CN103499633B - 基于饱和奶溶液的奶粉中三聚氰胺的快速检测方法 - Google Patents
基于饱和奶溶液的奶粉中三聚氰胺的快速检测方法 Download PDFInfo
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- CN103499633B CN103499633B CN201310481242.2A CN201310481242A CN103499633B CN 103499633 B CN103499633 B CN 103499633B CN 201310481242 A CN201310481242 A CN 201310481242A CN 103499633 B CN103499633 B CN 103499633B
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- melamine
- solution
- saturated
- milk
- milk powder
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- 229920000877 Melamine resin Polymers 0.000 title claims abstract description 93
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 title claims abstract description 92
- 235000013336 milk Nutrition 0.000 title claims abstract description 90
- 239000008267 milk Substances 0.000 title claims abstract description 90
- 210000004080 milk Anatomy 0.000 title claims abstract description 90
- 229920006395 saturated elastomer Polymers 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 43
- 239000000843 powder Substances 0.000 title claims abstract description 40
- 239000000243 solution Substances 0.000 claims abstract description 60
- 238000001514 detection method Methods 0.000 claims abstract description 27
- 239000007864 aqueous solution Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000009791 electrochemical migration reaction Methods 0.000 claims description 20
- 239000012153 distilled water Substances 0.000 claims description 18
- 150000002500 ions Chemical class 0.000 claims description 10
- 235000011837 pasties Nutrition 0.000 claims description 5
- 238000012360 testing method Methods 0.000 abstract description 12
- 239000002904 solvent Substances 0.000 abstract description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 235000013305 food Nutrition 0.000 description 6
- 235000013365 dairy product Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 238000001871 ion mobility spectroscopy Methods 0.000 description 2
- 238000002203 pretreatment Methods 0.000 description 2
- 235000020185 raw untreated milk Nutrition 0.000 description 2
- 208000000913 Kidney Calculi Diseases 0.000 description 1
- 206010029148 Nephrolithiasis Diseases 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 201000001531 bladder carcinoma Diseases 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000020243 first infant milk formula Nutrition 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 235000013350 formula milk Nutrition 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 238000001294 liquid chromatography-tandem mass spectrometry Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011896 sensitive detection Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000004885 tandem mass spectrometry Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 210000003932 urinary bladder Anatomy 0.000 description 1
- 208000010570 urinary bladder carcinoma Diseases 0.000 description 1
- 230000002485 urinary effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
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CN201310481242.2A CN103499633B (zh) | 2013-10-15 | 2013-10-15 | 基于饱和奶溶液的奶粉中三聚氰胺的快速检测方法 |
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CN201310481242.2A CN103499633B (zh) | 2013-10-15 | 2013-10-15 | 基于饱和奶溶液的奶粉中三聚氰胺的快速检测方法 |
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CN103499633A CN103499633A (zh) | 2014-01-08 |
CN103499633B true CN103499633B (zh) | 2015-10-21 |
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Families Citing this family (1)
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CN109470762B (zh) * | 2017-09-07 | 2020-12-29 | 中国科学院大连化学物理研究所 | 一种准确识别丙泊酚注射液是否过期的方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101726533A (zh) * | 2008-10-17 | 2010-06-09 | 中国科学院大连化学物理研究所 | 一种快速、灵敏的检测三聚氰胺的方法 |
CN101852767A (zh) * | 2009-04-01 | 2010-10-06 | 中国科学院大连化学物理研究所 | 一种快速检测痕量三聚氰胺的方法 |
CN101936946A (zh) * | 2009-06-30 | 2011-01-05 | 同方威视技术股份有限公司 | 利用离子迁移谱(ims)技术检测食品或饲料中三聚氰胺的方法 |
CN203224476U (zh) * | 2013-05-02 | 2013-10-02 | 中华人民共和国南通出入境检验检疫局 | 基于高场非对称离子迁移谱技术的食品安全快速检测设备 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2011145186A (ja) * | 2010-01-15 | 2011-07-28 | Mitsubishi Heavy Ind Ltd | 放射性元素検出用化合物及びこれを利用する放射性元素検出用器具並びに放射性元素検出方法 |
JP2012117926A (ja) * | 2010-12-01 | 2012-06-21 | Taiyo Nippon Sanso Corp | 同位体濃度の分析方法 |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101726533A (zh) * | 2008-10-17 | 2010-06-09 | 中国科学院大连化学物理研究所 | 一种快速、灵敏的检测三聚氰胺的方法 |
CN101852767A (zh) * | 2009-04-01 | 2010-10-06 | 中国科学院大连化学物理研究所 | 一种快速检测痕量三聚氰胺的方法 |
CN101936946A (zh) * | 2009-06-30 | 2011-01-05 | 同方威视技术股份有限公司 | 利用离子迁移谱(ims)技术检测食品或饲料中三聚氰胺的方法 |
CN203224476U (zh) * | 2013-05-02 | 2013-10-02 | 中华人民共和国南通出入境检验检疫局 | 基于高场非对称离子迁移谱技术的食品安全快速检测设备 |
Non-Patent Citations (1)
Title |
---|
三聚氰胺检测方法的专利技术进展;李勇;《光谱学与光谱分析》;20101130;第30卷(第11期);第91-92页 * |
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Effective date of registration: 20190620 Address after: No. 899 Industrial Road, Fengxian District, Shanghai 201400 Patentee after: SHANGHAI ZHIRAN DAIRY TECHNOLOGY CO.,LTD. Address before: 214070 305, room 1, 599 West Building Road, Liyuan Development Zone, Wuxi, Jiangsu. Patentee before: WUXI XRESEARCH PRODUCT DESIGN AND RESEARCH Co.,Ltd. |
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Denomination of invention: Method for fast detecting melamine in milk powder based on saturated milk solution Effective date of registration: 20200311 Granted publication date: 20151021 Pledgee: Inner Mongolia Mengniu Dairy (Group) Co.,Ltd. Pledgor: SHANGHAI ZHIRAN DAIRY TECHNOLOGY Co.,Ltd. Registration number: Y2020980000623 |
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Date of cancellation: 20231017 Granted publication date: 20151021 Pledgee: INNER MONGOLIA MENGNIU DAIRY (GROUP) Co.,Ltd. Pledgor: MILKLAND (TIANJIN) FOOD TECHNOLOGY CO.,LTD.|SHANGHAI ZHIRAN DAIRY TECHNOLOGY CO.,LTD. Registration number: Y2020980000623 |
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