of the present invention by this figure can be added to and comprise in all products in this area, as cream frost, emulsion, cleansing milk, shampoo, bath gel, handwashing liquid, toothpaste, cosmetic water, facial mask essence, wet tissue series products etc., moisture retention and lasting effect are played to skin.
By measuring the evaporation capacity of TEWL value reflection water from skin surface, after use moisturizer, skin barrier is repaired, and TEWL value reduces, and therefore compositions of the present invention has than conventional moisturizer preferably moistening effect.
Embodiment 4
Anti-(pressing down) bacterium test---moisture-keeping bacterium-restraining ring measures (Odontothrips loti).
With reference to " test of sterile products inspection technology specification 2.1.8.2 bacterial restrain ", American Pharmacopeia USP35-<51>AntimicrobialEffect ivenessTesting, " cosmetics health specification (version in 2007) " " Part IV Micro biological Tests method " in " disinfection technology standard (version in 2002) ".
1. test strain: escherichia coli (Escherichiacoli), staphylococcus aureus (Staphylococcusaureus), bacillus subtilis (Bacillussubtilis), Candida albicans (Candidaalbicans).
2. test specimen: 1#-4# moisture-keeping composition in embodiment 1, working concentration is 2%.
3. the judgement of bacteriostasis: inhibition zone diameter is greater than 7mm person, has been judged to bacteriostasis.Inhibition zone diameter is less than or equal to 7mm person, is judged to without bacteriostasis.3 times repeated trials all has bacteriostasis result person, and it is qualified to be judged to.Experimental result is in table 3.
Table 3. moisture-keeping composition is to the bacterial restrain (mm) of antibacterial and fungus
As can be seen from Table 3, natural moisture preserving compositions of the present invention all has certain inhibitory action to antibacterial, fungus.
Embodiment 5
Moisture-keeping composition Oxidation Resistance Test.
By moisture-keeping composition 4# dissolve with methanol, formulation content is the methanol solution 2mL of 0.5%, 1.0%, 1.5%, 2.0%, 3.0%, 5.0% respectively, add 1 of 0.5mmol/L respectively, bitter diazanyl (DPPH) the methanol solution 2mL of 1-diphenyl-2-, after mixing 15s, placing 30min, take methanol as A reference, survey absorbance in 517nm, be designated as Ar; Draw 2mL methanol and DPPH mixing 15s respectively, placing 30min, take methanol as reference, surveys absorbance, be designated as A in 517nm
0.And calculate clearance rate according to following formula.
In formula: K is DPPH free radical scavenging activity, %.
Can find out in Fig. 3, moisture-keeping composition can reach 62% to the clearance rate of DPPH free radical under 0.5% use amount, and increases along with the increase clearance rate of consumption thereupon.This moisture-keeping composition visible has very strong antioxidation.
Claims (9)
1. the long-acting moisture-keeping composition of natural plants, is characterized in that, described compositions contains: shinyleaf yellowhorn oil, synergetic effect additive and solvent.
2. moisture-keeping composition according to claim 1, is characterized in that, in described compositions, synergetic effect additive is the mixture of at least one in sorbitol, Polyethylene Glycol, 1,2-decanediol, Sensiva SC50.
3. moisture-keeping composition according to claim 1, is characterized in that, in described compositions, solvent is one or both the mixture in water, shinyleaf yellowhorn shell aqueous extract, Lignum Xanthoceratis branch aqueous extract, Lignum Xanthoceratis leaf aqueous extract.
4. moisture-keeping composition according to claim 1, is characterized in that, in described compositions, shinyleaf yellowhorn oil weight percentage is 1.0-40%; Be preferably 5.0-15%.
5., according to the arbitrary described moisture-keeping composition of claim 1 or 2, it is characterized in that, in described compositions, synergetic effect additive weight percentage is 1.0-50%; Be preferably 20-45%.
6., according to the arbitrary described moisture-keeping composition of claim 1 or 3, it is characterized in that, in described compositions, solvent weight percent content is weight of solvent percentage composition is 20-80%, is preferably 40-70%.
7. moisture-keeping composition according to claim 3, is characterized in that,
Described shinyleaf yellowhorn fruit shell aqueous extract is make to be soaked in water the solution of shinyleaf yellowhorn shell gained, preparation method: by 100%, take the shinyleaf yellowhorn shell of 10%-50%, be cut into small pieces or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described shinyleaf yellowhorn shell aqueous extract;
Described Lignum Xanthoceratis branch aqueous extract is make to be soaked in water the solution of Lignum Xanthoceratis branch gained, preparation method: by 100%, take the Lignum Xanthoceratis branch of 10%-50%, be cut into segment or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described Lignum Xanthoceratis branch aqueous extract;
Described Lignum Xanthoceratis leaf aqueous extract is make to be soaked in water the solution of Lignum Xanthoceratis fruit leaf gained, preparation method: by 100%, take the Lignum Xanthoceratis leaf of 10%-50%, be cut into small pieces or clay into power, add in 50%-90% water, under room temperature, soak 1-24 hour, then 40-100 DEG C of heating in water bath about 15 minutes, filter, get supernatant and be described Lignum Xanthoceratis leaf aqueous extract.
8. according to the arbitrary described moisture-keeping composition of claim 1-7 for comprising all products of this area personal care articles or wet tissue, as the purposes of cream frost, emulsion, cleansing milk, shampoo, bath gel, handwashing liquid, toothpaste, cosmetic water, facial mask essence, wet tissue series products.
9. one kind contains personal care articles or the wet tissue of the arbitrary described compositions of claim 1-7.
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| CN107375071A (en) * | 2017-07-29 | 2017-11-24 | 贵州苗源实业有限公司 | A kind of formula and preparation method of Rosa roxburghii stoste facial mask |
| CN107496241A (en) * | 2017-09-07 | 2017-12-22 | 师海全 | A kind of preparation method of the facial mask containing shiny-leaved yellowhorn bioactive ingredients |
| CN107669532A (en) * | 2016-12-12 | 2018-02-09 | 青岛大学 | Suncream |
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| CN112245352A (en) * | 2020-10-30 | 2021-01-22 | 佳尔美(深圳)智能科技有限公司 | Xanthoceras sorbifolia essence and application thereof |
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| CN107496241A (en) * | 2017-09-07 | 2017-12-22 | 师海全 | A kind of preparation method of the facial mask containing shiny-leaved yellowhorn bioactive ingredients |
| CN108852975A (en) * | 2018-08-23 | 2018-11-23 | 璧电健 | Pure natural striae of pregnancy remediation composition |
| CN110101596A (en) * | 2019-06-24 | 2019-08-09 | 北京美科兴业生物科技有限公司 | A kind of preparation method and its usage containing beta glucan complex composition |
| CN112245352A (en) * | 2020-10-30 | 2021-01-22 | 佳尔美(深圳)智能科技有限公司 | Xanthoceras sorbifolia essence and application thereof |
| CN112402788A (en) * | 2020-10-30 | 2021-02-26 | 佳尔美(深圳)智能科技有限公司 | Biological electrical stimulation meridian membrane and stimulation device |
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