CN103493968B - 一种高纯度油用牡丹籽蛋白粉的制备方法 - Google Patents
一种高纯度油用牡丹籽蛋白粉的制备方法 Download PDFInfo
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- CN103493968B CN103493968B CN201310434518.1A CN201310434518A CN103493968B CN 103493968 B CN103493968 B CN 103493968B CN 201310434518 A CN201310434518 A CN 201310434518A CN 103493968 B CN103493968 B CN 103493968B
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- peony seeds
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- 108090000623 proteins and genes Proteins 0.000 title abstract description 7
- 102000004169 proteins and genes Human genes 0.000 title abstract description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 29
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 81
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- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- 238000009413 insulation Methods 0.000 claims description 14
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- 239000013049 sediment Substances 0.000 claims description 14
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- 239000002253 acid Substances 0.000 claims description 8
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- 241000233805 Phoenix Species 0.000 claims description 7
- 239000003513 alkali Substances 0.000 claims description 7
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- 239000010734 process oil Substances 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 7
- 238000001694 spray drying Methods 0.000 claims description 7
- 238000013517 stratification Methods 0.000 claims description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
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- QQUHMASGPODSIW-UHFFFAOYSA-N Albiflorin Natural products C=1C=CC=CC=1C(=O)OCC12C(=O)OC3(C)CC(O)C1CC32OC1OC(CO)C(O)C(O)C1O QQUHMASGPODSIW-UHFFFAOYSA-N 0.000 description 2
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- 241000219226 Acer truncatum Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
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- QQUHMASGPODSIW-ICECTASOSA-N albiflorin Chemical compound O([C@@]12C[C@H]3[C@H](O)C[C@@]1(OC(=O)[C@]32COC(=O)C=1C=CC=CC=1)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O QQUHMASGPODSIW-ICECTASOSA-N 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
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- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- YKRGDOXKVOZESV-UHFFFAOYSA-N paeoniflorin Natural products O1C(C)(C2(CC34)OC5C(C(O)C(O)C(CO)O5)O)CC3(O)OC1C24COC(=O)C1=CC=CC=C1 YKRGDOXKVOZESV-UHFFFAOYSA-N 0.000 description 1
- 235000021118 plant-derived protein Nutrition 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Peptides Or Proteins (AREA)
- Medicines Containing Plant Substances (AREA)
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103960717B (zh) * | 2014-04-09 | 2015-05-06 | 洛阳春魁农业开发有限公司 | 一种牡丹植物蛋白饮料及其制备方法 |
CN103960718B (zh) * | 2014-04-09 | 2015-07-22 | 洛阳春魁农业开发有限公司 | 一种高营养牡丹饮料及其制备方法 |
CN103937865B (zh) * | 2014-04-28 | 2015-04-08 | 李�杰 | 牡丹多肽,及制备方法和应用 |
CN104017850B (zh) * | 2014-06-26 | 2016-10-12 | 河南科技大学 | 一种用牡丹籽饼粕制备牡丹小肽的方法及牡丹小肽的应用 |
CN104087424B (zh) * | 2014-08-04 | 2016-06-29 | 安阳市晶华油脂工程有限公司 | 一步萃取、分离牡丹鲜花精油、水溶液、脂质的方法 |
CN110226664A (zh) * | 2019-07-16 | 2019-09-13 | 山西潞安石圪节智华生物科技有限公司 | 一种牡丹籽蛋白粉的制备方法 |
CN113383851B (zh) * | 2021-07-02 | 2023-09-01 | 山东省科学院菏泽分院 | 一种提取油用牡丹分离蛋白的方法 |
CN114525169B (zh) * | 2022-01-19 | 2022-11-15 | 西安海斯夫生物科技有限公司 | 一种连续分级处理牡丹籽的方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1284504A (zh) * | 2000-08-24 | 2001-02-21 | 李振铎 | 从脱脂大豆粕中同时提取异黄酮、皂甙、低聚糖和蛋白的方法 |
CN101095454A (zh) * | 2007-06-23 | 2008-01-02 | 西藏宇妥藏药研究有限公司 | 一种采用膜分离技术从谷物籽粒中分离蛋白质的方法 |
CN102491898A (zh) * | 2011-11-16 | 2012-06-13 | 中国农业科学院农产品加工研究所 | 由葵花粕中同时提取绿原酸和葵花蛋白的方法 |
CN102994208A (zh) * | 2011-08-05 | 2013-03-27 | 洛阳天香牡丹开发有限公司 | 一种牡丹制品的提取方法 |
CN103113434A (zh) * | 2013-02-27 | 2013-05-22 | 河南科技大学 | 一种从油用牡丹籽饼粕中制备单萜苷的方法 |
CN103130850A (zh) * | 2013-02-27 | 2013-06-05 | 河南科技大学 | 一种从油用牡丹籽饼粕中制备芍药苷的方法 |
Family Cites Families (1)
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JP2006206584A (ja) * | 2004-12-27 | 2006-08-10 | Tohoku Univ | アミロイドβ蛋白の凝集抑制剤、凝集アミロイドβ蛋白の分解剤、抗痴呆薬および抗痴呆性食品 |
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Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1284504A (zh) * | 2000-08-24 | 2001-02-21 | 李振铎 | 从脱脂大豆粕中同时提取异黄酮、皂甙、低聚糖和蛋白的方法 |
CN101095454A (zh) * | 2007-06-23 | 2008-01-02 | 西藏宇妥藏药研究有限公司 | 一种采用膜分离技术从谷物籽粒中分离蛋白质的方法 |
CN102994208A (zh) * | 2011-08-05 | 2013-03-27 | 洛阳天香牡丹开发有限公司 | 一种牡丹制品的提取方法 |
CN102491898A (zh) * | 2011-11-16 | 2012-06-13 | 中国农业科学院农产品加工研究所 | 由葵花粕中同时提取绿原酸和葵花蛋白的方法 |
CN103113434A (zh) * | 2013-02-27 | 2013-05-22 | 河南科技大学 | 一种从油用牡丹籽饼粕中制备单萜苷的方法 |
CN103130850A (zh) * | 2013-02-27 | 2013-06-05 | 河南科技大学 | 一种从油用牡丹籽饼粕中制备芍药苷的方法 |
Non-Patent Citations (3)
Title |
---|
JP特开2006-206584A 2006.08.10 |
姜绍通,等.乙醇浸提法制备菜籽浓缩蛋白的工艺研究.《食品科学》.2009,第30卷(第4期),第123-126页. * |
庞雪风,等.牡丹籽油的提取及蛋白制备工艺的研究.《食品工业》.2013,第34卷(第8期),第73-76页. * |
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Effective date of registration: 20200706 Address after: 403-72, 4th floor, building 1, yinkun science and Technology Park, no.6, Fenghua Road, Gaoxin, Luoyang area, China (Henan) pilot Free Trade Zone, 471000 Patentee after: Luoyang wanjingxiang peony industry group Co.,Ltd. Address before: 471000 Xiyuan Road, Jianxi District, Henan, No. 48, No. Patentee before: HENAN University OF SCIENCE AND TECHNOLOGY |
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Effective date of registration: 20240129 Address after: No. 1 Wanjingxiang, Zhougou Village, Lvdian Town, Yichuan County, Luoyang City, Henan Province, 471313 Patentee after: Wanjingxiang agricultural technology development (Luoyang) Co.,Ltd. Country or region after: China Address before: Room 403-72, 4th Floor, Building 1, Yinkun Science and Technology Park, No. 6 Gaoxin Fenghua Road, Luoyang Area, China (Henan) Pilot Free Trade Zone, 471000 Patentee before: Luoyang wanjingxiang peony industry group Co.,Ltd. Country or region before: China |