CN109260056A - A kind of mosquito-proof sting bath foam of infant's draft and preparation method thereof - Google Patents

Abstract

The embodiment of the invention discloses mosquito-proof sting bath foams of a kind of infant's draft and preparation method thereof.The ingredient of the mosquito-proof sting bath foam of draft includes water, moisturizer, antioxidant, pH adjusting agent, surfactant etc.；It is succinct to contain a variety of natural plants such as Folium Artemisiae Argyi extract, spiceleaf day blue certain herbaceous plants with big flowers essential oil, oil of Cymbopogon winterianus.This product it is clean, safe, no added (without essence, non-pigment, preservative free, without hormone), shield product mild formulation design is washed using infant, irritation is reduced while each ingredient collocation enhancing effect, enhance the external barrier function of infant's skin, effectively solve the problem of that summer baby's hidrosis attracts bite by mosquitos.

Description

A kind of mosquito-proof sting bath foam of infant's draft and preparation method thereof

Technical field

The present invention relates to washing product technical fields, and in particular to a kind of mosquito-proof sting bath foam of infant's draft and its Preparation method.

Background technique

Infant distributes that heat is more, and respiratory rate is very fast, and fever is easily perspired, lactic acid and ammonium class chemical combination in infant's sweat The ingredients such as object have extremely strong attraction to mosquito.In addition infant bears a pretty, delicate skin, and subcutaneous lipid is few, same to compare vulnerable to stimulation Adult more causes mosquito, redness, blister is easy to appear after bite by mosquitos, and be difficult to heal.

It is single or functional component effect is not strong to wash shield product efficacy ingredient for existing shower on the market, not anti-for infant Effective product of bite by mosquitos.

Summary of the invention

The embodiment of the present invention is designed to provide a kind of mosquito-proof sting bath foam of infant's draft, is that pre- child-resistant is outstanding It is easy in summer by bite by mosquitos, and this product uses in nature a variety of potent natural plants essences progress compound to enhance product Protection effect.This product uses natural composite vegetables extractive, non-stimulated to human body, and there is mosquito to know special smell, except clear Clean skin is moistened outside skin, additionally it is possible to be effectively prevent biting for mosquito, be takeed good care of the delicate skin of baby.The embodiment of the present invention also provides The preparation method of the mosquito-proof sting bath foam of infant's draft.

To achieve the above object, the embodiment of the present invention provides a kind of mosquito-proof sting bath foam of infant's draft, the baby The mosquito-proof sting bath foam of child's draft includes herbal ingredients mixture, the herbal ingredients mixture include Folium Artemisiae Argyi extract, The blue certain herbaceous plants with big flowers essential oil of spiceleaf day and oil of Cymbopogon winterianus.

Further, the mosquito-proof sting bath foam of infant's draft includes water, moisturizer, antioxidant, pH adjusting Agent, surfactant and the herbal ingredients mixture；By weight percentage, folium artemisiae argyi is extracted in the herbal ingredients mixture Content of the object in the bath foam is 0.1-0.5%, and content of the blue certain herbaceous plants with big flowers essential oil of spiceleaf day in the bath foam is 0.01- 0.05%, content of the oil of Cymbopogon winterianus in the bath foam is 0.01-0.05%.

Folium artemisiae argyi is the dried leaf of compositae plant Chinese mugwort (Artemisia argyi Levl.et Vant.).It is more in south China See.Picking when summer flower is not opened removes impurity, dries.It is folium artemisiae argyi bitter, pungent, it is warm-natured.Liver,spleen,kidney is returned to pass through.It is bitter dry pungent scattered, Energy rationale blood warm meridians, expels cold-dampness, stops crymodynia；External application removing dampness to stop itchin.Folium Artemisiae Argyi extract is brown powder product, with drying Folium artemisiae argyi medicinal material be raw material, contain volatile oil component, flavones ingredient, triterpenes components, have mosquito repellent, antibacterial, inhibit allergy The release of medium, antianaphylactic effect.Wet sore scabies, removing dampness to stop itchin can be controlled, and has inhibition to a variety of viruses and bacterium and kills Wound effect, and have certain preventive and therapeutic effect to respiratory disease.

The blue certain herbaceous plants with big flowers (Pelargonium graveolens L'Herit.) of spiceleaf day, is perennial herb or shrub shape, spiceleaf Fish pelargonium because plant have volatile aroma due to it is very popular, can be used for making essential oil.Rose pelargonium essential oil is by more than 30 kinds Terpenoid and its derivative are formed, and main component is spiceleaf grass alcohol (geraniol), citronellol (citronellol), linalool (linalool), citronellyl formate (citronellyl first), formic acid spiceleaf grass ester (spiceleaf first) and menthones (peppermint) etc..It can Balance skin secretion, to eczema, burn, shingles zoster and pernio it is beneficial.Pale debility skin uses rose pelargonium essential oil It is ruddy and vibrant afterwards.Rose pelargonium essential oil can also alleviate body and mind, can calm down the impatient and dejected of mood, take away undesirable Mood, relieving psychological pressure allow entire people more to loosen, and the lymphatic system of energy body, toxin expelling, strengthen immunity.

Lemongrass (Cymbopogon citratus.) alias Bao Mao is perennial herb.Because naturally containing citrus scented, therefore again Referred to as lemon grass (Cymbopogon citratus).It is rather good to treat rheumatism effect, and migraine can be treated, it is anti-infective, improve digestive function, mosquito is driven away in deodorization Son, flea reduce the bacterium in ward.Oil of Cymbopogon winterianus is extracted from nardgrass plant, with dry grass distillation and , taste is the synthesis of fruit perfume and lavender.Its anthelminthic effect is significant, and has broad-spectrum antiseptic and bactericidal effect, and has straight Connect the effect for inhibiting influenza virus.Can be anti-infective, Cress improves greasy unclean skin.Freshness is assigned, body and mind is restored Balance (especially sick stage just more).It is the essential oil that purposes is most wide in aromatotherapy and medical method.Lemongrass and flores aurantii, fingered citron It, can be with softening skin after mandarin orange reconciles.

Further, the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic acid monoesters disodium, cocounut oil acyl Aminocarbonyl propyl glycine betaine, lauryl sulfosuccinic acid monoester disodium and laurel alcohol ether phosphate potassium, by weight percentage, fat Content of the alcohol polyoxyethylene ether sulfosuccinic acid monoester disodium in the bath foam is 3%~10%, preferably 8%-10%；Coconut palm Content of the oleamidopropyl betaine in the bath foam is 6%~10%, preferably 8%~10%；Lauryl sulfonation amber Content of the amber acid monoester disodium in the bath foam is 10%~15%, preferably 10%~12%；Laurel alcohol ether phosphate potassium Content in the bath foam is 3%~12%, preferably 6%~10%.

Further, the moisturizer includes pyrrolidone sodium carboxylate, and by weight percentage, pyrrolidone sodium carboxylate exists Content in the bath foam is 0.3%-1%.The embodiment of the present invention uses pyrrolidone sodium carboxylate as the main of moisturizer Ingredient is one of substance in skin, has the characteristics of physiological activity, moisture retention, good hygroscopicity because it is natural moisturizing factor.

Further, the moisturizer further includes glycerol, 1,3-BDO and sorbierite, by weight percentage, glycerol Content in the bath foam is 5%~12%, preferably 8%~10%；Content of the 1,3 butylene glycol in the bath foam It is 0.5%~1%；Content of the sorbierite in the bath foam is 0.5%~1%.

Further, the pH adjusting agent includes citric acid, and by weight percentage, citric acid is in the bath foam Content is 0.1~0.5%.

Further, the antioxidant includes parahydroxyacet-ophenone, and by weight percentage, parahydroxyacet-ophenone is in institute Stating the content in bath foam is 0.5%~1%.

Further, the mosquito-proof sting bath foam of infant's draft further includes foaming agent.In one embodiment, The foaming agent can be Dodecyl Polyoxyethylene Ether ammonium sulfate, and by weight percentage, Dodecyl Polyoxyethylene Ether sulfuric acid Content of the ammonium in the bath foam is 3-8%.

Further, the mosquito-proof sting bath foam of infant's draft further includes thickener.In one embodiment, The thickener can be Arabic gum, and by weight percentage, content of the Arabic gum in the bath foam is 0.1%-0.2%.

The other side of the embodiment of the present invention additionally provides the preparation of the mosquito-proof sting bath foam of infant's draft Method, the method includes the following steps:

(1) precise raw material, while equipment holding cleaning according to the proportion；

(2) water, part of the surface activating agent and foaming agent are stirred dissolution under the conditions of 75 DEG C, are then added remaining Surfactant and part moisturizer, stirring be heated to 85 DEG C, keep 30min；

(3) mixture of step (2) is cooled to 45 DEG C, Folium Artemisiae Argyi extract is added, is stirred evenly；

(4) remaining moisturizer and the blue certain herbaceous plants with big flowers essential oil of spiceleaf day and oil of Cymbopogon winterianus are added in the mixture of step (3), It stirs evenly；

(5) thickener stirred evenly is added in the mixture of step (4), is stirred evenly；

(6) antioxidant is added in said mixture, is stirred evenly；

(7) citric acid is added in the mixture of step (6), 30min is sufficiently stirred；

(8) through after the assay was approved, semi-finished product discharging stores.

Further, step (4) at least stirs 30min, such as 30-40min.

In one embodiment, the part of the surface activating agent being firstly added in step (2) is fatty alcohol polyoxy second Alkene ether sulfosuccinic acid monoester disodium and cocamidopropyl betaine.

In one embodiment, the part moisturizer being added in step (2) is pyrrolidone sodium carboxylate.

The embodiment of the present invention has the advantages that

1, this formula functional component can reach mosquito proof effect, and each adding ingredient and content proportion in few dosage By carefully studying and effect test, compatibility synergy are good；

2, specifically, blue certain herbaceous plants with big flowers (Mozzie buster) essential oil of spiceleaf day has the function of that balance skin is secreted, to eczema, burn, Shingles zoster and pernio are beneficial；Oil of Cymbopogon winterianus has light fruit fragrant and the overall flavor of lavender, can pure and fresh brains, make skin Skin softening, cleaning Oily and sweat mixed with dirt；Folium Artemisiae Argyi extract contains volatile oil component, flavones ingredient, triterpenes components, energy Enough mosquito repellents, antibacterial, the release for inhibiting Anaphylactic mediator, antiallergy；

3, easy to use, daily shower uses this product to use as bath foam when cleaning can reach ideal mosquito repellent effect Fruit, smell is pleasant, pleasant pure and fresh.

Specific embodiment

Embodiments of the present invention are illustrated by particular specific embodiment below, those skilled in the art can be by this explanation Content disclosed by book is understood other advantages and efficacy of the present invention easily.

It should be clear that structure shown in this specification, ratio, size etc., only to cooperate the revealed content of specification, with Understand for those skilled in the art and read, be not intended to limit the invention enforceable qualifications, therefore does not have technically Essential meaning, the modification of any structure, the change of proportionate relationship or the adjustment of size can be generated not influencing the present invention Under effect and the purpose that can reach, should all still it fall in the range of disclosed technology contents obtain and can cover.Meanwhile The term on cited such as "upper", "lower", " left side ", the right side in this specification ", " centre " is merely convenient to being illustrated for narration, and It is non-that to limit the scope of the invention, relativeness is altered or modified, under the content of no substantial changes in technology, when Also it is considered as the enforceable scope of the present invention.

Embodiment 1

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 10%, cocamidopropyl betaine 8%, lauryl sulfosuccinic acid monoester disodium 12%, lauryl alcohol Phosphate potassium 7%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 10%, 1,3 butylene glycol 1%, sorbierite 1%；It is anti- Oxidant includes parahydroxyacet-ophenone 0.5%；PH adjusting agent includes citric acid 0.1%；Herbal ingredients mixture includes that folium artemisiae argyi mentions Take object 0.1%, the blue certain herbaceous plants with big flowers essential oil 0.01% of spiceleaf day, oil of Cymbopogon winterianus 0.01%；Thickener includes Arabic gum 0.1%；Foaming agent Including Dodecyl Polyoxyethylene Ether ammonium sulfate 5%；Remaining is water.

Preparation method includes the following steps:

(1) precise raw material, while equipment holding cleaning according to the proportion；

(2) by water, fatty alcohol polyoxyethylene ether sulfosuccinic acid monoesters disodium and cocamidopropyl betaine and Foaming agent is stirred dissolution under the conditions of 75 DEG C, and lauryl sulfosuccinic acid monoester disodium and lauryl alcohol phosphoric acid is then added Ester potassium, pyrrolidone sodium carboxylate, stirring are heated to 85 DEG C, keep 30min；

(3) mixture of step (2) is cooled to 45 DEG C, Folium Artemisiae Argyi extract is added, is stirred evenly；

(4) step (3) are added in glycerol, 1,3-BDO and sorbierite and the blue certain herbaceous plants with big flowers essential oil of spiceleaf day and oil of Cymbopogon winterianus Mixture in, stir 35min, stir evenly；

(5) thickener stirred evenly is added in the mixture of step (4), is stirred evenly；

(6) antioxidant is added in said mixture, is stirred evenly；

(7) citric acid is added in the mixture of step (6), 30min is sufficiently stirred；

(8) through after the assay was approved, semi-finished product discharging stores.

Following embodiment and comparative example, relative to embodiment 1, in addition to not adding the ingredient lacked, preparation method is the same as real Apply example 1.

Embodiment 2

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 9%, cocamidopropyl betaine 10%, lauryl sulfosuccinic acid monoester disodium 10%, lauryl alcohol Phosphate potassium 9%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 10%, 1,3 butylene glycol 1%, sorbierite 1%；It is anti- Oxidant includes parahydroxyacet-ophenone 0.8%；PH adjusting agent includes citric acid 0.1%；Herbal ingredients mixture includes that folium artemisiae argyi mentions Take object 0.1%, the blue certain herbaceous plants with big flowers essential oil 0.01% of spiceleaf day, oil of Cymbopogon winterianus 0.01%；Thickener includes Arabic gum 0.2%；Foaming agent Including Dodecyl Polyoxyethylene Ether ammonium sulfate 5%；Remaining is water.

Embodiment 3

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 8%, cocamidopropyl betaine 8%, lauryl sulfosuccinic acid monoester disodium 12%, lauryl alcohol phosphorus Acid esters potassium 5%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 8%, 1,3 butylene glycol 1%, sorbierite 1%；Antioxygen Agent includes parahydroxyacet-ophenone 0.8%；PH adjusting agent includes citric acid 0.1%；Herbal ingredients mixture includes folium artemisiae argyi extraction Object 0.1%, the blue certain herbaceous plants with big flowers essential oil 0.01% of spiceleaf day, oil of Cymbopogon winterianus 0.01%；Thickener includes Arabic gum 0.2%；Foaming agent packet Include Dodecyl Polyoxyethylene Ether ammonium sulfate 5%；Remaining is water.

Embodiment 4

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 8%, cocamidopropyl betaine 10%, lauryl sulfosuccinic acid monoester disodium 10%, lauryl alcohol Phosphate potassium 11%；Moisturizer includes pyrrolidone sodium carboxylate 0.4%, glycerol 12%, 1,3 butylene glycol 0.8%, sorbierite 0.6%；Antioxidant includes parahydroxyacet-ophenone 0.6%；PH adjusting agent includes citric acid 0.4%；Herbal ingredients mixture packet Include Folium Artemisiae Argyi extract 0.5%, the blue certain herbaceous plants with big flowers essential oil 0.05% of spiceleaf day, oil of Cymbopogon winterianus 0.01%；Thickener includes Arabic gum 0.15%；Foaming agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 6%；Remaining is water.

Embodiment 5

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 8%, cocamidopropyl betaine 7%, lauryl sulfosuccinic acid monoester disodium 13%, lauryl alcohol phosphorus Acid esters potassium 7%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 9%, 1,3 butylene glycol 0.6%, sorbierite 0.8%； Antioxidant includes parahydroxyacet-ophenone 0.8%；PH adjusting agent includes citric acid 0.2%；Herbal ingredients mixture includes folium artemisiae argyi Extract 0.1%, the blue certain herbaceous plants with big flowers essential oil 0.01% of spiceleaf day, oil of Cymbopogon winterianus 0.05%；Thickener includes Arabic gum 0.15%；Foaming Agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 7%；Remaining is water.

Embodiment 6

The mosquito-proof sting bath foam of infant's draft described in the present embodiment includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 10%, cocamidopropyl betaine 6%, lauryl sulfosuccinic acid monoester disodium 14%, lauryl alcohol Phosphate potassium 3%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 6%, 1,3 butylene glycol 0.8%, sorbierite 0.8%；Antioxidant includes parahydroxyacet-ophenone 1%；PH adjusting agent includes citric acid 0.3%；Herbal ingredients mixture includes Folium Artemisiae Argyi extract 0.2%, the blue certain herbaceous plants with big flowers essential oil 0.02% of spiceleaf day, oil of Cymbopogon winterianus 0.04%；Thickener includes Arabic gum 0.15%； Foaming agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 4%；Remaining is water.

Comparative example 1

The mosquito-proof sting bath foam of infant's draft described in this comparative example includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant include cocamidopropyl betaine 8%, Lauryl sulfosuccinic acid monoester disodium 13%, laurel alcohol ether phosphate potassium 15%；Moisturizer includes pyrrolidone sodium carboxylate 0.3%, glycerol 8%, 1,3 butylene glycol 1.5%；PH adjusting agent includes citric acid 0.4%；Herbal ingredients mixture includes folium artemisiae argyi Extract 0.3%, the blue certain herbaceous plants with big flowers essential oil 0.03% of spiceleaf day, oil of Cymbopogon winterianus 0.03%；Thickener includes Arabic gum 0.2%；Foaming Agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 3%；Remaining is water.

Comparative example 2

The mosquito-proof sting bath foam of infant's draft described in this comparative example includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 7%, lauryl sulfosuccinic acid monoester disodium 8%, laurel alcohol ether phosphate potassium 8%；Moisturizer includes pyrroles Alkanone carboxylic acid sodium 0.3%, glycerol 15%, sorbierite 0.8%；Antioxidant includes parahydroxyacet-ophenone 0.6%；Herbal ingredients are mixed Closing object includes Folium Artemisiae Argyi extract 0.3%, the blue certain herbaceous plants with big flowers essential oil 0.03% of spiceleaf day, oil of Cymbopogon winterianus 0.03%；Thickener includes Arab Glue 0.1%；Foaming agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 8%；Remaining is water.

Comparative example 3

The mosquito-proof sting bath foam of infant's draft described in this comparative example includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 15%, cocamidopropyl betaine 8%, laurel alcohol ether phosphate potassium 8%；Moisturizer includes pyrrolidones Carboxylic acid sodium 0.3%, 1,3 butylene glycol 0.8%, sorbierite 0.2%；PH adjusting agent includes citric acid 0.3%；Herbal ingredients mixing Object includes Folium Artemisiae Argyi extract 0.3%, the blue certain herbaceous plants with big flowers essential oil 0.03% of spiceleaf day, oil of Cymbopogon winterianus 0.03%；Thickener includes Arabic gum 0.2%；Foaming agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 6%；Remaining is water.

Comparative example 4

The mosquito-proof sting bath foam of infant's draft described in this comparative example includes following component (base by weight percentage In the mosquito-proof sting bath foam of infant's draft): the surfactant includes fatty alcohol polyoxyethylene ether sulfosuccinic Acid monoester disodium 15%, cocamidopropyl betaine 12%, lauryl sulfosuccinic acid monoester disodium 6%；Moisturizer packet Include glycerol 3%, 1,3 butylene glycol 0.8%, sorbierite 0.6%；Antioxidant includes parahydroxyacet-ophenone 0.8%；Herbal ingredients Mixture includes Folium Artemisiae Argyi extract 0.3%, the blue certain herbaceous plants with big flowers essential oil 0.03% of spiceleaf day, oil of Cymbopogon winterianus 0.03%；Thickener includes for I Primary glue 0.1%；Foaming agent includes Dodecyl Polyoxyethylene Ether ammonium sulfate 5%；Remaining is water.

Detect test result

1,5g sample is respectively taken to the above embodiments 1-6 and comparative example 1-4 product obtained, according to Q/ASMRH17-2017 " infant's shampoo used also as bath lotion " standard requirements and GB/T13531.1-2008 (dilution method), GB/T 29679-2013 standard, The detection in terms of organoleptic indicator and physical and chemical index is carried out, judgment basis is as follows:

Appearance (Q/ASMRH17-2017): transparent, translucent or emulsion liquid；

Color (Q/ASMRH17-2017): meet regulation color；

Fragrance (Q/ASMRH17-2017): meet regulation fragrance；

PH value (GB/T 13531.1-2008): 4.0-8.5；

Effective substance % (GB/T 29679-2013): >=8%；

Heat-resisting (Q/ASMRH17-2017): (40 ± 1) DEG C/for 24 hours, restore room temperature without layering, metachromatism；

Cold-resistant (Q/ASMRH17-2017): -5 DEG C~-10 DEG C/for 24 hours, restore room temperature without layering, metachromatism.

As a result it see the table below.

1 organoleptic indicator of table and physical and chemical index testing result

It can be seen from Table 1 that the sample in embodiment 1-6 all meets every organoleptic indicator and physical and chemical index detection mark Standard, wherein embodiment 1-3 has better appearance and color relative to embodiment 4-6, and substance content is also higher；And And embodiment 1 has best appearance and color, is colorless and transparent thick liquid, and have high substance content.

In contrast, the sample in comparative example 1-4, appearance and color are not satisfactory, and substance content is declined； In addition, there is different degrees of layering and/or discoloration in heat-resisting and cold-resistant detection in this four samples.

Furthermore the sample in embodiment 1-6, relative to the sample in comparative example 1-4, pH value is distributed in relatively narrow range It is interior, be conducive to product control；And the sample pH fluctuation in comparative example 1-4 is larger.

All test samples all meet fragrance examination criteria.

2, acute skin thorn is carried out to 1 sample of embodiment according to Ministry of Public Health's " cosmetics safety technical specification " (version in 2015) Swash property test.

2.1 tested materials: colorless and transparent thick liquid, when experiment as former state.

2.2 experimental animals: 4 adults, healthy, skin zero damage regular grade new zealand rabbit are selected, by Guangdong Province's medicine Experimental Animal Center (three water basely) provides [animal productiong licensing number: SCXK (Guangdong) 2014-0035, Quality of Experimental Animals conjunction Lattice card number: 44411600004414], feed is supplied by collaboration medical bioengineering Co., Ltd of Jiangsu Province.

2.3 feeding managements: in regular grade animal house, (experimental animal uses credit number: SYXK (Guangdong) for new zealand rabbit raising 2016-0110), single cage is raised, free water feed, laboratory temperature: 16-26 DEG C, relative humidity: 40-70%RH.

2.4 contamination methods: regular grade new zealand rabbit 4, half male and half female.About 24 hours before test, by experimental animal back Backbone two sides coat is cut, and epidermis, the left and right each about 3cm × 3cm of unhairing range can not be damaged.Tested material about 0.5ml is taken to be applied to It on the left of animal on skin, is then covered with two layers of gauze (2.5cm × 2.5cm) and one layer of glassine paper, then with nonirritant adhesive plaster It is fixed with bandage.Other side skin is as control.The application time is 2h, and it is tested to remove residual with pure water after the test Object.

2.5 observation operations: position dermoreaction is smeared in 1,24, the 48 and 72h observation after eliminating tested material, by " makeup Product technical specification of security " (version in 2015) skin irritation/corrosion test table 1 " skin wound repair scoring " carry out skin it is anti- It should score, overall merit is carried out with the average value of animal subject integral.According to 24,48, that 72h respectively observes time point top is equal Value presses " cosmetics safety technical specification " (version in 2015) skin irritation/corrosion test table 2 " skin irritatin strength grading " Determine skin irritatin intensity.The observation time limit is usually no more than 14d.

2.6 test results:

Tested new zealand rabbit skin does not occur skin wound repair within the observation period, and 24,48 and 72h respectively observes time point most High integral mean value is 0 point.It is pierced according to Ministry of Health of the People's Republic of China " cosmetics safety technical specification " (version in 2015) skin Swash property/corrosion test standard judgement, baby's shampoo used also as bath lotion acute skin irritation intensity provided in an embodiment of the present invention is nothing Irritation.It the results are shown in Table 2.

2 tested material of table is to new zealand rabbit acute skin irritation test result

Conclusion: tested material is nonirritant to new zealand rabbit acute skin irritation.

3, acute Eye irritation is carried out to 1 sample of embodiment according to Ministry of Public Health's " cosmetics safety technical specification " (version in 2015) Property test (30s flushing).

3.1 tested materials: colorless and transparent thick liquid, when experiment as former state.

3.2 experimental animals: 3 adult regular grade new zealand rabbits are selected, (three is water base by Guangdong Medical Lab Animal Center Ground) provide [animal productiong licensing number: SCXK (Guangdong) 2014-0035, Quality of Experimental Animals quality certification number: 44411600004414], feed is by the supply of collaboration medical bioengineering Co., Ltd of Jiangsu Province.

3.3 feeding managements: in regular grade animal house, (experimental animal uses credit number: SYXK (Guangdong) for new zealand rabbit raising 2016-0110), single cage is raised, free water feed, laboratory temperature: 16-26 DEG C, relative humidity: 40-70%RH.

Interior eyes inspection for 24 hours before 3.4 tests: with the hands thumb and index finger gently pull open the palpebra inferior of new zealand rabbit eyes, The fluorescein sodium dilution 2 for instilling 2% to animal conjunctiva capsule drips, and so that upper and lower eyelid is passively closed about 1s prevents medical fluid from flowing out, so After unclamp both hands, give free rein to be closed.The fluorescein sodium to animal eyes is slowly rinsed with enough pure water after 30s to rinse Until clean, observed after 1 hour, have no that irritation, corneal defect and conjunctival damage, 3 new zealand rabbits occur in animal eyes It is completely used for testing.

3.5 contamination methods: with the hands thumb and index finger gently pull open the palpebra inferior of eyes on the right side of new zealand rabbit, by 0.1mL/ Only tested material is directly painted into the conjunctival sac of new zealand rabbit eyes, so that upper and lower eyelid is passively closed about 1s prevents its outflow, until It is very fast with enough, flow velocity but the water flow of animal eye injury will not be caused to rinse 30s when 30s.Left side eyes do not handle work certainly Body control.2% fluorescein sodium dilution is instilled after observation for 24 hours, is cleaned up after 30s.

3.6 clinical examinations and scoring: after being painted into tested material 1h, for 24 hours, 48h, 72h and 4d and 7d be to animal eyes Eyeball is checked.It, can termination test if 72h does not occur stimulate the reaction.If it find that involving cornea or having other Eye irritations Effect, recuperator to determine that invertibity or the irreversibility of the damage need to extend observing time is not usually no more than 21d in 7d, And provide the visual report of 7d, 14d, 21d.In addition to observing cornea, iris, conjunctiva, other detrimental effects should should all When recording and report.It should all be by " cosmetics safety technical specification " (version in 2015) acute eye irritation/corruption in each check Corrosion tests the integral of table 1 " standards of grading of eye damage " record Eye irritation reaction.

3.7 evaluation of result: with to animal corneal after tested material, iris or conjunctiva it is each it is comfortable for 24 hours, 48h or 72h observe time point Stimulate the reaction top and recovery time evaluation, press " cosmetics safety technical specification " (version in 2015) acute Eye irritation Property/corrosion test table 3 " eye irritation reaction classification " determines tested material to the stimulus intensity of eye.

3.8 test result

The right eye of 3 tested new zealand rabbits does not occur irritative response within the observation period.Left eye (control eye) is without any Irritation occurs." cosmetics safety technical specification " (version in 2015) acute eye irritation table 3 " eye irritation reaction classification " Grade scale determine, infant's shampoo used also as bath lotion acute ocular stimulus intensity (30s flushings) provided in an embodiment of the present invention be nothing Irritation.Appraisal result is shown in Table 3.

3 tested material of table is to new zealand rabbit acute ocular irritation test appraisal result

Experiment condition: 30s is rinsed

Conclusion: tested material is nonirritant to the acute eye irritation of new zealand rabbit (30s flushing).

Infant's shampoo used also as bath lotion obtained of the embodiment of the present invention is isolated foreign matter and skin using oil components, is strengthened Barrier forms natural protective film；It is non-stimulated to human body using natural composite vegetables extractive, and with the special of mosquito identification Smell, except cleaning skin is moistened in addition to skin, additionally it is possible to effectively prevent biting for mosquito, take good care of the delicate skin of baby；Daily shower Using this product to use when cleaning as bath foam can reach ideal repelling effect, and smell is pleasant, pleasant pure and fresh.

Although above having used general explanation and specific embodiment, the present invention is described in detail, at this On the basis of invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Therefore, These modifications or improvements without departing from theon the basis of the spirit of the present invention are fallen within the scope of the claimed invention.

Claims (10)

1. a kind of mosquito-proof sting bath foam of infant's draft, which is characterized in that the mosquito-proof sting of infant's draft is taken a shower Liquid includes herbal ingredients mixture, and the herbal ingredients mixture includes Folium Artemisiae Argyi extract, the blue certain herbaceous plants with big flowers essential oil of spiceleaf day and lemongrass essence Oil.

2. the mosquito-proof sting bath foam of infant's draft according to claim 1, which is characterized in that infant's draft Mosquito-proof sting bath foam includes water, moisturizer, antioxidant, pH adjusting agent, surfactant and herbal ingredients mixing Object；By weight percentage, content of the Folium Artemisiae Argyi extract in the bath foam is 0.1- in the herbal ingredients mixture 0.5%, content of the blue certain herbaceous plants with big flowers essential oil of spiceleaf day in the bath foam is 0.01-0.05%, and oil of Cymbopogon winterianus is in the bath foam Content be 0.01-0.05%.

3. the mosquito-proof sting bath foam of infant's draft according to claim 2, which is characterized in that the surfactant Including fatty alcohol polyoxyethylene ether sulfosuccinic acid monoesters disodium, cocamidopropyl betaine, lauryl sulfosuccinate Monoesters disodium and laurel alcohol ether phosphate potassium, by weight percentage, fatty alcohol polyoxyethylene ether sulfosuccinic acid monoesters disodium Content in the bath foam is 3%~10%；Content of the cocamidopropyl betaine in the bath foam is 6% ~10%；Content of the lauryl sulfosuccinic acid monoester disodium in the bath foam is 10%~15%；Lauryl alcohol phosphoric acid Content of the ester potassium in the bath foam is 3%~12%.

4. the mosquito-proof sting bath foam of infant's draft according to claim 3, which is characterized in that the moisturizer includes Pyrrolidone sodium carboxylate, glycerol, 1,3-BDO and sorbierite, by weight percentage, pyrrolidone sodium carboxylate are washed one's hair described Content in bath foam is 0.3%-1%, and content of the glycerol in the bath foam is 5%~12%, and 1,3-BDO is described Content in bath foam is 0.5%~1%, and content of the sorbierite in the bath foam is 0.5%~1%.

5. the mosquito-proof sting bath foam of infant's draft according to claim 4, which is characterized in that the pH adjusting agent packet Citric acid is included, by weight percentage, content of the citric acid in the bath foam is 0.1~0.5%.

6. the mosquito-proof sting bath foam of infant's draft according to claim 5, which is characterized in that the antioxidant packet Parahydroxyacet-ophenone is included, by weight percentage, content of the parahydroxyacet-ophenone in the bath foam is 0.5%~1%.

7. the mosquito-proof sting bath foam of infant's draft according to claim 6, which is characterized in that infant's draft Mosquito-proof sting bath foam further includes foaming agent Dodecyl Polyoxyethylene Ether ammonium sulfate, and by weight percentage, and lauryl alcohol is poly- Content of the ethylene oxide ether ammonium sulfate in the bath foam is 3-8%.

8. the mosquito-proof sting bath foam of infant's draft according to claim 7, which is characterized in that infant's draft Mosquito-proof sting bath foam further includes thickener Arabic gum, and by weight percentage, Arabic gum is in the bath foam Content be 0.1%-0.2%.

9. the preparation method of the mosquito-proof sting bath foam of infant's draft according to claim 8, which is characterized in that described Method includes the following steps:

(1) precise raw material, while equipment holding cleaning according to the proportion；

(2) water, part of the surface activating agent and foaming agent are stirred dissolution under the conditions of 75 DEG C, remaining table is then added Face activating agent and part moisturizer, stirring are heated to 85 DEG C, keep 30min；

(3) mixture of step (2) is cooled to 45 DEG C, Folium Artemisiae Argyi extract is added, is stirred evenly；

(4) remaining moisturizer and the blue certain herbaceous plants with big flowers essential oil of spiceleaf day and oil of Cymbopogon winterianus are added in the mixture of step (3), stirring Uniformly；

(5) thickener stirred evenly is added in the mixture of step (4), is stirred evenly；

(6) antioxidant is added in said mixture, is stirred evenly；

(7) citric acid is added in the mixture of step (6), 30min is sufficiently stirred；

(8) through after the assay was approved, semi-finished product discharging stores.

10. preparation method according to claim 9, which is characterized in that step (4) at least stirs 30min.