CN103301183A - Processing method of milkvetch root fried with honey - Google Patents
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Abstract
The invention provides a processing method of milkvetch root fried with honey. The processing method of milkvetch root fried with honey comprises the following steps of: (1) taking 15-30% by mass of refined honey of crude astragalus membranaceus medicinal slices, adding water, and mixing uniformly, wherein the mass ratio of refined honey to water is 1: (0.5-1.5); (2) placing the crude astragalus membranaceus medicinal slices into the refined honey added with water, blending uniformly, moistening for 40 minutes to 2 hours until the refined honey is fully absorbed by the astragalus membranaceus medicinal slices; and (3) placing the moistened astragalus membranaceus medicinal slices into a microwave container, carrying out microwave heating for 3-5 minutes at high power, turning over once at each 2 minutes during the microwave heating, then placing into a baking oven at 80-100 DEG C, and baking for 30-50 minutes until the surfaces of the medicinal slices are deep yellow or light brown yellow, taking out, airing at room temperature, screening chippings, and sealing, thereby obtaining traditionally Chinese medicine milkvetch root fried with honey medicinal slices. The processing method provided by the invention is stable in technology, and is simple to operate; appearances of the medicinal slices are uniform; the extraction ratio of effective ingredients is high; the quality of medicinal slices among different batches has no obvious difference.
Description
Technical field
The present invention relates to a kind of concocting method of Radix Astragali (processed with Mel), belong to technical field of Chinese medicines.
Background technology
The Radix Astragali is the leguminous plant Radix Astagali
Astragalus.membranaceus (Fisch.
)Bge.var.
Mongholicus(Bge.) Hsiao or Radix Astragali
Astragalus membranaceus(Fisch.) dry root of Bge..The Radix Astragali has tonifying Qi and lifting yang, strengthening superficial resistance to stop perspiration, and inducing diuresis to remove edema promotes the production of body fluid and nourishes blood, the stagnant blood stasis dispelling of row, expelling pus and toxin by strengthening QI, effects such as expelling pus and promoting granulation.It is weak to can be used for the deficiency of vital energy, anorexia and loose stool, and sinking of QI of middle-JIAO, the chronic diarrhea proctoptosis, the metrorrhagia of having blood in stool, the exterior deficiency spontaneous perspiration, deficiency of vital energy edema, interior-heat is quenched one's thirst, blood deficiency and yellow complexion, hemiplegia, the arthralgia pain numbness, carbuncle is difficult bursts, and bursts for a long time and disease such as does not hold back.
The Radix Astragali is widely used clinically medicinal with a long history of China.And in the concrete practice, the Radix Astragali must be made the decoction pieces of different size and can use through following an example to do.Chinese medicine astragalus has multiple concocting method in ancient times, the concocting method recorded of successive dynasties comprise steam, processed with honey, processed with wine, processed with salt, parch, stir-frying with ginger juice etc., but wherein majority now eliminated need not, that uses till today and be most widely used only is the processed with honey method.The Pharmacopoeia of the People's Republic of China 2010 editions has recorded the Radix Astragali and two kinds of decoction pieces specifications of Radix Astragali Preparata, and the concocting method pharmacopeia of Radix Astragali Preparata is defined as: get astragalus mongholicus tablet, fry to tack-free according to processed with honey method (appendix II D).
Therefore the processing procedure of Radix Astragali Preparata though pharmacopeia has regulation, does not have concrete parameter, and it is bigger influenced by subjective factors to the judgement of concocting process and the degree of process of preparing Chinese medicine, and quality often has bigger difference between different batches Radix Astragali Preparata decoction pieces, and clinical efficacy is difficult to guarantee.There is bibliographical information to adopt warming over fire after applying ointment and microwave method to prepare the Radix Astragali Preparata decoction pieces.The warming over fire after applying ointment concocting process is more easy to control, but concocted time is long, and the microwave processing time is short, obtains processed product effective component extraction rate height, but but has the uneven problem of concocting.
Summary of the invention
In order to solve above-mentioned the deficiencies in the prior art, the invention provides a kind of concocting method of new Radix Astragali (processed with Mel), this method process stabilizing, simple to operate, the decoction pieces outward appearance is even, effective component extraction rate height, prepared slice quality no significant difference between different batches.
The present invention is achieved by the following technical solutions:
The present invention adopts the method for smoking behind the first microwave, can prepare high-quality Radix Astragali (processed with Mel) decoction pieces fast.
This method is to be raw material with the Radix Astragali decoction pieces, and step is as follows:
(1) get the refined honey of Radix Astragali prepared slice quality 15～30%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:(0.5～1.5);
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 40 min-2 h are fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) above-mentioned moistening is good Radix Astragali decoction pieces places in the microwave container, HIGH-POWERED MICROWAVES heating 3-5 min, stirred once every 2 minutes during the microwave heating, smoke 30-50 min for 80-100 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
It is adjuvant that the present invention adopts refined honey, in the aqueous solution of refined honey, mix the Radix Astragali decoction pieces thoroughly the moistening certain hour after, be placed in the microwave container, HIGH-POWERED MICROWAVES heating certain hour is heated to decoction pieces surface buff to sundown in the rearmounted baking oven.One aspect of the present invention has remedied traditional processing procedure by the drawback of operator's subjective observation control process of preparing Chinese medicine degree, effectively utilized simultaneously the short and uniform advantage of baking oven for heating of microwave heating time, make prepared slice quality more stable, product quality is convenient to control more, can effectively guarantee clinical efficacy and drug safety.
Concocting method of the present invention simply saves time, easy operating, and the Radix Astragali Preparata decoction pieces color even that makes, glossy, can reach the tradition process of preparing Chinese medicine to the requirement of appearance character.HPLC finger printing by Radix Astragali (processed with Mel) decoction pieces that traditional concocting method, bibliographical information method and this method are made and main component content are relatively, the result shows, the Radix Astragali (processed with Mel) that this law makes can detect Radix Astragali principal character peak, finger printing is three's no significant difference relatively, and the content that the Radix Astragali (processed with Mel) decoction pieces that this method makes records flavone and astragaloside will be higher than other concocting methods.
(1) preparation of sample
1. the inventive method: get the 25g refined honey, add water 20ml, mixing joins in the 100g Radix Astragali decoction pieces, mix thoroughly, moistening to honey is exhausted, put in the microwave oven HIGH-POWERED MICROWAVES and handle 4 min, during stirred once every 2 minutes, take out, put in the baking oven 100 ℃ and smoke 30 min, take out the cold of drying in the air, namely get the Radix Astragali (processed with Mel) decoction pieces.
2. roast method is better than traditional processed with honey method, so the bibliographical information of smoking with reference to the Radix Astragali [[1] Liu Ping, Zhang Yafang, Hu Hankun, etc. Radix Astragali (processed with Mel) process of preparing craft discussion [J]. Chinese patent medicine, 1995,17(9): 19; [2] Yang Zhonglin, Li Xushen, Radix Stephaniae Tetrandrae lance. with the optimum condition [J] of orthogonal experiment method screening Radix Astragali (processed with Mel). Chinese crude drug, 1995,18(9): 457; [3] Zhang Dianqin, pavilion passes book. the new method of Chinese medicine processed with honey [J]. and the Jiangsu traditional Chinese medical science, 1998,19(6): 38; [4] Tao Hong, Zhen Hanchen. the discussion of Radix Astragali (processed with Mel) method [J]. Colleges Of Traditional Chinese Medicine Of Guangxi, 1997,19(8): 21; [5] Yang Zhixiong, Tang Yonghong, Chen Xikun, the best Deng. the preferred Radix Astragali (processed with Mel) of orthogonal experiment method is concocted condition [J]. the time precious traditional Chinese medical science traditional Chinese medicines, 2008,19(3): 722], according to this Radix Astragali decoction pieces inventory, be evaluation criterion to reach the traditional appearance character requirement, adopt roast method to prepare the Radix Astragali (processed with Mel) decoction pieces, method is as follows: get the 25g refined honey, add water 20ml, mixing, join in the 100g Radix Astragali decoction pieces, mix thoroughly, moistening to honey is exhausted, put in the baking oven 100 ℃ and smoke 80min, take out the cold of drying in the air, namely.
3. microwave method can improve Radix Astragali effective ingredient dissolution rate, so with reference to bibliographical information [Yang Zhixiong, the Tang Yonghong of Radix Astragali microwave processing, Chen Xikun, the best Deng. the preferred Radix Astragali (processed with Mel) of orthogonal experiment method is concocted condition [J]. the time precious traditional Chinese medical science traditional Chinese medicines, 2008,19(3): 722], according to this Radix Astragali Preparata decoction pieces inventory, be evaluation criterion to reach the traditional appearance character requirement, adopt microwave method that the Radix Astragali is carried out processed with honey, preparation Radix Astragali (processed with Mel) decoction pieces, concrete grammar is as follows: get the 25g refined honey, add water 20ml, mixing joins in the 100g Radix Astragali decoction pieces, mix thoroughly, moistening to honey is exhausted, and puts 100% microwave firepower heat treated 5min, and the centre is stirred 1 time, the taking-up cold of drying in the air, namely.
4. the Radix Astragali Preparata decoction pieces sample that is equipped with of traditional law system: get the 25g refined honey, add water 20ml, mixing joins in the 100g Radix Astragali decoction pieces, mix thoroughly, moistening to honey is exhausted, and puts in the Chinese medicine processing temperature control furnace, and slow fire is fried and processed to decoction pieces surface buff, the taking-up cold of drying in the air, sieve removes chip, gets the Radix Astragali Preparata decoction pieces.
(2) appearance character relatively
As accompanying drawing, wherein Fig. 1 is 180 ℃ of stir-fry 15min pictures; Fig. 2 is 100 ℃ of baking 80min pictures; Fig. 3 is microwave 5min picture; Fig. 4 is microwave 4min+ baking 30min picture.
From appearance character, the Radix Astragali Preparata decoction pieces that this law and warming over fire after applying ointment make, color even, glossiness is good; When microwave method reaches process of preparing Chinese medicine degree at majority, have more Jiao and stick with paste sheet; The Radix Astragali Preparata decoction pieces focal spot that tradition stir-fry method makes is many, low in glossiness.
(3) flavones ingredient assay
Chromatographic conditionPhenomenex Luna C
18Post (250 mm * 4.6 mm, 5 μ m); Being mobile phase A with the acetonitrile, is Mobile phase B with 0.1% phosphate aqueous solution, carries out gradient elution according to table 1; Flow velocity: 1 mlmin
-1Detect wavelength: 251 nm.
Table 1 gradient elution table
The preparation of need testing solutionGet above-mentioned each Radix Astragali Preparata sample powder (cross 40 mesh sieves) 1 g, accurately claim surely, add methanol 50 ml, heating and refluxing extraction 40 min filter, and filtrate decompression is recycled to dried, add dissolve with methanol and are settled in the 10 ml measuring bottles, get need testing solution.
The preparation of reference substance solutionIt is an amount of that precision takes by weighing calycosin glycosides, ononin, calycosin, formononetin, adds the solution that dissolve with methanol is made 60 μ g/ml, 40 μ g/ml, 35 μ g/ml, 20 μ g/ml respectively, shakes up, in contrast product solution.
AlgoscopyAccurate reference substance solution and each 10 μ l of need testing solution of drawing inject chromatograph of liquid, measure according to above-mentioned chromatographic condition, each concocting method are made each component content compares in the Radix Astragali Preparata.
Be the difference of different each composition of concocting method of more direct embodiment, compare with the form of marking that the component content soprano is decided to be 100 fens.The high-load numerical value of this composition of sample is concocted in other sample size scores=this sample composition content * 100/4 kind.The results are shown in Table 2.
The different concocting methods of table 2 make Radix Astragali Preparata sample size comparative result
By table 2 as seen, calycosin glycosides and formononetin content are all concocted the Radix Astragali Preparata obtain for the highest with the present invention, ononin and calycosin content are also all higher, and the present invention of ononin content is only a little less than microwave method, and the present invention of calycosin content is only a little less than warming over fire after applying ointment.The Radix Astragali Preparata that four flavones ingredient content sums make with this law is for the highest.
(4) assay of astragaloside
Chromatographic conditionThermo Syncronis C
18Post (250 mm * 4.6 mm, 5 μ m); Be mobile phase with acetonitrile-water (32:68), column temperature: 25 ℃, evaporative light scattering detector detects, 110 ℃ of drift tube temperatures, nitrogen volume flow 3.0 Lmin
-1
The preparation of reference substance solutionIt is an amount of to get the astragaloside reference substance, and accurate the title decides, and adds methanol and makes the solution that per 1 m1 contains 0.5 mg, namely.
The preparation of need testing solutionGet about 4 g of powder in this product, the accurate title, decide, and puts in the apparatus,Soxhlet's, add methanol 40 m1, merceration spends the night, and it is an amount of to add methanol again, reflux 4 hours, extracting solution reclaim solvent and are concentrated into driedly, and residue adds water 10 ml, slight fever makes dissolving, extracts 4 times each 40 ml with water saturated n-butyl alcohol jolting, merge n-butyl alcohol liquid, fully wash 2 times each 40 ml with ammonia solution, discard ammoniacal liquor, n-butyl alcohol liquid evaporate to dryness, residue add water 5 m1 makes dissolving, put cold, by D101 type macroporous adsorptive resins, with water 50 m1 eluting, discard water liquid, reuse 40% ethanol 30 ml eluting discard eluent, continue with 70% ethanol, 80 ml eluting, collect eluent, evaporate to dryness, residue adds dissolve with methanol, be transferred in the 5 ml measuring bottles, add methanol to scale, shake up, namely.
AlgoscopyAccurate reference substance solution 10 μ l, 20 μ l of drawing respectively, need testing solution 20 μ l inject chromatograph of liquid, measure, and calculate content with external standard two-point method logarithmic equation, each concocting method are made each component content compares in the Radix Astragali Preparata.
Be the difference of the different concocting methods of clearer embodiment, compare with the form of marking that the Astragaloside content soprano is decided to be 100 fens.The high-load numerical value of sample astragaloside is concocted in content * 100/4 of astragaloside kind in other sample Astragaloside content scoring=these samples.The results are shown in Table 3.
The different concocting methods of table 3 make Radix Astragali Preparata sample size comparative result
By table 3 as seen, this law is concocted the Radix Astragali Preparata that obtains and is compared with other concocting methods, and the Astragaloside content that records is for the highest.
(4) the HPLC collection of illustrative plates relatively
The Radix Astragali Preparata that the HPLC finger printing chromatographic condition that employing is set up makes different concocting methods carries out the HPLC collection of illustrative plates relatively.
Chromatographic conditionPhenomenex luna C
18Post (4.6 mm * 250 mm, 5 μ m)
Chromatographic columnMobile phase: acetonitrile-0.1% phosphate aqueous solution is as the eluent gradient eluting.Detect wavelength 210 nm, flow velocity: 1mlmin
-1, column temperature: 30 ℃. and gradient condition length sees the following form.Sample size: 10 μ l.
Table 4 gradient elution flow sheet
The preparation of need testing solution:Powder 1 g in the sample thief powder (crossing 40 mesh sieves), accurate methanol 50 mL that add claim to decide weight, supersound extraction 60 min are put coldly, weigh again, supply weight, shake up, filter, filtrate is evaporated to dried for 60 ℃, get residue, add dissolve with methanol, and be settled to 5 ml, through 0.45 μ m membrane filtration, namely.
Assay methodAccurate each need testing solution 10 μ l that draw inject high performance liquid chromatograph.Fig. 5 is different processed product stacking charts (S1 the present invention, S2 warming over fire after applying ointment, S3 microwave method, S4 tradition methods)
By the stacking chart as seen, the Radix Astragali Preparata that the present invention makes and tradition are processed the difference that Radix Astragali Preparata decoction pieces that the stir-fry method makes does not have obvious matter, the peak area of the main chromatographic peak of part even will be higher than traditional method and Radix Astragali Preparata that other concocting methods make.
Comprehensive above-mentioned experimental result shows that Radix Astragali Preparata that the present invention makes is better than the concocting method of the Radix Astragali Preparata of traditional process of preparing Chinese medicine method and existing bibliographical information.
Method of the present invention, easy and simple to handle, it is even, glossy to concoct the Radix Astragali Preparata decoction pieces outward appearance that obtains, and concocted time is shorter, and concocting process is easy to control.The Radix Astragali Preparata decoction pieces main constituent content height that makes, the Radix Astragali Preparata prepared slice quality prepared than literature method and traditional method is good.
Description of drawings
Fig. 1 is 180 ℃ and fries the 15min picture;
Fig. 2 is 100 ℃ of baking 75min pictures;
Fig. 3 is microwave 5min picture;
Fig. 4 is microwave 2min+ baking 30min picture;
Fig. 5 is different processed product stacking charts (S1 the present invention, S2 warming over fire after applying ointment, S3 microwave method, S4 tradition methods).
The specific embodiment
The present invention is further illustrated below in conjunction with embodiment.
Embodiment 1
(1) get the refined honey of Radix Astragali prepared slice quality 25%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:0.5;
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 1h is fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) with above-mentioned moistening good Radix Astragali decoction pieces place in the microwave container, behind high-power heating 4 min, stirred once every 2 minutes during this time, smoke 30 min for 100 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
Embodiment 2
(1) get the refined honey of Radix Astragali prepared slice quality 20%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:1;
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 1h is fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) with above-mentioned moistening good Radix Astragali decoction pieces place in the microwave container, behind high-power heating 4 min, stirred once every 2 minutes during this time, smoke 50 min for 80 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
Embodiment 3
(1) get the refined honey of Radix Astragali prepared slice quality 15%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:1.5;
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 40 min are fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) with above-mentioned moistening good Radix Astragali decoction pieces place in the microwave container, behind high-power heating 3 min, stirred once every 2 minutes during this time, smoke 40 min for 100 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
Embodiment 4
(1) get the refined honey of Radix Astragali prepared slice quality 30%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:1;
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 1.5h is fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) with above-mentioned moistening good Radix Astragali decoction pieces place in the microwave container, behind the high-power heating 4.5min, stirred once every 2 minutes during this time, smoke 50 min for 80 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
Claims (1)
1. the concocting method of a Radix Astragali (processed with Mel) comprises the steps:
(1) get the refined honey of Radix Astragali prepared slice quality 15～30%, add water, mixing, wherein, the mass ratio of refined honey and water is 1:(0.5～1.5);
(2) the Radix Astragali decoction pieces is placed the above-mentioned refined honey that adds water, mix thoroughly, moistening 40 min-2 h are fully exhausted by Radix Astragali decoction pieces to refined honey;
(3) above-mentioned moistening is good Radix Astragali decoction pieces places in the microwave container, HIGH-POWERED MICROWAVES heating 3-5 min, stirred once every 2 minutes during the microwave heating, smoke 30-50 min for 80-100 ℃ in the rearmounted baking oven, to decoction pieces surface buff to sundown, take out, dry in the air to room temperature, sieve removes chip, and sealing namely obtains Chinese medicine Radix Astragali (processed with Mel) decoction pieces.
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| CN104257735A (en) * | 2014-09-23 | 2015-01-07 | 苏州市天灵中药饮片有限公司 | Method for preparing milkvetch root fried with honey |
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| CN105267288A (en) * | 2015-11-16 | 2016-01-27 | 刘发元 | Processing method of radix astragali decoction pieces |
| CN109078044A (en) * | 2018-09-28 | 2018-12-25 | 安徽汇中州中药饮片有限公司 | Baikal skullcap root decoction pieces processing procedure |
| CN109464494A (en) * | 2018-12-22 | 2019-03-15 | 北京能济中药饮片有限公司 | A kind of processing method of preparing astragalus membranaceus |
| CN110141593A (en) * | 2019-05-28 | 2019-08-20 | 黄再强 | A kind of preparation method of fresh Radix Notoginseng honey piece |
| CN111220784A (en) * | 2020-02-18 | 2020-06-02 | 山东省中医药研究院 | Honey-roasted white mulberry root-bark and quality evaluation method |
| CN112190606A (en) * | 2020-10-27 | 2021-01-08 | 河南华夏药材有限公司 | Processing method of honey-fried astragalus membranaceus |
| CN114081913A (en) * | 2021-10-12 | 2022-02-25 | 华南理工大学 | Method for microwave curing and processing rehmannia decoction pieces |
| CN113892637A (en) * | 2021-11-04 | 2022-01-07 | 承德医学院 | Preparation method of astragalus honey tablets |
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