CN103221479B - 凝聚无定形含氟聚合物胶乳的方法 - Google Patents

凝聚无定形含氟聚合物胶乳的方法 Download PDF

Info

Publication number
CN103221479B
CN103221479B CN201180055770.0A CN201180055770A CN103221479B CN 103221479 B CN103221479 B CN 103221479B CN 201180055770 A CN201180055770 A CN 201180055770A CN 103221479 B CN103221479 B CN 103221479B
Authority
CN
China
Prior art keywords
latex
particle
amorphous fluoropolymer
inorganic nano
fluoropolymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201180055770.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN103221479A (zh
Inventor
泰里·A·谢费尔宾
埃里克·W·阿代尔
沃纳·M·A·格鲁泰尔特
景乃勇
布兰特·U·科尔布
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
Original Assignee
3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN103221479A publication Critical patent/CN103221479A/zh
Application granted granted Critical
Publication of CN103221479B publication Critical patent/CN103221479B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C08L27/02Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L27/12Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08L27/20Homopolymers or copolymers of hexafluoropropene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/14Treatment of polymer emulsions
    • C08F6/22Coagulation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/16Monomers containing bromine or iodine
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18Monomers containing fluorine
    • C08F214/26Tetrafluoroethene
    • C08F214/262Tetrafluoroethene with fluorinated vinyl ethers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L27/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
    • C08L27/02Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L27/12Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08L27/18Homopolymers or copolymers or tetrafluoroethene

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
CN201180055770.0A 2010-11-18 2011-11-10 凝聚无定形含氟聚合物胶乳的方法 Expired - Fee Related CN103221479B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US41501810P 2010-11-18 2010-11-18
US61/415,018 2010-11-18
PCT/US2011/060170 WO2012067936A2 (en) 2010-11-18 2011-11-10 Method of coagulating an amorphous fluoropolymer latex

Publications (2)

Publication Number Publication Date
CN103221479A CN103221479A (zh) 2013-07-24
CN103221479B true CN103221479B (zh) 2016-06-22

Family

ID=46084576

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180055770.0A Expired - Fee Related CN103221479B (zh) 2010-11-18 2011-11-10 凝聚无定形含氟聚合物胶乳的方法

Country Status (5)

Country Link
US (1) US8969469B2 (enExample)
EP (1) EP2640781B1 (enExample)
JP (1) JP5908921B2 (enExample)
CN (1) CN103221479B (enExample)
WO (1) WO2012067936A2 (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5837619B2 (ja) * 2011-02-04 2015-12-24 スリーエム イノベイティブ プロパティズ カンパニー ジルコニウム酸化物ナノ粒子を含む非晶質ペルフルオロポリマー
EP2920261B1 (en) 2012-11-14 2017-09-13 3M Innovative Properties Company Fluoropolymer coatings suitable for films of photovoltaic modules
CN105814102A (zh) * 2013-12-11 2016-07-27 3M创新有限公司 高度氟化弹性体
WO2018132306A1 (en) 2017-01-10 2018-07-19 Vermeer Manufacturing Company Systems and methods for dosing slurries to remove suspended solids
JP7218859B2 (ja) * 2018-11-28 2023-02-07 Toyo Tire株式会社 ゴム状重合体の製造方法
CN116063608B (zh) * 2022-12-20 2025-08-12 浙江巨化技术中心有限公司 一种含氟聚合物乳液的后处理方法

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1462046A (en) 1973-03-05 1977-01-19 Ici Ltd Coagulated filled fluorocarbon polymer dispersions
US4035565A (en) * 1975-03-27 1977-07-12 E. I. Du Pont De Nemours And Company Fluoropolymer containing a small amount of bromine-containing olefin units
US4153661A (en) 1977-08-25 1979-05-08 Minnesota Mining And Manufacturing Company Method of making polytetrafluoroethylene composite sheet
US4281092A (en) 1978-11-30 1981-07-28 E. I. Du Pont De Nemours And Company Vulcanizable fluorinated copolymers
US4232126A (en) 1978-12-18 1980-11-04 E. I. Du Pont De Nemours And Company Nontacky shaped objects from polymer latices
US4694045A (en) * 1985-12-11 1987-09-15 E. I. Du Pont De Nemours And Company Base resistant fluoroelastomers
US5037579A (en) 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
GB2299098B (en) 1995-03-17 1999-06-16 Campbell Dussek Ltd Water-swellable compositions
DE19544912A1 (de) * 1995-12-01 1997-06-05 Gore W L & Ass Gmbh PTFE-Körper aus mikroporösem Polytetrafluorethylen mit Füllstoff und Verfahren zu dessen Herstellung
GB2319067B (en) 1996-11-06 2000-06-28 T & N Technology Ltd Forming a bearing
US6329058B1 (en) 1998-07-30 2001-12-11 3M Innovative Properties Company Nanosize metal oxide particles for producing transparent metal oxide colloids and ceramers
US6482562B2 (en) 1999-03-10 2002-11-19 Eastman Kodak Company Toner particles of controlled morphology
JP4779280B2 (ja) 1999-09-01 2011-09-28 ダイキン工業株式会社 含フッ素弾性状共重合体組成物の製造方法
WO2001032782A1 (en) 1999-11-04 2001-05-10 Daikin Industries, Ltd. Molded elastomer for semiconductor production apparatus and crosslinkable fluoroelastomer composition
ITMI20021202A1 (it) * 2002-06-04 2003-12-04 Ausimont Spa Composizioni di fluoropolimeri e particelle inorganiche nanometriche
JP3985164B2 (ja) * 2003-09-29 2007-10-03 Toto株式会社 機能性コーティング材及び機能性複合材並びにその製造方法
US20050107544A1 (en) 2003-11-13 2005-05-19 Shuhong Wang Plasma resistant curable fluoroelastomer composition
US20060141015A1 (en) 2004-12-07 2006-06-29 Centre Des Technologies Textiles Antimicrobial material
US7638581B2 (en) * 2004-12-30 2009-12-29 3M Innovative Properties Company Fluoropolymer nanoparticle coating composition
US7241437B2 (en) 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
JP5061446B2 (ja) 2005-03-04 2012-10-31 旭硝子株式会社 含フッ素エラストマーラテックス、その製造方法、含フッ素エラストマーおよび含フッ素ゴム成形品
US7488781B2 (en) 2005-05-25 2009-02-10 Gore Enterprise Holdings, Inc. High purity transparent perfluoroelastomer parts and a process to produce the same
US20060270780A1 (en) 2005-05-25 2006-11-30 Ping Xu High purity perfluoroelastomer composites and a processes to produce the same
ITMI20051397A1 (it) 2005-07-21 2007-01-22 Solvay Solexis Spa Polveri fini di fluoropolimeri
EP1937762B1 (en) * 2005-09-30 2011-06-29 DuPont-Mitsui Fluorochemicals Company, Ltd. A polymer composition with uniformly distributed nano-sized inorganic particles
JP5252612B2 (ja) * 2005-09-30 2013-07-31 三井・デュポンフロロケミカル株式会社 樹脂複合体組成物およびその製造方法
US20080081182A1 (en) * 2006-10-02 2008-04-03 Pham Hoai Nam Fluoropolymer blends with inorganic layered compounds
JP2008115336A (ja) * 2006-11-07 2008-05-22 Du Pont Mitsui Fluorochem Co Ltd 接着性フッ素樹脂複合体組成物
US7956112B2 (en) 2006-12-04 2011-06-07 E. I. Du Pont De Nemours And Company Aqueous fluoropolymer dispersion stabilized with amine oxide surfactant and process for making coagulated fluoropolymer resin
CN101945824B (zh) 2007-12-28 2014-07-23 3M创新有限公司 制备含氧化锆的纳米粒子的方法
US8926081B2 (en) * 2009-06-30 2015-01-06 Hewlett-Packard Development Company, L.P. Ink-jet overcoats including latex polymers and inorganic nano particles

Also Published As

Publication number Publication date
CN103221479A (zh) 2013-07-24
US8969469B2 (en) 2015-03-03
US20130289188A1 (en) 2013-10-31
JP2013543048A (ja) 2013-11-28
WO2012067936A2 (en) 2012-05-24
WO2012067936A3 (en) 2012-08-02
EP2640781A4 (en) 2014-03-26
EP2640781B1 (en) 2016-12-28
JP5908921B2 (ja) 2016-04-26
EP2640781A2 (en) 2013-09-25

Similar Documents

Publication Publication Date Title
CN103221479B (zh) 凝聚无定形含氟聚合物胶乳的方法
CN100404566C (zh) 四氟乙烯聚合物水性分散液、其制造方法、四氟乙烯聚合物粉末以及四氟乙烯聚合物成型体
CN106084104B (zh) 聚四氟乙烯水性分散液的制造方法
EP2638083B1 (en) Reducing the telogenic behavior of hydrocarbon-containing surfactants in aqueous dispersion fluoromonomer polymerization
JP3673475B2 (ja) フッ素含有乳化剤を実質的に含まないフルオロポリマー水性分散液の製造方法
JP6201236B2 (ja) フルオロモノマーの水性重合における核形成
EP3074430B1 (en) Employing polyalkylene oxides for nucleation in aqueous polymerization of fluoromonomer
JP6801660B2 (ja) 変性ポリテトラフルオロエチレンの水性乳化液、ファインパウダーおよび延伸多孔体の製造方法
JP2003522232A (ja) 超清浄なフルオロポリマー
JP6615105B2 (ja) 脂肪族非イオン性界面活性剤で安定化させたテトラフルオロエチレンポリマー分散液
CN102639574A (zh) 聚四氟乙烯水性乳化液及其制造方法、使用该水性乳化液获得的聚四氟乙烯水性分散液、聚四氟乙烯细粉以及拉伸多孔体
TWI530518B (zh) 包含氧化鋯奈米粒子之非晶形全氟聚合物
JP2012513532A (ja) フッ素化イオノマーの核を有するフルオロポリマー粒子
EP2007819A1 (en) Fluoropolymer dispersion purification
CN101652392B (zh) 采用了含氟羧酸化合物的含氟聚合物的制造方法
EP2094784B1 (en) Aqueous fluoropolymer dispersion stabilized with amine oxide surfactant and process for making coagulated fluoropolymer resin
JP2010525149A (ja) 陰イオン交換樹脂およびpH依存性界面活性剤を用いてフルオロポリマー分散物からフッ素化乳化剤を除去するための方法並びにpH依存性界面活性剤を含有するフルオロポリマー分散物
CN115956091A (zh) 改性聚四氟乙烯水性分散液
KR101409098B1 (ko) 미립 중합체에 고체 입자를 분산시키는 방법
TW201430030A (zh) 包含溶劑之過氧化物-可固化之氟聚合物組合物及其使用方法
CN103554560A (zh) 一种原位生成的不饱和脂肪酸锌盐补强天然橡胶的制备方法
WO2012067937A2 (en) Method of coagulating an amorphous fluoropolymer using modified inorganic nanoparticles
WO2020079618A1 (en) Sprayable powder of fluoropolymer particles
CN115340648A (zh) 含氟化二氧化硅纳米颗粒的含氟聚合物的制备方法和含氟橡胶的制备方法
CN101184791A (zh) 含氟聚合物水性分散液及其制造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160622

Termination date: 20191110

CF01 Termination of patent right due to non-payment of annual fee