CN109078044A - Baikal skullcap root decoction pieces processing procedure - Google Patents
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- CN109078044A CN109078044A CN201811142350.6A CN201811142350A CN109078044A CN 109078044 A CN109078044 A CN 109078044A CN 201811142350 A CN201811142350 A CN 201811142350A CN 109078044 A CN109078044 A CN 109078044A
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- radix scutellariae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/539—Scutellaria (skullcap)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/63—Arthropods
- A61K35/64—Insects, e.g. bees, wasps or fleas
- A61K35/644—Beeswax; Propolis; Royal jelly; Honey
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9068—Zingiber, e.g. garden ginger
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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Abstract
The invention discloses a kind of processing procedures of baikal skullcap root decoction pieces, processed comprising net system, steeping in wine, ginger and jujube juice system, honey and etc., it is processed using rhizoma zingiberis and dry jujube as auxiliary material, effectively enhance radix scutellariae tonifying Qi and lifting yang, Gu table, the effect of cold dispelling are conducive to the performance of radix scutellariae warm nature, simultaneously can also stopping nausea and vomiting by lowering the adverse flow of QI, the absorption of effective ingredient.Using honey as efficacy-enhancing ingredient, and the effect of there is synergistic effect, enhance radix scutellariae tonifying middle-Jiao and Qi is processed with the method for honey toast.The effect of steeping in wine, which processes, can promote radix scutellariae diuretic and maintain drug, apocenosis, expelling pus and promoting granulation, while can inhibit infecting for medicinal material surface microorganism, it prevents putrid and deteriorated.The present invention has that processing step is few simultaneously, easy to operate, can large-scale application the advantages of, provide important reference for the processing procedure improvement of radix scutellariae.
Description
Technical field
The present invention relates to the prepared slices of Chinese crude drugs to process field more particularly to a kind of processing procedure of baikal skullcap root decoction pieces.
Background technique
Chinese medicine contains several chemical components, including toxic, effective component, and the main function of Chinese medicine preparation is that " attenuation increases
Effect ", most Chinese medicines can make less toxic by reasonable processing procedure, but since concocting method and auxiliary material are different, with tradition
Chinese medicine health product is compared, and material base may be substantially change, and drug effect also can increase drug effect with significant change occurs
Purpose, Chinese medicine can reach the therapeutic effect got twice the result with half the effort under appropriate processing procedure.
Radix scutellariae is clinically widely used in medicinal with a long history in China.And in concrete practice, radix scutellariae have to pass through according to
Method processes, and the medicine materical crude slice that different size is made can be applied.Baikal skullcap root is in ancient times there are many concocting method, the big gun that the successive dynasties are recorded
Method processed include steam, sweet system, wine system, salt system, frying, ginger juice etc., but wherein majority is superseded does not have to, and uses till today
And what is be most widely used is only bake with honey.The Pharmacopoeia of the People's Republic of China 2010 editions have been recorded radix scutellariae and toast radix scutellariae two
Kind medicine materical crude slice specification, processs the concocting method States Pharmacopoeia specifications of radix scutellariae are as follows: takes scutellaria tablet, fries according to bake with honey (appendix II D) to tack-free.
Process radix scutellariae processing procedure, though pharmacopeia has regulation, without design parameter, thus to concocting process and process degree judgement by
Subjective factor is affected, and quality often has biggish difference between different batches toast baikal skullcap root decoction pieces, and clinical efficacy is difficult to ensure.
There is document report using drying method and microwave method preparation toast baikal skullcap root decoction pieces.Drying method concocting process is relatively easy to control, but concocted time is long,
The microwave processing time is short, obtains processed product effective component extraction rate height, but there is a problem of processing unevenness.
Summary of the invention
The technical problem to be solved in the present invention: how to be contained by the effective component that processing procedure appropriate improves baikal skullcap root decoction pieces
Amount.
In order to solve the above technical problems, the present invention provides technical solution below:
A kind of processing procedure of baikal skullcap root decoction pieces, comprising the following steps:
(1) radix scutellariae complete stool fresh goods is removed into cauline leaf and soil, main root is taken to shine to surface moisture 20~35%；
(2) by radix scutellariae fresh goods using warm water impregnate 15~30min, using 30~60kHz of frequency ultrasonic cleaning 30~
60min is pulled out and is cooled down；
(3) after using 9~15%VOL of alcoholic strength, the yellow rice wine of 60~70g/L of total reducing sugar to impregnate 1~6h the radix scutellariae after net system
Slice drying, 1~2mm of slice thickness；
(4) by after drying scutellaria tablet leaching plus ginger and jujube juice, 30~60min of bored profit, set water proof in container steam 30~
90min takes out drying；
(5) refined honey is diluted by the weight ratio of 1:3~15 with boiled water, the weight ratio of refined honey dilution and radix scutellariae is 1~5:
1, saturating dilution is inhaled to scutellaria tablet, sets and is fried with slow fire buff in pot, with loose tack-free for degree, is collected i.e. after taking out airing
Obtain baikal skullcap root decoction pieces.
Preferably, the temperature that the warm water impregnates is 40~60 DEG C.
Preferably, the ginger and jujube juice the preparation method is as follows:
(1) pure water will be added after rhizoma zingiberis and the slice weighing of dry jujube and impregnates 1~2h；
(2) above-mentioned immersion mixture is boiled into 30~120min, is stirred continuously in boiling part；
(3) it cools down after boiling, is filtered using double gauze, take filtrate to obtain the final product.
It is further preferred that the weight ratio of the rhizoma zingiberis and dry jujube is 2~5:1.
It is further preferred that the weight of the pure water is 5~10 times of the sum of rhizoma zingiberis and dry jujube weight.
Preferably, the temperature of the mild fire is 90~120 DEG C.
Preferably, the drying condition is 50~60 DEG C of 6~10h of drying.
It is that the present invention obtains the utility model has the advantages that
(1) soil and bubble remaining on radix scutellariae can be effectively removed by ultrasonic cleaning, is conducive to improve subsequent yellow rice wine leaching
The efficiency of bubble.
(2) it is processed using rhizoma zingiberis and dry jujube as auxiliary material, effectively enhances radix scutellariae tonifying Qi and lifting yang, Gu table, the work of cold dispelling
With, be conducive to the performance of radix scutellariae warm nature, while can also stopping nausea and vomiting by lowering the adverse flow of QI, the absorption of effective ingredient.
(3) it using honey as efficacy-enhancing ingredient, and is processed with the method for honey toast with synergistic effect, enhancing radix scutellariae tonifying middle-Jiao and Qi
Effect.
(4) the effect of steeping in wine, which processes, can promote radix scutellariae diuretic and maintain drug, apocenosis, expelling pus and promoting granulation, while can inhibit medicinal material surface
Microorganism is infected, and is prevented putrid and deteriorated.
Specific embodiment
Specific embodiments of the present invention will be described in further detail below, to help those skilled in the art couple
Inventive concept of the invention, technical solution have more complete, accurate and deep understanding.
The following is an embodiment of the present invention:
Embodiment 1:
Baikal skullcap root decoction pieces are processed as follows:
(1) radix scutellariae complete stool fresh goods is removed into cauline leaf and soil, main root is taken to shine to surface moisture 35%；
(2) radix scutellariae fresh goods is impregnated into 30min using 40 DEG C of warm water, 30min is cleaned by ultrasonic using frequency 30kHz, is pulled out
It cools down；
(3) it is sliced drying after using alcoholic strength 9%VOL, the yellow rice wine of total reducing sugar 70g/L to impregnate 6h the radix scutellariae after net system, is cut
Piece thickness 1mm；
(4) ginger and jujube juice is prepared:
(A) 15kg pure water will be added after 2kg rhizoma zingiberis and the dry jujube slice weighing of 1kg and impregnates 1h；
(B) above-mentioned immersion mixture is boiled into 30min, is stirred continuously in boiling part；
(C) it cools down after boiling, is filtered using double gauze, take filtrate to obtain the final product.
(5) the scutellaria tablet leaching after drying is added into ginger and jujube juice, bored profit 30min sets water proof in container and steams 90min, takes out 50
DEG C drying 6h；
(6) appearance color is light, viscosity is big, smell faint scent, and sweet honey of various flowers raw honey is heated to 120 DEG C, and water content is 8%
When collect cool down it is spare.
(7) refined honey is diluted by the weight ratio of 1:3 with boiled water, the weight ratio of refined honey dilution and radix scutellariae is 1:1, to radix scutellariae
Piece inhales saturating dilution, sets (90~120 DEG C) of mild fire in pot and fries to brown color, with loose tack-free for degree, collects after taking out airing
Up to baikal skullcap root decoction pieces.
Embodiment 2:
Baikal skullcap root decoction pieces are processed as follows:
(1) radix scutellariae complete stool fresh goods is removed into cauline leaf and soil, main root is taken to shine to surface moisture 20%；
(2) radix scutellariae fresh goods is impregnated into 15min using 60 DEG C of warm water, 60min is cleaned by ultrasonic using frequency 60kHz, is pulled out
It cools down；
(3) it is sliced drying after using alcoholic strength 15%VOL, the yellow rice wine of total reducing sugar 60g/L to impregnate 1h the radix scutellariae after net system, is cut
Piece thickness 2mm；
(4) ginger and jujube juice is prepared:
(A) 10kg pure water will be added after 800g rhizoma zingiberis and the dry jujube slice weighing of 200g and impregnates 2h；
(B) above-mentioned immersion mixture is boiled into 120min, is stirred continuously in boiling part；
(C) it cools down after boiling, is filtered using double gauze, take filtrate to obtain the final product.
(5) the scutellaria tablet leaching after drying is added into ginger and jujube juice, bored profit 60min sets water proof in container and steams 30min, takes out 60
DEG C drying 10h；
(6) appearance color is light, viscosity is big, smell faint scent, and sweet honey of various flowers raw honey is heated to 120 DEG C, and water content exists
Collected when 10% cool down it is spare.
(7) refined honey is diluted by the weight ratio of 1:15 with boiled water, the weight ratio of refined honey dilution and radix scutellariae is 5:1, to Huang
A kind of reed mentioned in ancient books piece inhales saturating dilution, sets (90~120 DEG C) of mild fire in pot and fries to golden yellow, with loose tack-free for degree, receives after taking out airing
It takes up to baikal skullcap root decoction pieces.
Embodiment 3:
Baikal skullcap root decoction pieces are processed as follows:
(1) radix scutellariae complete stool fresh goods is removed into cauline leaf and soil, main root is taken to shine to surface moisture 30%；
(2) radix scutellariae fresh goods is impregnated into 25min using 50 DEG C of warm water, 45min is cleaned by ultrasonic using frequency 45kHz, is pulled out
It cools down；
(3) it is sliced drying after using alcoholic strength 12%VOL, the yellow rice wine of total reducing sugar 65g/L to impregnate 3h the radix scutellariae after net system, is cut
Piece thickness 1.5mm；
(4) ginger and jujube juice is prepared:
(A) 4.8kg pure water will be added after 500g rhizoma zingiberis and the dry jujube slice weighing of 100g and impregnates 1.5h；
(B) above-mentioned immersion mixture is boiled into 80min, is stirred continuously in boiling part；
(C) it cools down after boiling, is filtered using double gauze, take filtrate to obtain the final product.
(5) the scutellaria tablet leaching after drying is added into ginger and jujube juice, bored profit 45min sets water proof in container and steams 60min, takes out 55
DEG C drying 8h；
(6) appearance color is light, viscosity is big, smell faint scent, and sweet honey of various flowers raw honey is heated to 130 DEG C, and water content is 5%
When collect cool down it is spare.
(7) refined honey is diluted by the weight ratio of 1:9 with boiled water, the weight ratio of refined honey dilution and radix scutellariae is 3:1, to radix scutellariae
Piece inhales saturating dilution, sets (90~120 DEG C) of mild fire in pot and fries to buff, with loose tack-free for degree, collects after taking out airing
Up to baikal skullcap root decoction pieces.
In order to detect the content of effective component in baikal skullcap root decoction pieces prepared by the present invention, tested as follows:
Reducing sugar test in baikal skullcap root decoction pieces: precision weigh the baikal skullcap root decoction pieces prepared in embodiment 1-3, common honey toast radix scutellariae and
Raw each l0g of radix scutellariae is diluted to scale to wash in 500m1 measuring bottle, filters.Filtrate moves in buret.Another accurate measurement
Alkaline cupric tartrate test solution l Oml is titrated by the method that pharmacopeia neutral and alkali cupric tartrate test solution is demarcated with sample liquid, and will drop
Determine the content that reduced sugar is calculated as follows in result.
A: every milliliter alkaline cupric tartrate test solution is equivalent to the grams of DEXTROSE ANHYDROUS；
W: the grams of each sample is weighed；
V: ml of sample liquid consumed by titrating.
As a result as follows:
The content of reduced sugar in 1 baikal skullcap root decoction pieces of table
The loss of effective component is less during the present invention processes radix scutellariae as the result is shown for table 1, the Huang of embodiment 1-3 preparation
Active constituent content in a kind of reed mentioned in ancient books medicine materical crude slice is apparently higher than honey toast baikal skullcap root decoction pieces, retains effective component to greatest extent.
The total number of bacteria of baikal skullcap root decoction pieces each sample is measured, storage period mildew, situation of damaging by worms: stores la at room temperature, periodically
Its mildew, situation of damaging by worms is observed, according to the cosmetic variation of each sample, situations such as mildew, moth erosion scores.With the best for 10 points,
Other each sample score respectively as reference.
Experimental result is as follows:
Appearance, total number of bacteria and the store quality situation of 2 baikal skullcap root decoction pieces of table
Table 2 the results show that the present invention, which prepares baikal skullcap root decoction pieces total number of bacteria, is considerably less than control sample, the table in storage period
Now also it is significantly better than control group, mildew and moth erosion situation significantly reduce, and are conducive to the storage and safe handling of radix scutellariae.
In conclusion soil and bubble remaining on radix scutellariae can be effectively removed by ultrasonic cleaning, be conducive to improve subsequent
The efficiency that yellow rice wine impregnates.It is processed using rhizoma zingiberis and dry jujube as auxiliary material, effectively enhances radix scutellariae tonifying Qi and lifting yang, Gu table, cold dispelling
Effect, be conducive to the performance of radix scutellariae warm nature, at the same can also stopping nausea and vomiting by lowering the adverse flow of QI, the absorption of effective ingredient.Using honey conduct
Efficacy-enhancing ingredient, and the effect of there is synergistic effect, enhance radix scutellariae tonifying middle-Jiao and Qi is processed with the method for honey toast.Steeping in wine processing can promote Huang
The effect of a kind of reed mentioned in ancient books diuretic and maintain drug, apocenosis, expelling pus and promoting granulation, while can inhibit infecting for medicinal material surface microorganism, it prevents putrid and deteriorated.
The present invention has that processing step is few simultaneously, easy to operate, can large-scale application the advantages of, mentioned for the processing procedure improvement of radix scutellariae
Important reference is supplied.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement for the various unsubstantialities that the inventive concept and technical scheme of the present invention carry out, or not improved by this
The conception and technical scheme of invention directly apply to other occasions, within the scope of the present invention.Guarantor of the invention
Shield range should be determined by the scope of protection defined in the claims.
Claims (7)
1. a kind of processing procedure of baikal skullcap root decoction pieces, which comprises the following steps:
(1) radix scutellariae complete stool fresh goods is removed into cauline leaf and soil, main root is taken to shine to surface moisture 20~35%；
(2) radix scutellariae fresh goods is impregnated into 15~30min using warm water, 30~60min, fishing is cleaned by ultrasonic using 30~60kHz of frequency
It cools down out；
(3) it is sliced after using 9~15%VOL of alcoholic strength, the yellow rice wine of 60~70g/L of total reducing sugar to impregnate 1~6h the radix scutellariae after net system
Drying, 1~2mm of slice thickness；
(4) the scutellaria tablet leaching after drying is added into ginger and jujube juice, 30~60min of bored profit sets water proof in container and steams 30~90min, takes
It dries out；
(5) refined honey being diluted by the weight ratio of 1:3~15 with boiled water, the weight ratio of refined honey dilution and radix scutellariae is 1~5:1, to
Scutellaria tablet inhales saturating dilution, sets and is fried with slow fire buff in pot, with loose tack-free for degree, collects after taking out airing up to radix scutellariae
Medicine materical crude slice.
2. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 1, it is characterised in that: the temperature that the warm water impregnates
It is 40~60 DEG C.
3. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 1, it is characterised in that: the preparation side of the ginger and jujube juice
Method is as follows:
(1) pure water will be added after rhizoma zingiberis and the slice weighing of dry jujube and impregnates 1~2h；
(2) above-mentioned immersion mixture is boiled into 30~120min, is stirred continuously in boiling part；
(3) it cools down after boiling, is filtered using double gauze, take filtrate to obtain the final product.
4. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 3, it is characterised in that: the weight of the rhizoma zingiberis and dry jujube
Amount is than being 2~5:1.
5. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 3, it is characterised in that: the weight of the pure water is dry
5~10 times of the sum of ginger and dry jujube weight.
6. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 1, it is characterised in that: the temperature of the mild fire is 90
~120 DEG C.
7. a kind of processing procedure of baikal skullcap root decoction pieces according to claim 1, it is characterised in that: the drying condition be 50~
60 DEG C of 6~10h of drying.
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| CN109541071A (en) * | 2018-12-29 | 2019-03-29 | 宁夏明德中药饮片有限公司 | A kind of radix scutellariae preparation process screening technique |
| CN109876036A (en) * | 2019-03-27 | 2019-06-14 | 济南禾宝中药材有限公司 | A kind of baikal skullcap root decoction pieces processing procedure |
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Application publication date: 20181225 |
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| RJ01 | Rejection of invention patent application after publication |