CN103519003A - Multi-element feed taking silicon hydroxyl apatite as carrier and preparation method thereof - Google Patents
Multi-element feed taking silicon hydroxyl apatite as carrier and preparation method thereof Download PDFInfo
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Abstract
The invention discloses multi-element feed taking silicon hydroxyl apatite as a carrier and a preparation method thereof. The feed comprises the following raw materials in parts by mass: 20 to 40 parts of fish protein active polypeptide, 75 to 90 parts of sunflower seed meal, 55 to 70 parts of soybean phospholipid, 30 to 45 parts of soda powder, 25 to 45 parts of citric acid, bran, fish meal, 25 to 45 parts of mineral substance, 2 to 10 parts of vitamin, 20 to 25 parts of nanometer sustained release carrier and the like. The preparation method comprises the following steps: (1) mixing the soybean phospholipid, the soda powder and the citric acid and stirring uniformly to obtain a puffed material; (2) crushing and uniformly mixing the bran, the fish meal, the mineral substance and the vitamin to obtain base feed; (3) uniformly mixing the fish protein active polypeptide and the sunflower seed meal to obtain auxiliary feed; (4) completely stirring and mixing the puffed material, the base feed and the auxiliary feed; and (5) placing the mixture into a pelletizer, pelletizing and drying. The feed can comprehensively regulate the immune function of aquatic animals, can be floated gradually after being used, is convenient to observe and reduces pollution to water.
Description
technical field:
The present invention relates to a kind of aquaculture feed and manufacture method thereof, be specifically related to a kind of silicon hydroxyapatite that utilizes as polynary feed and the manufacture method thereof of carrier, belong to culture fishery.
background technology:
Along with the development of culture fishery in recent years, the demand of aquaculture feed is also increasing.The aquatic feeds that at present culture fishery is used mainly contains two kinds, heavy forage and buoyancy feed.
The particle of heavy forage is meeting sedimentation after throwing is supported, and aquatic biological can be ingested smoothly.Losss but heavy forage in use easily scatters in water, and the situation of ingesting that after feed granules sedimentation, user cannot observe aquatic biological, thereby it exists that feed nutrient easily scatters and disappears, easy polluted-water and the shortcoming such as cannot normally observe.
Buoyancy feed is that feed granules can float up to the water surface after throwing is supported, and aquatic biological is all ingested at nearly water surface place, and user can well observe the situation of ingesting of aquatic products, effectively controls foster the measuring of throwing of feed.But because feed floats up to the water surface after throw supporting, aquatic biological must be ingested in superjacent waters, and centering, lower floor's aquatic biological, be unfavorable for that it ingests and increased physical consumption.Therefore, current aquaculture feed is badly in need of further improving.
In addition, active peptides is used in culture fishery can strengthen the equilibrium of amino acid and other nutrient to absorb, significantly improve the utilization rate of aquatic product to mineral matter elements such as calcium, iron, magnesium, zinc, promote the rehabilitation of aquatic product trophism, improve immunity of organisms, improve production performance, aquatic product seedling percent is obviously improved.And, sunflower meal is that the Northwest extracts the accessory substance after sunflower oil, its aboundresources, cheap, contain rich in protein, generally, between 30-40%, particularly wherein contain the unrighted acids such as a certain amount of linoleic acid, and these unrighted acids are animals self, can not synthesize, during shortage, may produce harmful effect to each cell in body and organ, can produce growth rate reduction, the minimizing of bait efficiency and seedling percent reduction etc.
summary of the invention:
The present invention seeks to, be used for making up the deficiencies in the prior art, and provide a kind of, can nurse one's health aquatic product animal immune function, increase seedling percent and pest-resistant sterilization composite multi-component feed and manufacture method thereof comprehensively.
To achieve these goals, technical scheme of the present invention is as follows:
The pest-resistant sterilization composite multi-component of the present invention feed, raw material forms content and is respectively by mass fraction:
Fish protein active polypeptide 20-40 part, sunflower meal 75-90 part, soybean lecithin 55-70 part, soda ash 30-45 part, citric acid 25-45 part, wheat bran 40-128 part, fish meal 10-85 part, mineral matter 25-45 part, vitamin 2-10 part, Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, nano controlled-release carrier 20-25 part,
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
Above-mentioned mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
Said vitamin is the mixture of vitamin A, vitamin B2, pyridoxamine, cobalamin, vitamin D and vitamin E.
The manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, basal feed is pulverized and be uniformly mixed into wheat bran, fish meal, mineral matter, vitamin;
(3) according to proportioning described in claim 1, fish protein active polypeptide, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) auxiliary feed, nano controlled-release carrier that the basal feed that puff step (1) being obtained, (2) obtain, (3) obtain are fully uniformly mixed;
(5) mixture making in step (4) is placed in comminutor, through granulation, dry obtain pest-resistant sterilization composite multi-component feed;
Wherein, the manufacture method of fish protein active polypeptide is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated fish albumen is added to pancreatin, the weight of described pancreatin is the 2-3% of fish protein raw materials weight, and its enzymolysis time is 3-3.5 hour, and its hydrolysis temperature is 30-45 ℃;
(C) after step (B), go out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
Beneficial effect of the present invention is as follows:
The present invention adds fish protein active polypeptide in aquaculture feed, can strengthen animal absorbs the equilibrium of amino acid and other nutrient, significantly improve the utilization rate of animal to mineral matter elements such as calcium, iron, magnesium, zinc, promote animal nutritional rehabilitation, improve immunity of organisms, improve production performance, animal seedling percent is obviously improved, the present invention also adds the sunflower oil accessory substance sunflower meal that raw material resources are abundant in aquaculture feed, owing to containing rich in protein in sunflower meal, especially contain unrighted acid-linoleic acid that animal itself can not be synthetic, can avoid that acid heat or during metabolic disorder because of unsaturated fat, harmful effect to body cell and organ generation, can prevent the phenomenon that growth of animal rate reduces and seedling percent reduces, the present invention has added puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and by oil layer, wrap up outside feed granules, thereby feed granules can not scatter in water, be convenient to ingesting of aquatic products, also avoided feed nutrient scattering and disappearing in water, and reduced the pollution of feed granules to water body.In feed, added the Chinese herbal medicine with the sick function of anti parasitic, the parasite disease that can fundamentally prevent and treat, through actual verification, the present invention can reduce the generation of parasite disease and reduce the quantity that infects parasitic disease; The Chinese herbal medicine particle with bactericidal effect, by fermentation, is fully played the effect of various compositions, is applied to that water body is rapid-action, action time is lasting, environmental protection and have bactericidal effect; In addition, the present invention fills a prescription rationally, and preparation method is simple.
the specific embodiment:
for technological means, creation characteristic that the present invention is realized, reach object and effect is easy to understand, below in conjunction with concrete enforcement, further set forth the present invention.
Embodiment mono-:
Pest-resistant sterilization composite multi-component feed of the present invention, raw material forms content and is respectively by mass fraction:
20 parts of fish protein active polypeptides, 75 parts of sunflower meals, 55 parts of soybean lecithins, 30 parts of soda ash, 25 parts of citric acids, 40 parts, wheat bran, 10 parts of fish meal, 25 parts, mineral matter, 2 parts of vitamins, 5 parts of Pinus massonianas, 12 parts of China trees, 20 parts, garlic, 16 parts of pumpkin, 6 parts of Chinese tallowtree leafs, 10 parts of fragrant eupatorium herbs, 10 parts of Eupatorium adenophorums, 10 parts of guayule rubbers, 10 parts of kuh-sengs, 15 parts, Chinese gall, 20 parts, nano controlled-release carrier;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
Wherein, mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
Wherein, vitamin is the mixture of vitamin A, vitamin B2, pyridoxamine, cobalamin, vitamin D and vitamin E.
The manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, basal feed is pulverized and be uniformly mixed into wheat bran, fish meal, mineral matter, vitamin;
(3) according to proportioning described in claim 1, fish protein active polypeptide, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) auxiliary feed, nano controlled-release carrier that the basal feed that puff step (1) being obtained, (2) obtain, (3) obtain are fully uniformly mixed;
(5) mixture making in step (4) is placed in comminutor, through granulation, dry obtain pest-resistant sterilization composite multi-component feed;
Wherein, the manufacture method of fish protein active polypeptide is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated fish albumen is added to pancreatin, the weight of described pancreatin is 2% of fish protein raw materials weight, and its enzymolysis time is 3 hours, and its hydrolysis temperature is 30 ℃;
(C) after step (B), go out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
The present invention adds fish protein active polypeptide in aquaculture feed, can strengthen animal absorbs the equilibrium of amino acid and other nutrient, significantly improve the utilization rate of animal to mineral matter elements such as calcium, iron, magnesium, zinc, promote animal nutritional rehabilitation, improve immunity of organisms, improve production performance, animal seedling percent is obviously improved.
The present invention also adds the sunflower oil accessory substance sunflower meal that raw material resources are abundant in aquaculture feed, owing to containing rich in protein in sunflower meal, especially contain unrighted acid-linoleic acid that animal itself can not be synthetic, can avoid that acid heat or during metabolic disorder because of unsaturated fat, harmful effect to body cell and organ generation, can prevent the phenomenon that growth of animal rate reduces and seedling percent reduces.
The present invention has added puff and soybean lecithin in aquaculture feed, puff absorbs the reaction of moisture generating gasification after feedstuff feeding, produce gas, soybean lecithin forms oil layer at particle skin in feed granules water absorption course, prevent gas leak, when the proportion of feed granules is lighter than water, particle can slowly float, be convenient to the situation of ingesting that user observes aquatic products, slowly floating aquatic product feed of the present invention can slowly float after throwing something and feeding, and by oil layer, wrap up outside feed granules, thereby feed granules can not scatter in water, be convenient to ingesting of aquatic products, also avoided feed nutrient scattering and disappearing in water, and reduced the pollution of feed granules to water body.
Embodiment bis-:
Pest-resistant sterilization composite multi-component feed of the present invention, raw material consists of fish protein active polypeptide, sunflower meal, soybean lecithin, soda ash, citric acid, wheat bran, fish meal, mineral matter, vitamin;
Each constituent content is respectively by mass fraction:
40 parts of fish protein active polypeptides, 90 parts of sunflower meals, 70 parts of soybean lecithins, 45 parts of soda ash, 45 parts of citric acids, 128 parts, wheat bran, 85 parts of fish meal, 45 parts, mineral matter, 10 parts of vitamins, 15 parts of Pinus massonianas, 24 parts of China trees, 30 parts, garlic, 27 parts of pumpkin, 13 parts of Chinese tallowtree leafs, 20 parts of fragrant eupatorium herbs, 20 parts of Eupatorium adenophorums, 20 parts of guayule rubbers, 20 parts of kuh-sengs, 26 parts, Chinese gall, 25 parts, nano controlled-release carrier;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
Wherein, mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
Wherein, vitamin is the mixture of vitamin A, vitamin B2, pyridoxamine, cobalamin, vitamin D and vitamin E.
The manufacture method of aquaculture feed of the present invention, comprises following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, basal feed is pulverized and be uniformly mixed into wheat bran, fish meal, mineral matter, vitamin;
(3) according to proportioning described in claim 1, fish protein active polypeptide, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall, wolf's milk, cordate houttuynia and tarragon are uniformly mixed into auxiliary feed;
(4) auxiliary feed, nano controlled-release carrier that the basal feed that puff step (1) being obtained, (2) obtain, (3) obtain are fully uniformly mixed;
(5) mixture making in step (4) is placed in comminutor, through granulation, dry obtain pest-resistant sterilization composite multi-component feed;
Wherein, the manufacture method of fish protein active polypeptide is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated fish albumen is added to pancreatin, the weight of described pancreatin is 3% of fish protein raw materials weight, and its enzymolysis time is 3.5 hours, and its hydrolysis temperature is 45 ℃;
(C) after step (B), go out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
More than show and described basic principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof
.
Claims (5)
1. utilize silicon hydroxyapatite as a polynary feed for carrier, it is characterized in that, raw material forms content and is respectively by mass fraction:
Fish protein active polypeptide 20-40 part, sunflower meal 75-90 part, soybean lecithin 55-70 part, soda ash 30-45 part, citric acid 25-45 part, wheat bran 40-128 part, fish meal 10-85 part, mineral matter 25-45 part, vitamin 2-10 part, Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, nano controlled-release carrier 20-25 part,
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.
2. filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
3. polynary feed according to claim 1, is characterized in that,
Described mineral matter is the mixture of ferrous sulfate, zinc sulfate, calcium phosphate and sodium chloride.
4. polynary feed according to claim 1, is characterized in that, described vitamin is the mixture of vitamin A, vitamin B2, pyridoxamine, cobalamin, vitamin D and vitamin E.
5. according to the manufacture method of the aquaculture feed described in claim 1-3 any one, comprise following step:
(1) according to proportioning described in claim 1, soybean lecithin, soda ash, citric acid are mixed, and be stirred into puff;
(2) according to proportioning described in claim 1, basal feed is pulverized and be uniformly mixed into wheat bran, fish meal, mineral matter, vitamin;
(3) according to proportioning described in claim 1 fish protein active polypeptide, sunflower meal, Pinus massoniana, China tree, garlic, pumpkin, Chinese tallowtree leaf, fragrant eupatorium herb, Eupatorium adenophorum, guayule rubber, kuh-seng, Chinese gall;
Be uniformly mixed into auxiliary feed;
(4) auxiliary feed, nano controlled-release carrier that the basal feed that puff step (1) being obtained, (2) obtain, (3) obtain are fully uniformly mixed;
(5) mixture making in step (4) is placed in comminutor, through granulation, dry obtain pest-resistant sterilization composite multi-component feed;
The manufacture method of described fish protein active polypeptide is as follows:
(A) by after the pretreatment such as the dissolving of crude fish protein powder, purification separation, sterilizing, sterilization;
(B) pretreated fish albumen is added to pancreatin, the weight of described pancreatin is the 2-3% of fish protein raw materials weight, and its enzymolysis time is 3-3.5 hour, and its hydrolysis temperature is 30-45 ℃;
(C) after step (B), go out enzyme, separation, sterilization, sterilize, be drying to obtain finished product.
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| CN201310447781.4A CN103519003B (en) | 2013-09-27 | 2013-09-27 | A kind of silicone hydroxyl apatite that utilizes is as the polynary feed of carrier and manufacture method thereof |
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| CN201310447781.4A CN103519003B (en) | 2013-09-27 | 2013-09-27 | A kind of silicone hydroxyl apatite that utilizes is as the polynary feed of carrier and manufacture method thereof |
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