CN103519003B - A kind of silicone hydroxyl apatite that utilizes is as the polynary feed of carrier and manufacture method thereof - Google Patents
A kind of silicone hydroxyl apatite that utilizes is as the polynary feed of carrier and manufacture method thereof Download PDFInfo
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- CN103519003B CN103519003B CN201310447781.4A CN201310447781A CN103519003B CN 103519003 B CN103519003 B CN 103519003B CN 201310447781 A CN201310447781 A CN 201310447781A CN 103519003 B CN103519003 B CN 103519003B
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Abstract
Disclosed by the invention be a kind of silicone hydroxyl apatite that utilizes as the polynary feed of carrier and manufacture method thereof, feedstuff consists of mass fraction and is respectively: Fish protein active peptides 20-40 part, sunflower meal 75-90 part, soybean lecithin 55-70 part, soda ash 30-45 part, citric acid 25-45 part, wheat bran, fish meal, mineral matter 25-45 part, vitamin 2-10 part, nano controlled-release carrier 20-25 part etc.; Manufacture method step: (1) soybean lecithin, soda ash, citric acid mixing, and is stirred into puff; (2) wheat bran, fish meal, mineral matter, vitamin are pulverized and is uniformly mixed into basal feed; (3) Fish protein active peptides, sunflower meal are uniformly mixed into auxiliary feed; (4) puff, basal feed, auxiliary feed are fully uniformly mixed; (5) mixture is placed in comminutor, through granulation, drying.The present invention nurses one's health aquatic product animal immune function comprehensively and throwing can be floated after supporting gradually, is convenient to observe the pollution reduced water body.
Description
technical field:
the present invention relates to a kind of aquaculture feed and manufacture method thereof, be specifically related to a kind of silicone hydroxyl apatite that utilizes as the polynary feed of carrier and manufacture method thereof, belong to culture fishery.
background technology:
along with the development of culture fishery in recent years, the demand of aquaculture feed is also increasing.The aquatic feeds of current culture fishery mainly contains heavy property feed and two kinds, buoyancy feed.
particle meeting sedimentation after throwing is supported of heavy property feed, makes aquatic biological ingest smoothly.But heavy property feed in use easy losss of scattering in water, and after feed granules sedimentation, user cannot observe the situation of ingesting of aquatic biological, thus its have that feed nutrient easily scatters and disappears, easy polluted-water and cannot the shortcoming such as normal observation.
buoyancy feed is then that feed granules can float up to the water surface after throwing is supported, and aquatic biological is all ingested at approximately level place, and user well can observe the situation of ingesting of aquatic products, and amount is supported in the throwing effectively controlling feed.But due to feed throwing support after namely float up to the water surface, aquatic biological must be ingested in superjacent waters, and centering, lower floor's aquatic biological, be then unfavorable for that it is ingested and adds physical consumption.Therefore, current aquaculture feed is badly in need of improving further.
in addition, active peptides uses the equilibrium can strengthened amino acid and other nutrient to absorb in culture fishery, significantly improve the utilization rate of aquatic product to mineral matter elements such as calcium, iron, magnesium, zinc, promote the rehabilitation of aquatic product trophism, improve immunity of organisms, improve production performance, aquatic product seedling percent is significantly improved.And, sunflower meal is the accessory substance after the Northwest extracts sunflower oil, its aboundresources, cheap, containing rich in protein, general between 30-40%, particularly wherein containing unrighted acids such as a certain amount of linoleic acid, and these unrighted acids to be animals self can not synthesize, harmful effect may be produced to each cell in body and organ during shortage, growth rate reduction, Feed efficiency minimizing and seedling percent reduction etc. can be produced.
summary of the invention:
the present invention seeks to, be used for making up the deficiencies in the prior art, and provide one can nurse one's health aquatic product animal immune function comprehensively, increase seedling percent and pest-resistant sterilization composite multi-component feed and manufacture method thereof.
to achieve these goals, technical scheme of the present invention is as follows:
the present invention's pest-resistant sterilization composite multi-component feed, raw material composition content is respectively by mass fraction:
fish protein active peptides 20-40 part, sunflower meal 75-90 part, soybean lecithin 55-70 part, soda ash 30-45 part, citric acid 25-45 part, wheat bran 40-128 part, fish meal 10-85 part, mineral matter 25-45 part, vitamin 2-10 part, Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, nano controlled-release carrier 20-25 part,
the preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
above-mentioned mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
said vitamin is the mixture of vitamin A, vitamin B2, vitamin B6, vitamin B12, vitamin D and vitamin E.
the manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, wheat bran, fish meal, mineral matter, vitamin are pulverized and is uniformly mixed into basal feed;
(3) according to proportioning described in claim 1, Fish protein active peptides, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) the auxiliary feed that the basal feed that puff step (1) obtained, (2) obtain, (3) obtain, nano controlled-release carrier are fully uniformly mixed;
(5) mixture obtained in step (4) is placed in comminutor, obtains pest-resistant sterilization composite multi-component feed through granulation, drying;
wherein, the manufacture method of Fish protein active peptides is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated Fish protein is added pancreatin, the weight of described pancreatin is the 2-3% of Fish protein raw material weight, and its enzymolysis time is 3-3.5 hour, and its hydrolysis temperature is 30-45 DEG C;
(C) carried out after step (B) going out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
beneficial effect of the present invention is as follows:
the present invention adds Fish protein active peptides in aquaculture feed, the equilibrium of animal to amino acid and other nutrient can be strengthened absorb, significantly improve the utilization rate of animal to mineral matter elements such as calcium, iron, magnesium, zinc, promote Animal nutrition Sex Rehabilitation, improve immunity of organisms, improve production performance, animal seedling percent is significantly improved, the present invention also adds the abundant sunflower oil accessory substance sunflower meal of raw material resources in aquaculture feed, owing to containing rich in protein in sunflower meal, especially containing unrighted acid-linoleic acid that animal itself can not be synthesized, can avoid because of unsaturated fat acid heat or metabolic disorder time, to the harmful effect that body cell and organ produce, the phenomenon that growth of animal rate reduces and seedling percent reduces can be prevented, the present invention with the addition of puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin then forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, namely particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and wrapped up by oil layer outside feed granules, thus feed granules can not scatter in water, be convenient to ingesting of aquatic products, it also avoid feed nutrient scattering and disappearing in water, and decrease the pollution of feed granules to water body.With the addition of the Chinese herbal medicine with the sick function of anti parasitic in feed, the parasite disease that can fundamentally prevent and treat, through actual verification, the present invention can reduce the generation of parasite disease and reduce the quantity infecting parasitic disease; There is the Chinese herbal medicine particle of bactericidal effect, by fermentation, the effect of various composition fully played, be applied to that water body is rapid-action, action time is lasting, environmental protection and there is bactericidal effect; In addition, the present invention fills a prescription rationally, and preparation method is simple.
detailed description of the invention:
the technological means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with concrete enforcement, setting forth the present invention further.
embodiment one:
pest-resistant sterilization composite multi-component feed of the present invention, raw material composition content is respectively by mass fraction:
fish protein active peptides 20 parts, sunflower meal 75 parts, soybean lecithin 55 parts, soda ash 30 parts, citric acid 25 parts, 40 parts, wheat bran, fish meal 10 parts, 25 parts, mineral matter, vitamin 2 parts, Pinus massoniana 5 parts, China tree 12 parts, 20 parts, garlic, pumpkin 16 parts, Chinese tallowtree leaf 6 parts, fragrant eupatorium herb 10 parts, Eupatorium adenophorum 10 parts, guayule rubber 10 parts, kuh-seng 10 parts, 15 parts, Chinese gall, 20 parts, nano controlled-release carrier;
the preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
wherein, mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
wherein, vitamin is the mixture of vitamin A, vitamin B2, vitamin B6, vitamin B12, vitamin D and vitamin E.
the manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, wheat bran, fish meal, mineral matter, vitamin are pulverized and is uniformly mixed into basal feed;
(3) according to proportioning described in claim 1, Fish protein active peptides, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) the auxiliary feed that the basal feed that puff step (1) obtained, (2) obtain, (3) obtain, nano controlled-release carrier are fully uniformly mixed;
(5) mixture obtained in step (4) is placed in comminutor, obtains pest-resistant sterilization composite multi-component feed through granulation, drying;
wherein, the manufacture method of Fish protein active peptides is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated Fish protein is added pancreatin, the weight of described pancreatin is 2% of Fish protein raw material weight, and its enzymolysis time is 3 hours, and its hydrolysis temperature is 30 DEG C;
(C) carried out after step (B) going out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
the present invention adds Fish protein active peptides in aquaculture feed, the equilibrium of animal to amino acid and other nutrient can be strengthened absorb, significantly improve the utilization rate of animal to mineral matter elements such as calcium, iron, magnesium, zinc, promote Animal nutrition Sex Rehabilitation, improve immunity of organisms, improve production performance, animal seedling percent is significantly improved.
the present invention also adds the abundant sunflower oil accessory substance sunflower meal of raw material resources in aquaculture feed, owing to containing rich in protein in sunflower meal, especially containing unrighted acid-linoleic acid that animal itself can not be synthesized, can avoid because of unsaturated fat acid heat or metabolic disorder time, to the harmful effect that body cell and organ produce, the phenomenon that growth of animal rate reduces and seedling percent reduces can be prevented.
the present invention with the addition of puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin then forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, namely particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and wrapped up by oil layer outside feed granules, thus feed granules can not scatter in water, be convenient to ingesting of aquatic products, it also avoid feed nutrient scattering and disappearing in water, and decrease the pollution of feed granules to water body.
embodiment two:
pest-resistant sterilization composite multi-component feed of the present invention, raw material consists of Fish protein active peptides, sunflower meal, soybean lecithin, soda ash, citric acid, wheat bran, fish meal, mineral matter, vitamin;
each constituent content is respectively by mass fraction:
fish protein active peptides 40 parts, sunflower meal 90 parts, soybean lecithin 70 parts, soda ash 45 parts, citric acid 45 parts, 128 parts, wheat bran, fish meal 85 parts, 45 parts, mineral matter, vitamin 10 parts, Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, 25 parts, nano controlled-release carrier;
the preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
wherein, mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
wherein, vitamin is the mixture of vitamin A, vitamin B2, vitamin B6, vitamin B12, vitamin D and vitamin E.
the manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, wheat bran, fish meal, mineral matter, vitamin are pulverized and is uniformly mixed into basal feed;
(3) according to proportioning described in claim 1, Fish protein active peptides, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) the auxiliary feed that the basal feed that puff step (1) obtained, (2) obtain, (3) obtain, nano controlled-release carrier are fully uniformly mixed;
(5) mixture obtained in step (4) is placed in comminutor, obtains pest-resistant sterilization composite multi-component feed through granulation, drying;
wherein, the manufacture method of Fish protein active peptides is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated Fish protein is added pancreatin, the weight of described pancreatin is 3% of Fish protein raw material weight, and its enzymolysis time is 3.5 hours, and its hydrolysis temperature is 45 DEG C;
(C) carried out after step (B) going out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
more than show and describe general principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (3)
1. utilize silicone hydroxyl apatite as a polynary feed for carrier, it is characterized in that, raw material composition content is respectively by mass fraction:
Fish protein active peptides 20-40 part, sunflower meal 75-90 part, soybean lecithin 55-70 part, soda ash 30-45 part, citric acid 25-45 part, wheat bran 40-128 part, fish meal 10-85 part, mineral matter 25-45 part, vitamin 2-10 part, Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, nano controlled-release carrier 20-25 part,
The preparation method of described nano controlled-release carrier is:
(A) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(B) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition; To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound;
(C) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir 60 minutes with mechanical agitator 1200r/min, obtain nano controlled-release carrier;
Described polynary feed is prepared by following manufacture method, comprises following step:
(1) according to described proportioning, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to described proportioning, wheat bran, fish meal, mineral matter, vitamin are pulverized and is uniformly mixed into basal feed;
(3) according to described proportioning, Fish protein active peptides, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall are uniformly mixed into auxiliary feed;
(4) the auxiliary feed that the basal feed that puff step (1) obtained, step (2) obtain, step (3) obtain, nano controlled-release carrier are fully uniformly mixed;
(5) mixture obtained in step (4) is placed in comminutor, obtains polynary feed through granulation, drying.
2. polynary feed according to claim 1, is characterized in that,
Described mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
3. polynary feed according to claim 1, it is characterized in that, described vitamin is the mixture of vitamin A, vitamin B2, vitamin B6, vitamin B12, vitamin D and vitamin E.
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