CN103420408A - 一种纳米氧化铜的制备方法 - Google Patents
一种纳米氧化铜的制备方法 Download PDFInfo
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- CN103420408A CN103420408A CN2013102947374A CN201310294737A CN103420408A CN 103420408 A CN103420408 A CN 103420408A CN 2013102947374 A CN2013102947374 A CN 2013102947374A CN 201310294737 A CN201310294737 A CN 201310294737A CN 103420408 A CN103420408 A CN 103420408A
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- Prior art keywords
- mol
- cupric oxide
- mantoquita
- preparation
- nano cupric
- Prior art date
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- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 title claims abstract description 53
- 238000000034 method Methods 0.000 title abstract description 11
- 239000005751 Copper oxide Substances 0.000 title abstract description 5
- 229910000431 copper oxide Inorganic materials 0.000 title abstract description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 24
- 229920001732 Lignosulfonate Polymers 0.000 claims abstract description 18
- 229960004643 cupric oxide Drugs 0.000 claims description 25
- 235000019357 lignosulphonate Nutrition 0.000 claims description 15
- 239000004570 mortar (masonry) Substances 0.000 claims description 14
- 238000002360 preparation method Methods 0.000 claims description 12
- 239000007787 solid Substances 0.000 claims description 12
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 9
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 6
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 claims description 6
- 239000011575 calcium Substances 0.000 claims description 6
- 229910052791 calcium Inorganic materials 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 229920005610 lignin Polymers 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- -1 centrifugation Substances 0.000 claims description 3
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 3
- 239000002244 precipitate Substances 0.000 claims description 3
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 3
- 239000006227 byproduct Substances 0.000 abstract description 3
- 239000012071 phase Substances 0.000 abstract description 3
- 238000010532 solid phase synthesis reaction Methods 0.000 abstract description 3
- 239000002887 superconductor Substances 0.000 abstract description 3
- 230000007704 transition Effects 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 238000001354 calcination Methods 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 abstract description 2
- 125000000524 functional group Chemical group 0.000 abstract description 2
- 238000005054 agglomeration Methods 0.000 abstract 1
- 230000002776 aggregation Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000001879 copper Chemical class 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000004537 pulping Methods 0.000 abstract 1
- 238000003746 solid phase reaction Methods 0.000 abstract 1
- 230000008901 benefit Effects 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000005287 template synthesis Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
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- Crystals, And After-Treatments Of Crystals (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN201310294737.4A CN103420408B (zh) | 2013-07-12 | 2013-07-12 | 一种纳米氧化铜的制备方法 |
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CN201310294737.4A CN103420408B (zh) | 2013-07-12 | 2013-07-12 | 一种纳米氧化铜的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN103420408A true CN103420408A (zh) | 2013-12-04 |
CN103420408B CN103420408B (zh) | 2015-08-26 |
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CN201310294737.4A Active CN103420408B (zh) | 2013-07-12 | 2013-07-12 | 一种纳米氧化铜的制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103979600A (zh) * | 2014-05-30 | 2014-08-13 | 上海沃凯生物技术有限公司 | 一种超细氧化铜粉的制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101544393A (zh) * | 2008-05-05 | 2009-09-30 | 山东科技大学 | 一种纳米氧化铜两步固相合成的方法 |
CN102602976A (zh) * | 2012-03-09 | 2012-07-25 | 天津理工大学 | 一种CuO纳米薄膜的制备方法 |
CN102941110A (zh) * | 2012-11-16 | 2013-02-27 | 江苏大学 | 一种纳米氧化锌复合光催化剂的制备方法 |
-
2013
- 2013-07-12 CN CN201310294737.4A patent/CN103420408B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101544393A (zh) * | 2008-05-05 | 2009-09-30 | 山东科技大学 | 一种纳米氧化铜两步固相合成的方法 |
CN102602976A (zh) * | 2012-03-09 | 2012-07-25 | 天津理工大学 | 一种CuO纳米薄膜的制备方法 |
CN102941110A (zh) * | 2012-11-16 | 2013-02-27 | 江苏大学 | 一种纳米氧化锌复合光催化剂的制备方法 |
Non-Patent Citations (3)
Title |
---|
ZHANG, MENG等: "Microwave-assisted synthesis and characterization of CuO nanocrystals", 《JOURNAL OF DISPERSION SCIENCE AND TECHNOLOGY》 * |
李道华: "CuO纳米晶的一步超声室温固相合成及表征", 《西南民族大学学报•自然科学版》 * |
李道华: "CuO纳米晶的一步超声室温固相合成及表征", 《西南民族大学学报•自然科学版》, vol. 35, no. 5, 30 September 2009 (2009-09-30), pages 1032 - 1036 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103979600A (zh) * | 2014-05-30 | 2014-08-13 | 上海沃凯生物技术有限公司 | 一种超细氧化铜粉的制备方法 |
CN103979600B (zh) * | 2014-05-30 | 2016-08-31 | 上海沃凯生物技术有限公司 | 一种超细氧化铜粉的制备方法 |
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Publication number | Publication date |
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CN103420408B (zh) | 2015-08-26 |
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Effective date of registration: 20171117 Address after: 212100 Zhenjiang City, Jiangsu province Dantu District Tan Kwai Road No. 1 Patentee after: JIANGSU HUIZHI INTELLECTUAL PROPERTY SERVICES Co.,Ltd. Address before: Zhenjiang City, Jiangsu Province, 212013 Jingkou District Road No. 301 Patentee before: Jiangsu University |
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Effective date of registration: 20201023 Address after: No. 159, Chengjiang Middle Road, Jiangyin City, Wuxi City, Jiangsu Province Patentee after: Jiangyin Intellectual Property Operation Co.,Ltd. Address before: 212100 Zhenjiang City, Jiangsu province Dantu District Tan Kwai Road No. 1 Patentee before: JIANGSU HUIZHI INTELLECTUAL PROPERTY SERVICES Co.,Ltd. |
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Effective date of registration: 20240613 Address after: 210000 10th floor, building 5, juhuiyuan, phase II, Xuzhuang high tech Zone, 108 Xuanwu Avenue, Xuanwu District, Nanjing City, Jiangsu Province Patentee after: Nanjing Fuyuan advanced new material Research Institute Co.,Ltd. Country or region after: China Address before: No. 159, Chengjiang Middle Road, Jiangyin City, Wuxi City, Jiangsu Province Patentee before: Jiangyin Intellectual Property Operation Co.,Ltd. Country or region before: China |