CN103252542B - 电化学放电的纳米颗粒制备方法 - Google Patents
电化学放电的纳米颗粒制备方法 Download PDFInfo
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- CN103252542B CN103252542B CN201310185500.2A CN201310185500A CN103252542B CN 103252542 B CN103252542 B CN 103252542B CN 201310185500 A CN201310185500 A CN 201310185500A CN 103252542 B CN103252542 B CN 103252542B
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- 238000001816 cooling Methods 0.000 claims abstract description 4
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- 238000003487 electrochemical reaction Methods 0.000 claims abstract description 3
- 239000008151 electrolyte solution Substances 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims abstract description 3
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- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 239000012224 working solution Substances 0.000 claims description 7
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 4
- 229910052750 molybdenum Inorganic materials 0.000 claims description 4
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- 238000007599 discharging Methods 0.000 claims description 3
- 239000011810 insulating material Substances 0.000 claims description 3
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical group [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 2
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- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 7
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- 239000000919 ceramic Substances 0.000 description 6
- 239000005543 nano-size silicon particle Substances 0.000 description 6
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- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
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- 239000004065 semiconductor Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
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- 239000012620 biological material Substances 0.000 description 1
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- 239000003054 catalyst Substances 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
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- 238000010892 electric spark Methods 0.000 description 1
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- 239000003344 environmental pollutant Substances 0.000 description 1
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- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
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- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
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- 239000011540 sensing material Substances 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
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- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
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CN201310185500.2A CN103252542B (zh) | 2013-05-20 | 2013-05-20 | 电化学放电的纳米颗粒制备方法 |
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CN201310185500.2A CN103252542B (zh) | 2013-05-20 | 2013-05-20 | 电化学放电的纳米颗粒制备方法 |
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CN103252542A CN103252542A (zh) | 2013-08-21 |
CN103252542B true CN103252542B (zh) | 2015-07-29 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105127525B (zh) * | 2015-09-02 | 2020-06-19 | 广东工业大学 | 一种微电解放电加工工作液及微电解放电加工方法 |
CN108044125B (zh) * | 2017-09-14 | 2021-03-05 | 白银有色集团股份有限公司 | 一种利用液体隔膜放电等离子体制备Ag纳米颗粒的方法 |
CN111889832A (zh) * | 2020-06-28 | 2020-11-06 | 合肥百诺金科技股份有限公司 | 表面洁净和尺寸可控的液相电火花合成银纳米颗粒的方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101607328A (zh) * | 2008-06-17 | 2009-12-23 | 王正尧 | 振动板调律电解装置 |
CN101633065A (zh) * | 2009-07-30 | 2010-01-27 | 南京航空航天大学 | 微尺度脉冲电解射流加工系统及加工方法 |
CN102214817A (zh) * | 2010-04-09 | 2011-10-12 | 清华大学 | 一种碳/硅/碳纳米复合结构负极材料及其制备方法 |
CN102267708A (zh) * | 2011-07-01 | 2011-12-07 | 清华大学 | 一种结晶法制备碳酸锂纳米颗粒的方法 |
CN102603016A (zh) * | 2012-03-08 | 2012-07-25 | 中国科学院苏州纳米技术与纳米仿生研究所 | 纳米氧化镍的制备方法及其应用 |
CN102712464A (zh) * | 2009-09-18 | 2012-10-03 | 阿莫绿色技术有限公司 | 使用交流电电解制备金属纳米颗粒的方法和设备 |
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WO2007001347A2 (en) * | 2004-08-26 | 2007-01-04 | Board Of Trustees Of The University Of Arkansas | Apparatus and method for nano-scale electric discharge machining |
KR20100137308A (ko) * | 2009-06-22 | 2010-12-30 | 삼성전자주식회사 | 질화갈륨 나노 입자의 제조 방법 |
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Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101607328A (zh) * | 2008-06-17 | 2009-12-23 | 王正尧 | 振动板调律电解装置 |
CN101633065A (zh) * | 2009-07-30 | 2010-01-27 | 南京航空航天大学 | 微尺度脉冲电解射流加工系统及加工方法 |
CN102712464A (zh) * | 2009-09-18 | 2012-10-03 | 阿莫绿色技术有限公司 | 使用交流电电解制备金属纳米颗粒的方法和设备 |
CN102214817A (zh) * | 2010-04-09 | 2011-10-12 | 清华大学 | 一种碳/硅/碳纳米复合结构负极材料及其制备方法 |
CN102267708A (zh) * | 2011-07-01 | 2011-12-07 | 清华大学 | 一种结晶法制备碳酸锂纳米颗粒的方法 |
CN102603016A (zh) * | 2012-03-08 | 2012-07-25 | 中国科学院苏州纳米技术与纳米仿生研究所 | 纳米氧化镍的制备方法及其应用 |
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Application publication date: 20130821 Assignee: Jiangsu Liyuan battery material Co., Ltd. Assignor: Nanjing University of Aeronautics and Astronautics Contract record no.: 2016320000203 Denomination of invention: Method for preparing nanometer particles through electrochemistry discharging Granted publication date: 20150729 License type: Exclusive License Record date: 20161027 |
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Effective date of registration: 20180511 Address after: 225002 Tianshan Industrial Concentration Zone, Gaoyou City, Yangzhou, Jiangsu Patentee after: Yangzhou Liqiang lithium electric technology Co., Ltd. Address before: No. 29, Yu Dao Street, Bai Xia District, Nanjing, Jiangsu Patentee before: Nanjing University of Aeronautics and Astronautics |
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Effective date of registration: 20191108 Address after: 211156 No. C-81 Lukou Creative Intelligence Industrial Park, 37 Shenzhou Road, Lukou Street, Jiangning District, Nanjing City, Jiangsu Province Patentee after: Jiangsu Zaichi Technology Co., Ltd. Address before: 225002 Tianshan Industrial Concentration Zone, dianqiao Town, Gaoyou City, Yangzhou City, Jiangsu Province Patentee before: Yangzhou Liqiang lithium electric technology Co., Ltd. |