CN106833977A - Citral dendrobium candidum perfumed soap and preparation method thereof - Google Patents
Citral dendrobium candidum perfumed soap and preparation method thereof Download PDFInfo
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- CN106833977A CN106833977A CN201611162779.2A CN201611162779A CN106833977A CN 106833977 A CN106833977 A CN 106833977A CN 201611162779 A CN201611162779 A CN 201611162779A CN 106833977 A CN106833977 A CN 106833977A
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- dendrobium candidum
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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Abstract
The invention discloses citral dendrobium candidum perfumed soap and preparation method thereof, belong to daily and wash shield product scope.The perfumed soap is prepared by the raw material of following weight portion：5~10 parts of 35~50 parts of soap base, 20~40 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract and litsea citrate oil.Citral dendrobium candidum perfumed soap of the invention, possesses the citris aromas of natural extract citral and the intrinsic smell of dendrobium candidum, and the multiple effects such as wrinkle are gone in the low stimulation of pro-skin, foam stabilization, good antibacterial dirt-removing power, and whitening.
Description
Technical field
The present invention relates to a kind of perfumed soap, more particularly to a kind of citral dendrobium candidum perfumed soap and preparation method thereof belongs to day
With washing shield product scope.
Background technology
Perfumed soap is traditional washing product that each family commonly uses, and with the raising of quality of life, people are to perfumed soap
Requirement also more and more higher, most of bacteriostatic agents of presently commercially available perfumed soap using chemical reagent such as triclocarbans, long-term use
Risk also have to be assessed, and vdiverse in function, natural, safe perfumed soap is also progressively favored by masses.
The citral extracted from natural plants, with strong citrus scented, it possesses obvious antimycotic effect；
The bletilla striata possesses astringing to arrest bleeding, and the effect of detumescence and promoting granulation, its extract is also more protruded the resist drying damage effect of human body skin；
Dendrobium candidum also has certain Study On The Radioprotective to the fibrocyte of people's normal skin, and its polysaccharide, mucilaginous substance for being rich in
Deng composition to going the aspects such as wrinkle, delaying skin aging also to have certain effect；Occur perfumed soap function on the market more single, and antibacterial
Agent is generally chemical synthesis material, and citral dendrobium candidum perfumed soap is reached using the natural citral for extracting, the bletilla striata and dendrobium candidum
Non-stimulated to skin, effective antimycotic and wrinkle removal whitening effect is arrived.
The content of the invention
First technical problem to be solved by this invention is to provide a kind of citral dendrobium candidum perfumed soap, and the perfumed soap is utilized
Active ingredient in the citral and bletilla striata extract, the dendrobium candidum extract solution that are extracted from natural plants, reaches low to skin
Stimulation, the effectively multiple effect such as antimycotic and wrinkle removal whitening.
The citral dendrobium candidum perfumed soap, is prepared by the raw material of following weight portion：35~50 parts of soap base, iron sheet stone
20~40 parts of dry measure used in former times extract solution, 10~20 parts of bletilla striata extract, 5~10 parts of litsea citrate oil.
Preferably, above-mentioned citral dendrobium candidum perfumed soap, is prepared by the raw material of following weight portion：Soap base 35~45
Part, 20~30 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract, 5~10 parts of litsea citrate oil.
Second technical problem to be solved by this invention is to provide the preparation method of above-mentioned citral dendrobium candidum perfumed soap,
The preparation method is comprised the following steps：
The preparation of (a) soap base liquid：35~50 parts of soap base is taken, 85~90 DEG C is heated to and is completely dissolved to soap base；
The preparation of (b) soap lye：20~40 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract are added in above-mentioned soap base
In liquid, fully mix, 20~30min is heated at 65~70 DEG C, add 5~10 parts of litsea citrate oil, after being well mixed rapidly
To soap lye；
C () is into soap：Above-mentioned soap lye is poured into mould while hot, after being cooled to room temperature, soap is frozen into.
Wherein, in preparation method step (a) of above-mentioned citral dendrobium candidum perfumed soap, the mode of the heating adds for water-bath
Heat or heating using microwave.
Wherein, in preparation method step (b) of above-mentioned citral dendrobium candidum perfumed soap, the dendrobium candidum extract solution by with
Lower section method is obtained：
(1) in dendrobium candidum powder being added into extractor, to the pure water that 6~20 times of powder weight is added in extractor,
The pH value of liquid in extractor is adjusted to 4.5~5.5 under stirring condition；Powder is accounted under stirring condition to addition in extractor again
The cellulase of 0.8~2.0wt% and the pectase of 0.5~1.2wt%, are heated to 45~60 DEG C, after 3~4h of insulation, continue
90~100 DEG C are heated to, 15~30min is incubated, 300 mesh nylon cloths are crossed, the dregs of a decoction and first time filtrate is obtained；
(2) to the pure water for continuing 5~10 times of addition powder weight in the above-mentioned dregs of a decoction, 45~60 are heated under stirring condition
DEG C, after 0.8~1.2h of insulation, continue to be heated to 90~100 DEG C, 15~30min is incubated, 300 mesh nylon cloths are crossed, obtain second
Filtrate；
(3) merge first time filtrate and second filtrate, after standing 8~12h, take supernatant plate and frame filter press and squeezed
Filter, collects filtrate；
(4) the above-mentioned filtrate being collected into is placed in vacuum concentration pot, is 55~75 DEG C, -0.07~-0.08MPa in temperature
Vacuum condition under, concentrate the filtrate to the magma that relative density is 1.10~1.15, obtain dendrobium candidum extract solution.
Wherein, in preparation method step (b) of above-mentioned citral dendrobium candidum perfumed soap, the bletilla striata extract is by following
Method is obtained：
(1) by bletilla striata powder add refluxing extraction tank in, under stirring condition in refluxing extraction tank add bletilla striata powder weight
The pure water of 10~12 times of amount, is heated to 85~95 DEG C of 1.5~2h of refluxing extraction, crosses 300 mesh nylon cloths, obtains first time filtrate
And the dregs of a decoction；
(2) to the pure water that 5~8 times of bletilla striata powder weight is added in the above-mentioned dregs of a decoction, 85~95 DEG C of refluxing extractions 1 are heated to
~1.5h, crosses 300 mesh nylon cloths, obtains second filtrate；
(3) merge first time filtrate and second filtrate is placed in vacuum concentration pot, be 55~75 DEG C, -0.07 in temperature
Under the vacuum condition of~-0.08MPa, the magma that relative density is 1.10~1.15 is concentrated the filtrate to, obtain bletilla striata extract.
Wherein, in preparation method step (c) of above-mentioned citral dendrobium candidum perfumed soap, the actual conditions of the freezing is：
Temperature is -22~-18 DEG C, freezes 20~26h.
The beneficial effects of the invention are as follows：The citral dendrobium candidum perfumed soap that the present invention is provided, possesses natural extract lemon
The intrinsic smell of the citris aromas of aldehyde and the bletilla striata and dendrobium candidum, the perfumed soap possesses the low stimulation of pro-skin, foam stabilization, good
Antibacterial dirt-removing power and whitening go wrinkle etc. multiple effect.
Specific embodiment
The invention provides a kind of citral dendrobium candidum perfumed soap, the perfumed soap utilizes the lemon extracted from natural plants
Active ingredient in aldehyde and bletilla striata extract, dendrobium candidum extract solution, reaches to the low stimulation of skin, effectively antimycotic and wrinkle removal whitening
Etc. multiple effect.The citral dendrobium candidum perfumed soap, is prepared by the raw material of following weight portion：35~50 parts of soap base, iron
5~10 parts of 20~40 parts of skin dendrobium extract, 10~20 parts of bletilla striata extract and litsea citrate oil.
Preferably, above-mentioned citral dendrobium candidum perfumed soap, is prepared by the raw material of following weight portion：Soap base 35~45
Part, 20~30 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract, 5~10 parts of litsea citrate oil.
Further, present invention also offers the preparation method of above-mentioned citral dendrobium candidum perfumed soap, the preparation method bag
Include following steps：
The preparation of (a) soap base liquid：35~50 parts of soap base is taken, 85~90 DEG C is heated to and is completely dissolved to soap base；
The preparation of (b) soap lye：20~40 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract are added in above-mentioned soap base
In liquid, fully mix, 20~30min is heated at 65~70 DEG C, add 5~10 parts of litsea citrate oil, after being well mixed rapidly
To soap lye；
C () is into soap：Above-mentioned soap lye is poured into mould while hot, after being cooled to room temperature, soap is frozen into；The freezing it is specific
Condition is：Temperature is -22~-18 DEG C, freezes 20~26h.
Wherein, in preparation method step (a) of above-mentioned citral dendrobium candidum perfumed soap, the mode of the heating adds for water-bath
Heat or heating using microwave.
Wherein, in above-mentioned citral dendrobium candidum perfumed soap and preparation method thereof, the dendrobium candidum extract solution is by with lower section
Method is obtained：
(1) in dendrobium candidum powder being added into extractor, to the pure water that 6~20 times of powder weight is added in extractor,
The pH value of liquid in extractor is adjusted to 4.5~5.5 under stirring condition；Powder is accounted under stirring condition to addition in extractor again
The cellulase of 0.8~2.0wt% and the pectase of 0.5~1.2wt%, are heated to 45~60 DEG C, after 3~4h of insulation, continue
90~100 DEG C are heated to, 15~30min is incubated, 300 mesh nylon cloths are crossed, the dregs of a decoction and first time filtrate is obtained；
(2) to the pure water for continuing 5~10 times of addition powder weight in the above-mentioned dregs of a decoction, 45~60 are heated under stirring condition
DEG C, after 0.8~1.2h of insulation, continue to be heated to 90~100 DEG C, 15~30min is incubated, 300 mesh nylon cloths are crossed, obtain second
Filtrate；
(3) merge first time filtrate and second filtrate, after standing 8~12h, take supernatant plate and frame filter press and squeezed
Filter, collects filtrate；
(4) the above-mentioned filtrate being collected into is placed in vacuum concentration pot, is 55~75 DEG C, -0.07~-0.08MPa in temperature
Vacuum condition under, concentrate the filtrate to the magma that relative density is 1.10~1.15, obtain dendrobium candidum extract solution.
Wherein, in above-mentioned citral dendrobium candidum perfumed soap and preparation method thereof, the bletilla striata extract is by following methods system
：
(1) by bletilla striata powder add refluxing extraction tank in, under stirring condition in refluxing extraction tank add bletilla striata powder weight
The pure water of 10~12 times of amount, is heated to 85~95 DEG C of 1.5~2h of refluxing extraction, crosses 300 mesh nylon cloths, obtains first time filtrate
And the dregs of a decoction；
(2) to the pure water that 5~8 times of bletilla striata powder weight is added in the above-mentioned dregs of a decoction, 85~95 DEG C of refluxing extractions 1 are heated to
~1.5h, crosses 300 mesh nylon cloths, obtains second filtrate；
(3) merge first time filtrate and second filtrate is placed in vacuum concentration pot, be 55~75 DEG C, -0.07 in temperature
Under the vacuum condition of~-0.08MPa, the magma that relative density is 1.10~1.15 is concentrated the filtrate to, obtain bletilla striata extract.
Wherein, in preparation method step (b) of above-mentioned citral dendrobium candidum perfumed soap, litsea citrate oil in the raw material components
Can be obtained by commercially available, such as the litsea citrate oil of the natural medicinal oil Co., Ltd production of Jiangxi deodar；The litsea citrate oil also may be used
To be made by the steps：Fruit of a cubeb litsea tree fruit after crushing is placed in steamer, plus 0.8~1.2 times of fruit weight is pure
Water, opens steam generator and condensate collection device, during keep having the pure water of 0.8~1.2 times of fruit weight in steamer,
After extracting 2~3h, the grease in condensation collection liquid is separated, obtain final product litsea citrate oil.
Each material component act as in the present invention：Citral, citral tool are extracted from natural plants litsea citrate oil
There is strong citrus scented, it possesses obvious antimycotic effect；The bletilla striata possesses astringing to arrest bleeding, the effect of detumescence and promoting granulation, and it is carried
Thing is taken also more to protrude the resist drying damage effect of human body skin；Dendrobium candidum also has one to the fibrocyte of people's normal skin
Fixed Study On The Radioprotective, and the composition such as its polysaccharide, the mucilaginous substance that are rich in is to going the aspects such as wrinkle, delaying skin aging also to have one
It is set for using.With suitable proportioning be combined with each other above-mentioned component and be prepared into perfumed soap so that the perfumed soap by inventor through test of many times
Possess the low stimulation of pro-skin, foam stabilization, good antibacterial dirt-removing power and whitening and go the multiple effects such as wrinkle.
The present invention is made further explanation and description with reference to embodiments, embodiment is used merely to explain the present invention, and
Protection scope of the present invention is not intended to be limited to following examples, and the those of ordinary skill of the technical field is according to the present invention
Disclosure, be capable of achieving the purpose of the present invention.
Embodiment 1
Citral dendrobium candidum perfumed soap is prepared by following methods：
The preparation of (a) soap base liquid：Take 50 parts of soap base, heating water bath is to 85 DEG C to being completely dissolved；
The preparation of (b) soap lye：Add 20 parts of dendrobium candidum extract solution, 20 parts of bletilla striata extract in above-mentioned soap base liquid, fill
Divide and mix, 30min is heated at 65 DEG C, then add 10 parts of litsea citrate oil, be well mixed, be made soap lye；
C () is into soap：Well mixed soap lye is poured into mould while hot, after being cooled to room temperature, is placed in cold in -20 DEG C of refrigerators
Freeze 24h into soap, perfumed soap can be packaged into after taking-up.
Embodiment 2
Citral dendrobium candidum perfumed soap is prepared by following methods：
The preparation of (a) soap base liquid：Take 45 parts of soap base, heating using microwave is to 90 DEG C to being completely dissolved；
The preparation of (b) soap lye：Add 30 parts of dendrobium candidum extract solution, 20 parts of bletilla striata extract in above-mentioned soap base liquid, fill
Divide and mix, 20min is heated at 70 DEG C, then add 5 parts of litsea citrate oil, be well mixed, be made soap lye.
C () is into soap：Well mixed soap lye is poured into mould while hot, after being cooled to room temperature, is placed in cold in -20 DEG C of refrigerators
Freeze 24h into soap, perfumed soap can be packaged into after taking-up.
Embodiment 3
Citral dendrobium candidum perfumed soap is prepared by following methods：
The preparation of (a) soap base liquid：Take 35 parts of soap base, water-bath or heating using microwave are to 85 DEG C -90 DEG C to being completely dissolved.
The preparation of (b) soap lye：Add 40 parts of dendrobium candidum extract solution, 15 parts of bletilla striata extract in above-mentioned soap base liquid, fill
Divide and mix, 30min is heated at 65 DEG C, then add 10 parts of litsea citrate oil, be well mixed, be made soap lye.
C () is into soap：Well mixed soap lye is poured into mould while hot, after being cooled to room temperature, is placed in cold in -20 DEG C of refrigerators
Freeze 24h into soap, perfumed soap can be packaged into after taking-up.
Wherein, in above-described embodiment 1~3, dendrobium candidum extract solution is obtained by following methods：
(1) by dendrobium candidum powder addition extractor, to the pure water that 12 times of powder weight is added in extractor, stir
Under the conditions of add appropriate NaOH or hydrochloric acid, the pH value of liquid in extractor is adjusted to 5.0；Again to extractor under stirring condition
Middle addition accounts for the pectase of the cellulase and 0.7wt% of powder 1.0wt%, is heated to 52 DEG C, after insulation 3.5h, continues to heat
To 95 DEG C, 20min is incubated, crosses 300 mesh nylon cloths, obtain the dregs of a decoction and first time filtrate；
(2) to the pure water for continuing 7 times of addition powder weight in the above-mentioned dregs of a decoction, 52 DEG C, insulation are heated under stirring condition
After 1.0h, continue to be heated to 95 DEG C, be incubated 20min, cross 300 mesh nylon cloths, obtain second filtrate；
(3) merge first time filtrate and second filtrate, after standing 10h, take supernatant plate and frame filter press squeeze and filter,
Collect filtrate；
(4) the above-mentioned filtrate being collected into is placed in vacuum concentration pot, is 65 DEG C in temperature, -0.07~-0.08MPa's is true
Under empty condition, the magma that relative density is 1.12 is concentrated the filtrate to, obtain dendrobium candidum extract solution.
Wherein, in above-described embodiment 1~3, bletilla striata extract is obtained by following methods：
(1) by bletilla striata powder add refluxing extraction tank in, under stirring condition in refluxing extraction tank add bletilla striata powder weight
The pure water of 12 times of amount, is heated to 90 DEG C of refluxing extraction 2h, crosses 300 mesh nylon cloths, obtains first time filtrate and the dregs of a decoction；
(2) to the pure water that 7 times of bletilla striata powder weight is added in the above-mentioned dregs of a decoction, 90 DEG C of refluxing extraction 1.5h, mistake are heated to
300 mesh nylon cloths, obtain second filtrate；
(3) merge first time filtrate and second filtrate to be placed in vacuum concentration pot, be 60 DEG C in temperature, -0.07~-
Under the vacuum condition of 0.08MPa, the magma that relative density is 1.15 is concentrated the filtrate to, obtain bletilla striata extract.
Claims (7)
1. citral dendrobium candidum perfumed soap, it is characterised in that the perfumed soap is prepared by the raw material of following weight portion：Soap base 35
~50 parts, 20~40 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract, 5~10 parts of litsea citrate oil.
2. citral dendrobium candidum perfumed soap according to claim 1, it is characterised in that the perfumed soap by following weight portion original
Material is prepared：35~45 parts of soap base, 20~30 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract, litsea citrate oil 5~
10 parts.
3. the preparation method of citral dendrobium candidum perfumed soap described in claim 1 or 2, it is characterised in that the preparation method includes
Following steps：
The preparation of (a) soap base liquid：35~50 parts of soap base is taken, 85~90 DEG C is heated to and is completely dissolved to soap base；
The preparation of (b) soap lye：20~40 parts of dendrobium candidum extract solution, 10~20 parts of bletilla striata extract are added in above-mentioned soap base liquid
In, fully mix, 20~30min is heated at 65~70 DEG C, 5~10 parts of litsea citrate oil is added, obtained after being well mixed rapidly
Soap lye；
C () is into soap：Above-mentioned soap lye is poured into mould while hot, after being cooled to room temperature, soap is frozen into.
4. the preparation method of citral dendrobium candidum perfumed soap according to claim 3, it is characterised in that described in step (a)
The mode of heating is heating water bath or heating using microwave.
5. according to claim 3 or 4 citral dendrobium candidum perfumed soap preparation method, it is characterised in that in step (b),
The dendrobium candidum extract solution is obtained by following methods：
(1) by dendrobium candidum powder addition extractor, to the pure water that 6~20 times of powder weight is added in extractor, stir
Under the conditions of the pH value of liquid in extractor is adjusted to 4.5~5.5；Under stirring condition again in extractor add account for powder 0.8~
The cellulase of 2.0wt% and the pectase of 0.5~1.2wt%, are heated to 45~60 DEG C, after 3~4h of insulation, continue to be heated to
90~100 DEG C, 15~30min is incubated, crosses 300 mesh nylon cloths, obtain the dregs of a decoction and first time filtrate；
(2) to the pure water for continuing 5~10 times of addition powder weight in the above-mentioned dregs of a decoction, 45~60 DEG C are heated under stirring condition,
After 0.8~1.2h of insulation, continue to be heated to 90~100 DEG C, be incubated 15~30min, cross 300 mesh nylon cloths, obtain second filter
Liquid；
(3) merge first time filtrate and second filtrate, after standing 8~12h, take supernatant plate and frame filter press squeeze and filter,
Collect filtrate；
(4) the above-mentioned filtrate being collected into is placed in vacuum concentration pot, is 55~75 DEG C in temperature, -0.07~-0.08MPa's is true
Under empty condition, the magma that relative density is 1.10~1.15 is concentrated the filtrate to, obtain dendrobium candidum extract solution.
6. the preparation method of citral dendrobium candidum perfumed soap according to claim 5, it is characterised in that described in step (b)
Bletilla striata extract is obtained by following methods：
(1) in bletilla striata powder being added into refluxing extraction tank, to adding bletilla striata powder weight 10 in refluxing extraction tank under stirring condition
~12 times of pure water, is heated to 85~95 DEG C of 1.5~2h of refluxing extraction, crosses 300 mesh nylon cloths, obtains first time filtrate and medicine
Slag；
(2) to the pure water that 5~8 times of bletilla striata powder weight is added in the above-mentioned dregs of a decoction, be heated to 85~95 DEG C of refluxing extractions 1~
1.5h, crosses 300 mesh nylon cloths, obtains second filtrate；
(3) merge first time filtrate and second filtrate to be placed in vacuum concentration pot, be 55~75 DEG C in temperature, -0.07~-
Under the vacuum condition of 0.08MPa, the magma that relative density is 1.10~1.15 is concentrated the filtrate to, obtain bletilla striata extract.
7. the preparation method of citral dendrobium candidum perfumed soap according to claim 3, it is characterised in that described in step (c)
The actual conditions of freezing is：Temperature is -22~-18 DEG C, freezes 20~26h.
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| CN201611162779.2A CN106833977A (en) | 2016-12-15 | 2016-12-15 | Citral dendrobium candidum perfumed soap and preparation method thereof |
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| CN201611162779.2A CN106833977A (en) | 2016-12-15 | 2016-12-15 | Citral dendrobium candidum perfumed soap and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103536462A (en) * | 2012-07-12 | 2014-01-29 | 上海家化联合股份有限公司 | Preparation method and application of bletilla striata extract |
| CN105077051A (en) * | 2015-04-16 | 2015-11-25 | 闽南师范大学 | Functional food containing Dendrobium officinale and longan and preparation method thereof |
| CN105112181A (en) * | 2015-09-16 | 2015-12-02 | 中华全国供销合作总社南京野生植物综合利用研究所 | Functional plant essential oil handmade soap and preparation method thereof |
| CN105199862A (en) * | 2014-06-26 | 2015-12-30 | 应丽红 | Formula of detergent mixed with surfactant |
| CN105861196A (en) * | 2016-04-11 | 2016-08-17 | 赵加棚 | Purely natural dendrobe bletilla striata handmade soap and preparation method thereof |
-
2016
- 2016-12-15 CN CN201611162779.2A patent/CN106833977A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103536462A (en) * | 2012-07-12 | 2014-01-29 | 上海家化联合股份有限公司 | Preparation method and application of bletilla striata extract |
| CN105199862A (en) * | 2014-06-26 | 2015-12-30 | 应丽红 | Formula of detergent mixed with surfactant |
| CN105077051A (en) * | 2015-04-16 | 2015-11-25 | 闽南师范大学 | Functional food containing Dendrobium officinale and longan and preparation method thereof |
| CN105112181A (en) * | 2015-09-16 | 2015-12-02 | 中华全国供销合作总社南京野生植物综合利用研究所 | Functional plant essential oil handmade soap and preparation method thereof |
| CN105861196A (en) * | 2016-04-11 | 2016-08-17 | 赵加棚 | Purely natural dendrobe bletilla striata handmade soap and preparation method thereof |
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