CN103223700A - 一种氨基模塑料颗粒的造粒工艺 - Google Patents

一种氨基模塑料颗粒的造粒工艺 Download PDF

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CN103223700A
CN103223700A CN2013101198161A CN201310119816A CN103223700A CN 103223700 A CN103223700 A CN 103223700A CN 2013101198161 A CN2013101198161 A CN 2013101198161A CN 201310119816 A CN201310119816 A CN 201310119816A CN 103223700 A CN103223700 A CN 103223700A
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film plastics
amino film
prilling
amino
screw extruder
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CN103223700B (zh
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姚李
卓建平
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JIASHAN ZHONG AO COMPOSITE MATERIAL Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B29C48/04Particle-shaped
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25Component parts, details or accessories; Auxiliary operations
    • B29C48/92Measuring, controlling or regulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92009Measured parameter
    • B29C2948/92114Dimensions
    • B29C2948/92161Volume or quantity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92323Location or phase of measurement
    • B29C2948/92361Extrusion unit
    • B29C2948/9238Feeding, melting, plasticising or pumping zones, e.g. the melt itself
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92504Controlled parameter
    • B29C2948/92609Dimensions
    • B29C2948/92657Volume or quantity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2948/00Indexing scheme relating to extrusion moulding
    • B29C2948/92Measuring, controlling or regulating
    • B29C2948/92819Location or phase of control
    • B29C2948/92828Raw material handling or dosing, e.g. active hopper or feeding device

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

一种氨基模塑料颗粒的造粒工艺,包括以下步骤:a.挤压,将氨基模塑料通过进料阀送入到螺杆挤出机内,由螺杆挤出机加热挤压成块状并输送到轧辊机内;b.冷却,轧辊机将块状的氨基模塑料轧成片状后输送到网带,再进入到冷却设备进行冷却;c.粉碎,冷却后的氨基模塑料从出料阀输出进入到破碎机粉碎成粒;d.包装,粉碎后的颗粒经过分筛机分筛后分批包装。采用本发明所制作的氨基模塑料颗粒物理性能稳定,化学挥发物少,流动性稳定,可保持12-24个月左右,不易破碎。

Description

一种氨基模塑料颗粒的造粒工艺
技术领域
本发明涉及一种氨基模塑料颗粒的造粒工艺。 
背景技术
氨基模塑料(俗称电玉粉)在化工材料领域起到了非常重要的作用,特别是电玉粉成型为颗粒的生产工艺是非常重要的,电玉粉造粒的工艺主要包括捏合、干燥、冷却、破碎和包装,目前国内电玉粉造粒的捏合工艺主要是由尿素.甲醛.木浆.钛白粉等多种原材料经过反应锅捏合反应,此类产品工艺复杂,且需蒸汽和反应锅,物理性能不稳定,化学挥发物多,流动性易变,保质期3-6个月左右;故电玉粉造粒的易流动性能和强度上的不足急需改进,一种新的电玉粉造粒工艺尤其是一种新型的捏合工艺急需出现。 
发明内容
为了克服上述氨基模塑料造粒工艺上所存在的缺陷,本发明所要解决的技术问题是提供一种性能稳定、强度高的氨基模塑料颗粒的制作工艺。 
本发明解决上述技术问题的工艺包括如下步骤: 
一种氨基模塑料颗粒的造粒工艺,包括如下步骤: 
a.挤压,将氨基模塑料通过进料阀送入到螺杆挤出机内,由螺杆挤出机加热挤压成块状并输送到轧辊机内; 
b.冷却,轧辊机将块状的氨基模塑料轧成片状后输送到网带,再进入到冷却设备进行冷却; 
c.粉碎,冷却后的氨基模塑料从出料阀输出进入到破碎机粉碎成粒; 
d.包装,粉碎后的颗粒经过分筛机分筛后分批包装。 
上述的一种氨基模塑料颗粒的造粒工艺,螺杆挤出机的喂料频率为200HZ-800HZ,温度在70°-150°,转速为100rpm/min-400rpm/min,电流在45A-75A。 
上述的一种氨基模塑料颗粒的造粒工艺,轧辊机温度在45°-70°,工作 效率为300KG-1000KG/H,轧辊转速为3000n/min-5000n/min,电流为15A-45A。 
上述的一种氨基模塑料颗粒的造粒工艺,在所述的挤压工序中加入了绝缘增强剂,绝缘增强剂选自橡胶粉、蒙脱土、硅粉、碱性短纤维、热塑性树脂中的一种或几种的混合物。 
上述的一种氨基模塑料颗粒的造粒工艺,在所述挤压工序中加入了复配固化剂,复配固化剂选自固化剂D、草酸、氯化铵、苯磺酸、邻苯二甲酸其中的两种以上的物质。 
本发明的有益效果为:性能稳定,电玉粉经过螺杆机内加温、60-130°高温条件下与自身原料中的固化剂作用发生交联反应,这种反应同时放出水、酸、等低分子物质,通过螺杆机加热平衡温度的控制,使电玉粉在第一次加热时,由挤压捏合放酸的过程,从而来减低物料游离甲醛的浓度,加强物料的韧性,提高物料的密度,使树脂中分子链(线型、带支链)结构的改变,而达到稳定性能的效应;强度高,该物料通过轧辊机由块状轧成片状,通过轧辊机平衡温度加热挤压进一步加强了物料的致密度,光洁度,且由于该物料的密度较高,故不宜挥发,从而稳定了该料的流动性能,延长了物料的保质期,通过两次热效应后,开始冷却物料,进一步保护了该物料的各种物理性能,(流动性、收缩率、热变型温度、冲击强度、吸水性、绝缘电阻等)从而达到提高产品的强度以及稳定流动性的作用。 
附图说明
图1为本发明氨基模塑料造粒的工艺流程图 
具体实施方式
为使对本发明的结构特征及所达成的功效有更进一步的了解和认 识,用以较佳的实施例及附图配合详细的说明,说明如下: 
图1示出了本发明制作氨基模塑料颗粒的工艺流程,主要包括以下几个步骤: 
a.挤压,将氨基模塑料通过进料阀送入到螺杆挤出机内,由螺杆挤出机加热挤压成块状并输送到轧辊机内; 
b.冷却,轧辊机将块状的氨基模塑料轧成片状后输送到网带,再进入到冷却设备进行冷却; 
c.粉碎,冷却后的氨基模塑料从出料阀输出进入到破碎机粉碎成粒。 
d.包装,粉碎后的颗粒经过分筛机分筛后分批包装。 
螺杆挤出机的喂料频率为200HZ-800HZ,温度在70℃-150℃,转速为100rpm/min-400rpm/min,电流在45A-75A。 
轧辊机温度在45°-70°,工作效率为300KG-1000KG/H,轧辊转速为3000n/min-5000n/min,电流为15A-45A。 
电玉粉经过螺杆机内加温、70℃~120℃高温条件下与自身原料中的固化剂作用发生交联反应,这种反应同时放出水、酸、等低分子物质,通过螺杆机加热平衡温度的控制,使电玉粉在第一次加热时,由螺杆挤出机的螺杆挤压捏合放酸的过程,从而来减低物料游离甲醛的浓度,加强物料的韧性,提高物料的密度,使树脂中分子链(线型、带支链)结构的改变,而达到稳定性能的效应。 
该物料通过轧辊机由块状轧成片状,通过轧辊机平衡温度加热挤压进一步加强了物料的致密度,光洁度,且由于该物料的密度较高,故不宜挥发,从而稳定了该料的流动性能,延长了物料的保质期,通过两次热效应后,开始冷却物料,进一步保护了该物料的各种物理性能,(流动性、收缩率、热变型温度、冲击强度、吸水性、绝缘电阻等)从而达到提高产品的强度以及稳定流动性的作用。 
作为本发明的另一种改进,捏合工序中加入了绝缘增强剂,绝缘增强剂选自橡胶粉、蒙脱土、硅粉、碱性短纤维、热塑性树脂中的一种或两种或两种以上的物质。 
作为本发明更进一步的改进,捏合工序中加入了复配固化剂,复配固化剂选自固化剂D、草酸、氯化铵、苯磺酸、邻苯二甲酸其中的两种或两种以上的物质。 
实施例1,在本发明的捏合工序中添加的复配固化剂为固化剂D和氯化铵的组合物,固化剂D与氯化铵的含量比为1.5,添加的绝缘增强剂为橡胶粉和碱性短纤维的混合物,橡胶粉和碱性短纤维的含量比为0.8,螺杆挤出机的捏合温度控制在80℃-115℃,轧辊机的捏合温度控制在45℃-70℃,捏合时间为1.5h,干燥工序对捏合产物进行干燥,控制干燥温度为90℃-100℃,含水量为4%左右。 
实施例2,在本发明的捏合工序中添加的复配固化剂为邻苯二甲酸和氯化铵的组合物,邻苯二甲酸与氯化铵的含量比为1.5,添加的绝缘增强剂为硅粉和碱性短纤维的混合物,硅粉和碱性短纤维的含量比为0.8,螺杆挤出机的捏合温度控制在80℃-115℃,轧辊机的捏合温度控制在45℃-70℃,捏合时间为1.5h,干燥工序对捏合产物进行干燥,控制干燥温度为90℃-100℃,含水量为4%左右。 
以上显示和描述了本发明的基本原理、主要特征和本发明的优点。本行业的技术人员应该了解,本发明不受上述实施例的限制,上述实施例和说明书中描述的只是本发明的原理,在不脱离本发明精神和范围的前提下本发明还会有各种变化和改进,这些变化和改进都落入要求保护的本发明的范围内。本发明要求的保护范围由所附的权利要求书及其等同物界定。 

Claims (5)

1.一种氨基模塑料颗粒的造粒工艺,其特征在于,包括如下步骤:
a.挤压,将氨基模塑料通过进料阀送入到螺杆挤出机内,由螺杆挤出机加热挤压成块状并输送到轧辊机内;
b.冷却,轧辊机将块状的氨基模塑料轧成片状后输送到网带,再进入到冷却设备进行冷却;
c.粉碎,冷却后的氨基模塑料从出料阀输出进入到破碎机粉碎成粒;
d.包装,粉碎后的颗粒经过分筛机分筛后分批包装。
2.根据权利要求1所述的一种氨基模塑料颗粒的造粒工艺,其特征在于,螺杆挤出机的喂料频率为200HZ-800HZ,温度在70°-150°,转速为100rpm/min-400rpm/min,电流在45A-75A。
3.根据权利要求1所述的一种氨基模塑料颗粒的造粒工艺,其特征在于,轧辊机温度在45°-70°,工作效率为300KG-1000KG/H,轧辊转速为3000n/min-5000n/min,电流为15A-45A。
4.根据权利要求1所述的一种氨基模塑料颗粒的造粒工艺,其特征在于,在所述的挤压工序中加入了绝缘增强剂,绝缘增强剂选自橡胶粉、蒙脱土、硅粉、碱性短纤维、热塑性树脂中的一种或几种的混合物。
5.根据权利要求4所述的一种氨基模塑料颗粒的造粒工艺,其特征在于,在所述挤压工序中加入了复配固化剂,复配固化剂选自固化剂D、草酸、氯化铵、苯磺酸、邻苯二甲酸其中两种以上的物质。
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Publication number Priority date Publication date Assignee Title
CN107053517A (zh) * 2017-03-14 2017-08-18 山东高兴新材料股份有限公司 一种复合型氨基模塑料颗粒造粒工艺及设备
CN108908782A (zh) * 2018-06-22 2018-11-30 南京百美塑业有限公司 一种氨基模塑料颗粒的造粒方法
CN111394059A (zh) * 2020-03-29 2020-07-10 连云港中意航空材料有限公司 一种喷砂用树脂砂的制作方法
CN114228202A (zh) * 2021-12-28 2022-03-25 深圳市顺进科技有限公司 一种抛光金属使用治具制作工艺

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107053517A (zh) * 2017-03-14 2017-08-18 山东高兴新材料股份有限公司 一种复合型氨基模塑料颗粒造粒工艺及设备
CN108908782A (zh) * 2018-06-22 2018-11-30 南京百美塑业有限公司 一种氨基模塑料颗粒的造粒方法
CN111394059A (zh) * 2020-03-29 2020-07-10 连云港中意航空材料有限公司 一种喷砂用树脂砂的制作方法
CN114228202A (zh) * 2021-12-28 2022-03-25 深圳市顺进科技有限公司 一种抛光金属使用治具制作工艺

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