CN103445157A - Clarification method of ultrafiltration enzyme in preparation of ginseng juice - Google Patents

Clarification method of ultrafiltration enzyme in preparation of ginseng juice Download PDF

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Publication number
CN103445157A
CN103445157A CN2013103558890A CN201310355889A CN103445157A CN 103445157 A CN103445157 A CN 103445157A CN 2013103558890 A CN2013103558890 A CN 2013103558890A CN 201310355889 A CN201310355889 A CN 201310355889A CN 103445157 A CN103445157 A CN 103445157A
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ginseng
enzyme
juice
ultrafiltration
ultrafiltration enzyme
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CN103445157B (en
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胡耀辉
刘芳茗
王玉华
刘俊梅
朴春红
于寒松
代伟长
房鑫
张静晨
于晓明
李琢伟
吴杰
范春艳
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Jilin Agricultural University
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Jilin Agricultural University
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Abstract

The invention discloses a clarification method of ultrafiltration enzyme in the preparation of ginseng juice. The clarification method comprises the following steps: cutting clean ginseng into slices with the thickness of 5mm, adding purified water to a material-liquid ratio of 1:8-1:12, mincing by using a pulverizer, and then finely grinding ginseng pulp by using a colloid mill; adjusting pH value by adopting citric acid and lactic acid; carrying out high-temperature and high-pressure treatment; cooling, placing the ginseng pulp into an enzymolysis tank, adjusting pH value by using sodium bicarbonate, preserving heat and carrying out hydrolysis; and carrying out enzyme deactivation treatment at 100 DEG C, carrying out centrifugal treatment and filtering the ginseng pulp to obtain clarified ginseng juice. After the ginseng pulp prepared by the clarification method is treated by the ultrafiltration enzyme, macromolecular substances such as cellulose, pectin and protein are partially hydrolyzed to be in a micromolecular state, so that the ginseng juice is obviously clarified, the yield of the ginseng juice is increased, and the flavor of the ginseng juice is improved; meanwhile, the utilization rate of the ginseng can be effectively increased, the production process is easy, the operation is convenient, the cost is low, and the clarification method is suitable for large-scale industrial production.

Description

The defecation method of a kind of ultrafiltration enzyme in preparing ginseng juice
Technical field
The invention belongs to liquid ginseng product preparation field, relate in particular to the defecation method of a kind of ultrafiltration enzyme in preparing ginseng juice.
Background technology
Ginseng has the good reputation of " kings of hundred grass " since ancient times, why very rare, very famous and precious, main relevant with its medical value.In medical book Shennong's Herbal very early, just think, ginseng has the effect of " tonifying five zang organs, peace spirit, determine soul, only palpitation with fear, except perverse trend, the happy intelligence development of improving eyesight ", " take to make light of one's life by commiting suicide for a long time and prolong life ".Li Shizhen (1518-1593 A.D.) is also very praised highly ginseng in Compendium of Material Medica, thinks that it can " control all chronic diseases marked by deficiency of vital energy of male woman ".For thousands of years, ginseng all is listed in " top grade ".According to the regulation of " People's Republic of China's the law of food safety " and " new resource food management method ", it is new resource food that the Ministry of Public Health in 2012 ratifies ginseng (artificial growth), and edible position is: root and rhizome, ginseng is from the medicinal food resource that changes into.At present, ginseng can be widely used in the fields such as food, medicine, cosmetics and wine brewing.
In the production of liquid ginseng product, the clarification operation is the key that determines its presentation quality, as deals with improperly, not only affects product appearance, and directly has influence on quality and the stability of liquid ginseng product.The ultrafiltration enzyme is a kind of complex enzyme, not only can make ginseng slurry clarification, the compositions such as protein wherein, pectin, cellulose further can also be decomposed, and realizes the efficient utilization of ginseng.
Summary of the invention
The purpose of the embodiment of the present invention is to provide the defecation method of a kind of ultrafiltration enzyme in preparing ginseng juice, be intended to solve existing method of producing liquid ginseng product and lack scientific and reasonable design, cause the quality of liquid ginseng product of preparation and the problem of poor stability.
The embodiment of the present invention is achieved in that the defecation method of a kind of ultrafiltration enzyme in preparing ginseng juice, and the defecation method of this ultrafiltration enzyme in preparing ginseng juice comprises the following steps:
Step 1, get the sheet that clean ginseng is cut into 5 millimeters thickness, adding pure water to solid-liquid ratio is 1: 8~1: 12, with pulverizer, rubs, and then uses colloid mill fine grinding ginseng slurry;
Step 2, employing citric acid, lactic acid are adjusted the pH value;
Step 3, high temperature high pressure process;
Step 4, cooling, put into enzymatic vessel by the ginseng slurry, with sodium acid carbonate, regulates pH, insulation, hydrolysis;
Step 5,100 ℃ of enzymes that go out are processed, and carry out centrifugal treating and filter the ginseng juice that the ginseng slurry obtains clarification.
Further, if bright ginseng when the ginseng section adds pure water, solid-liquid ratio is 1: 8~1: 10; If trepang, solid-liquid ratio is 1: 10~1: 12.
Further, the pulverizer that the rubbing ginseng adopts can adopt cooking machine to replace.
Further, can adopt any one in citric acid, lactic acid while adjusting the pH value in step 2, also can use simultaneously; Adjust pH value to 3.2~3.8 in step 2.
Further, in step 3, the temperature of high temperature high pressure process is 105~115 ℃, and the processing time is 10~15 minutes.
Further, be cooled to 50~60 ℃ in step 4, before enzymolysis, adopt sodium acid carbonate to regulate pH to 3.8~4.2, the addition that adds the ultrafiltration enzyme carries out according to 80.0~100.0 milliliters/ton, and holding temperature is 50~60 ℃, and hydrolysis time is 2 hours.
Further, the time that the enzyme that goes out in step 5 is processed is 15~30 minutes, and the rotating speed of the centrifuge of centrifugal filtration ginseng slurry is 10000 rev/mins, and the centrifugal time is 10 minutes.
Further, described enzyme preparation is the ultrafiltration enzyme.
Further, northeast ginseng, Korean ginseng and American Ginseng and the red ginseng be prepared into by these ginsengs, suncured white ginseng root, sun-dried ginseng product all can adopt the liquid ginseng product of ultrafiltration enzyme clarification preparation.
The invention provides the defecation method of a kind of ultrafiltration enzyme in preparing ginseng juice, ginseng slurry prepared by the method is after the ultrafiltration enzyme is processed, the macromolecular substances partial hydrolysis such as cellulose, pectin, protein become little molecular state, ginseng juice is obviously clarified, improved the productive rate of ginseng juice and improved the local flavor of ginseng juice.The present invention can effectively improve the ginseng utilization rate, and production technology is simple, easy to operate, and cost is low, is suitable for large-scale industrial production.
The accompanying drawing explanation
Fig. 1 is the defecation method flow chart of ultrafiltration enzyme in preparing ginseng juice that the embodiment of the present invention provides.
The specific embodiment
In order to make purpose of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
Fig. 1 shows the flow process of the defecation method of ultrafiltration enzyme provided by the invention in preparing ginseng juice.For convenience of explanation, only show part related to the present invention.
The defecation method of ultrafiltration enzyme in preparing ginseng juice that the embodiment of the present invention provides comprises the following steps:
Step 1, get the sheet that clean ginseng is cut into 5 millimeters thickness, adding pure water to solid-liquid ratio is 1: 8~1: 12, with pulverizer, rubs, and then uses colloid mill fine grinding ginseng slurry;
Step 2, employing citric acid, lactic acid are adjusted the pH value;
Step 3, high temperature high pressure process;
Step 4, cooling, put into enzymatic vessel by the ginseng slurry, with sodium acid carbonate, regulates pH, insulation, hydrolysis;
Step 5,100 ℃ of enzymes that go out are processed, and carry out centrifugal treating and filter the ginseng juice that the ginseng slurry obtains clarification.
As a prioritization scheme of the embodiment of the present invention, if bright ginseng when the ginseng section adds pure water, solid-liquid ratio is 1: 8~1: 10; If trepang, solid-liquid ratio is 1: 10~1: 12.
As a prioritization scheme of the embodiment of the present invention, the pulverizer that rubs the ginseng employing can adopt cooking machine to replace.
As a prioritization scheme of the embodiment of the present invention, can adopt any one in citric acid, lactic acid while adjusting the pH value in step 2, also can use simultaneously; Adjust pH value to 3.2~3.8 in step 2.
As a prioritization scheme of the embodiment of the present invention, in step 3, the temperature of high temperature high pressure process is 105~115 ℃, and the processing time is 10~15 minutes.
A prioritization scheme as the embodiment of the present invention, be cooled to 50~60 ℃ in step 4, before enzymolysis, adopt sodium acid carbonate to regulate pH to 3.8~4.2, the addition that adds the ultrafiltration enzyme carries out according to 80.0~100.0 milliliters/ton, holding temperature is 50~60 ℃, and hydrolysis time is 2 hours.
As a prioritization scheme of the embodiment of the present invention, the time that the enzyme that goes out in step 5 is processed is 15~30 minutes, and the rotating speed of the centrifuge of centrifugal filtration ginseng slurry is 10000 rev/mins, and the centrifugal time is 10 minutes.
As a prioritization scheme of the embodiment of the present invention, described enzyme preparation is the ultrafiltration enzyme.
As a prioritization scheme of the embodiment of the present invention, northeast ginseng, Korean ginseng and American Ginseng and the red ginseng be prepared into by these ginsengs, suncured white ginseng root, sun-dried ginseng product all can adopt the liquid ginseng product of ultrafiltration enzyme clarification preparation.
Below in conjunction with drawings and the specific embodiments, application principle of the present invention is further described.
The defecation method of ultrafiltration enzyme in preparing ginseng juice that the embodiment of the present invention provides comprises the following steps:
S101: get the sheet that clean ginseng is cut into 5 millimeters thickness, adding pure water to solid-liquid ratio is 1: 8~1: 12, with pulverizer, rubs, and then uses colloid mill fine grinding ginseng slurry;
S102: adopt citric acid, lactic acid to adjust the pH value;
S103: high temperature high pressure process;
S104: cooling, the ginseng slurry is put into to enzymatic vessel, regulate pH with sodium acid carbonate, insulation, hydrolysis;
The S105:100 ℃ of enzyme that goes out processed, and carries out centrifugal treating and filters the ginseng juice that the ginseng slurry obtains clarification.
The specific embodiment below in conjunction with specific embodiment defecation method in preparing ginseng juice to the ultrafiltration enzyme is described in detail.
Embodiment 1
Get clean bright northeast ginseng 100 grams, be cut into the sheet of 5 millimeter thickness, add 1000 milliliters of pure water, use the abundant comminuting matter of food processor to even pulpous state, with citric acid, adjust pH value to 3.5, use high temperature and high pressure method to process the ginseng slurry, 110 ℃ of temperature, 10 minutes time.Be cooled to 50~60 ℃, the ginseng slurry is put into to enzymatic vessel, with sodium bicarbonate solution, regulate ginseng slurry pH to 4.0, heating water bath, add 0.105 milliliter of ultrafiltration enzyme, thermostatic effect 2 hours in the time of 55 ℃.After enzymolysis completes, ginseng is starched under 100 ℃ of conditions, and the enzyme that gone out is processed 15 minutes, then carries out centrifugal filtration processing (rotating speed of centrifuge is 10000 rev/mins, and the centrifugal time is 10 minutes), 930 milliliters, the ginseng juice of final acquisition clarification.
Embodiment 2
Get clean bright Korean ginseng 100 grams, be cut into the sheet of 5 millimeter thickness, add 1000 milliliters of pure water, use the abundant comminuting matter of food processor to even pulpous state, with citric acid, adjust pH value to 3.5, use high temperature and high pressure method to process the ginseng slurry, 110 ℃ of temperature, 15 minutes time.Be cooled to 50~60 ℃, the ginseng slurry is put into to enzymatic vessel, with sodium bicarbonate solution, regulate ginseng slurry pH to 4.0, heating water bath, add 0.1 milliliter of ultrafiltration enzyme, thermostatic effect 2 hours in the time of 55 ℃.After enzymolysis completes, ginseng is starched under 100 ℃ of conditions, and the enzyme that gone out is processed 15 minutes, then carries out centrifugal filtration processing (rotating speed of centrifuge is 10000 rev/mins, and the centrifugal time is 10 minutes), 915 milliliters, the ginseng juice of final acquisition clarification.
Embodiment 3
Get clean bright American Ginseng 100 grams, be cut into the sheet of 5 millimeter thickness, add 1000 milliliters of pure water, use the abundant comminuting matter of food processor to even pulpous state, with citric acid, adjust pH value to 3.5, use high temperature and high pressure method to process the ginseng slurry, 110 ℃ of temperature, 10 minutes time.Be cooled to 50~60 ℃, the ginseng slurry is put into to enzymatic vessel, with sodium bicarbonate solution, regulate ginseng slurry pH to 4.0, heating water bath, add 0.095 milliliter of ultrafiltration enzyme, thermostatic effect 2 hours in the time of 55 ℃.After enzymolysis completes, ginseng is starched under 100 ℃ of conditions, and the enzyme that gone out is processed 15 minutes, then carries out centrifugal filtration processing (rotating speed of centrifuge is 10000 rev/mins, and the centrifugal time is 10 minutes), 908 milliliters, the ginseng juice of final acquisition clarification.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.

Claims (9)

1. the defecation method of a ultrafiltration enzyme in preparing ginseng juice, is characterized in that, the defecation method of this ultrafiltration enzyme in preparing ginseng juice comprises the following steps:
Step 1, get clean ginseng and be cut into sheet, adding pure water to solid-liquid ratio is 1: 8~1: 12, with pulverizer, rubs, and then uses colloid mill fine grinding ginseng slurry;
Step 2, employing citric acid, lactic acid are adjusted the pH value;
Step 3, high temperature high pressure process;
Step 4, cooling, put into enzymatic vessel by the ginseng slurry, with sodium acid carbonate, regulates pH, insulation, hydrolysis;
Step 5,100 ℃ of enzymes that go out are processed, and carry out centrifugal treating and filter the ginseng juice that the ginseng slurry obtains clarification.
2. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, if bright ginseng when the ginseng section adds pure water, solid-liquid ratio is 1: 8~1: 10; If trepang, solid-liquid ratio is 1: 10~1: 12.
3. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, the pulverizer that rubs the ginseng employing can adopt cooking machine to replace.
4. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, can adopt any one in citric acid, lactic acid while in step 2, adjusting the pH value, also can use simultaneously; Adjust pH value to 3.2~3.8 in step 2.
5. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, in step 3, the temperature of high temperature high pressure process is 105~115 ℃, and the processing time is 10~15 minutes.
6. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, it is characterized in that, be cooled to 50~60 ℃ in step 4, before enzymolysis, adopt sodium acid carbonate to regulate pH to 3.8~4.2, the addition that adds the ultrafiltration enzyme carries out according to 80.0~100.0 milliliters/ton, holding temperature is 50~60 ℃, and hydrolysis time is 2 hours.
7. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, the time that the enzyme that goes out in step 5 is processed is 15~30 minutes, and the rotating speed of the centrifuge of centrifugal filtration ginseng slurry is 10000 rev/mins, and the centrifugal time is 10 minutes.
8. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, is characterized in that, described enzyme preparation is the ultrafiltration enzyme.
9. the defecation method of ultrafiltration enzyme as claimed in claim 1 in preparing ginseng juice, it is characterized in that, northeast ginseng, Korean ginseng and American Ginseng and the red ginseng be prepared into by these ginsengs, suncured white ginseng root, sun-dried ginseng product all can adopt the liquid ginseng product of ultrafiltration enzyme clarification preparation.
CN201310355889.0A 2013-08-11 2013-08-11 Clarification method of ultrafiltration enzyme in preparation of ginseng juice Active CN103445157B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104721245A (en) * 2015-03-28 2015-06-24 珲春绿源参业生物科技有限公司 Method for making ginseng extraction component by multi-enzyme enzymolysis
CN109757639A (en) * 2019-03-20 2019-05-17 战铁楠 A kind of ginseng ternary peptide beverage and preparation method thereof
CN109757641A (en) * 2019-03-20 2019-05-17 战铁楠 A kind of ginseng small-molecular peptides beverage and preparation method thereof

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CN1186637A (en) * 1998-01-14 1998-07-08 马辉 Health genseng drink and its preparing method
CN1325693A (en) * 2000-05-29 2001-12-12 厦门中卫多糖研究所 Process for preparing ginseng extract powder
KR20040023185A (en) * 2002-09-11 2004-03-18 한국홍삼제조 주식회사 Manufacturing method of black rootlets of ginseng
CN1535624A (en) * 2003-04-04 2004-10-13 ÷ Ginseng American ginseng beverage and its production process
CN101278954A (en) * 2007-04-04 2008-10-08 赵方林 Ginseng or American ginseng product with increased content of ginseng saponin Rg3 and method of preparing the same
CN102600222A (en) * 2012-04-13 2012-07-25 吉林农业大学 Method for increasing content of rare saponin in ginseng raw material by explosion of steam
CN102987482A (en) * 2012-11-29 2013-03-27 新疆天海绿洲农业科技股份有限公司 Concentrated red date juice and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1186637A (en) * 1998-01-14 1998-07-08 马辉 Health genseng drink and its preparing method
CN1325693A (en) * 2000-05-29 2001-12-12 厦门中卫多糖研究所 Process for preparing ginseng extract powder
KR20040023185A (en) * 2002-09-11 2004-03-18 한국홍삼제조 주식회사 Manufacturing method of black rootlets of ginseng
CN1535624A (en) * 2003-04-04 2004-10-13 ÷ Ginseng American ginseng beverage and its production process
CN101278954A (en) * 2007-04-04 2008-10-08 赵方林 Ginseng or American ginseng product with increased content of ginseng saponin Rg3 and method of preparing the same
CN102600222A (en) * 2012-04-13 2012-07-25 吉林农业大学 Method for increasing content of rare saponin in ginseng raw material by explosion of steam
CN102987482A (en) * 2012-11-29 2013-03-27 新疆天海绿洲农业科技股份有限公司 Concentrated red date juice and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104721245A (en) * 2015-03-28 2015-06-24 珲春绿源参业生物科技有限公司 Method for making ginseng extraction component by multi-enzyme enzymolysis
CN109757639A (en) * 2019-03-20 2019-05-17 战铁楠 A kind of ginseng ternary peptide beverage and preparation method thereof
CN109757641A (en) * 2019-03-20 2019-05-17 战铁楠 A kind of ginseng small-molecular peptides beverage and preparation method thereof

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