CN103221339B - 制备过渡金属混合氧化物的前体的方法 - Google Patents

制备过渡金属混合氧化物的前体的方法 Download PDF

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Publication number
CN103221339B
CN103221339B CN201180056226.8A CN201180056226A CN103221339B CN 103221339 B CN103221339 B CN 103221339B CN 201180056226 A CN201180056226 A CN 201180056226A CN 103221339 B CN103221339 B CN 103221339B
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transition metal
aqueous solution
potassium
mixed oxides
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CN103221339A (zh
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M·舒尔茨-多布里克
S·施勒德勒
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/20—Compounds containing manganese, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G45/22—Compounds containing manganese, with or without oxygen or hydrogen, and containing two or more other elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
    • C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621—Binders
    • H01M4/622—Binders being polymers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50—Manufacturing or production processes characterised by the final manufactured product

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CN201180056226.8A 2010-11-25 2011-11-24 制备过渡金属混合氧化物的前体的方法 Active CN103221339B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10192610 2010-11-25
EP10192610.3 2010-11-25
PCT/IB2011/055281 WO2012070012A1 (en) 2010-11-25 2011-11-24 Process for preparing precursors for transition metal mixed oxides

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CN103221339A CN103221339A (zh) 2013-07-24
CN103221339B true CN103221339B (zh) 2015-08-12

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EP (1) EP2457873B1 (cg-RX-API-DMAC7.html)
JP (1) JP6062865B2 (cg-RX-API-DMAC7.html)
KR (1) KR101963103B1 (cg-RX-API-DMAC7.html)
CN (1) CN103221339B (cg-RX-API-DMAC7.html)
TW (1) TW201231403A (cg-RX-API-DMAC7.html)
WO (1) WO2012070012A1 (cg-RX-API-DMAC7.html)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101446491B1 (ko) * 2012-03-16 2014-10-06 주식회사 엘지화학 리튬 복합 전이금속 산화물 제조용 전구체 및 그 제조방법
US10411258B2 (en) 2014-10-08 2019-09-10 Umicore Impurity containing cathode material with preferred morphology and method to prepare from impurity containing metal carbonate
WO2017104688A1 (ja) * 2015-12-15 2017-06-22 株式会社Ｇｓユアサ リチウム二次電池用正極活物質、正極活物質の前駆体の製造方法、正極活物質の製造方法、リチウム二次電池用正極及びリチウム二次電池
US12155103B2 (en) * 2019-03-20 2024-11-26 The Regents Of The University Of Colorado, A Body Corporate Electrochemical storage devices comprising chelated metals
CN111434617B (zh) * 2019-12-27 2022-05-27 蜂巢能源科技有限公司 铝包覆前驱体及其制备方法和应用
JP7661675B2 (ja) * 2020-02-25 2025-04-15 住友金属鉱山株式会社 リチウムイオン二次電池用正極活物質前駆体およびその製造方法、リチウムイオン二次電池用正極活物質およびその製造方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1396672A (zh) * 2002-07-26 2003-02-12 厦门大学 熔融碳酸盐燃料电池中多孔镍基阴极材料的表面改性方法
WO2006023092A2 (en) * 2004-07-30 2006-03-02 University Of Chicago Method and apparatus for preparation of spherical metal carbonates and lithium metal oxides for lithium rechargeable batteries
US20090226811A1 (en) * 2008-02-27 2009-09-10 Nippon Chemical Industrial Co., Ltd. Lithium nickel manganese cobalt composite oxide used as cathode active material for lithium rechargeable battery, manufacturing method thereof, and lithium rechargeable battery

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JP2001148249A (ja) * 1999-11-19 2001-05-29 Chuo Denki Kogyo Co Ltd リチウム二次電池用正極活物質材料とリチウム二次電池
WO2002041419A1 (en) * 2000-11-20 2002-05-23 Chuo Denki Kogyo Co., Ltd. Nonaqueous electrolyte secondary cell and positive electrode active material
US7205072B2 (en) * 2002-11-01 2007-04-17 The University Of Chicago Layered cathode materials for lithium ion rechargeable batteries
TWI279019B (en) * 2003-01-08 2007-04-11 Nikko Materials Co Ltd Material for lithium secondary battery positive electrode and manufacturing method thereof
US8062792B2 (en) * 2005-04-26 2011-11-22 Uchicago Argonne Llc Processes for making dense, spherical active materials for lithium-ion cells
JP4768562B2 (ja) * 2005-09-27 2011-09-07 石原産業株式会社 リチウム・遷移金属複合酸化物及びその製造方法並びにそれを用いてなるリチウム電池
JP4968945B2 (ja) 2008-02-01 2012-07-04 日本化学工業株式会社 複合炭酸塩およびその製造方法
JP4968944B2 (ja) 2008-02-01 2012-07-04 日本化学工業株式会社 複合炭酸塩およびその製造方法
US8465873B2 (en) * 2008-12-11 2013-06-18 Envia Systems, Inc. Positive electrode materials for high discharge capacity lithium ion batteries

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1396672A (zh) * 2002-07-26 2003-02-12 厦门大学 熔融碳酸盐燃料电池中多孔镍基阴极材料的表面改性方法
WO2006023092A2 (en) * 2004-07-30 2006-03-02 University Of Chicago Method and apparatus for preparation of spherical metal carbonates and lithium metal oxides for lithium rechargeable batteries
US20090226811A1 (en) * 2008-02-27 2009-09-10 Nippon Chemical Industrial Co., Ltd. Lithium nickel manganese cobalt composite oxide used as cathode active material for lithium rechargeable battery, manufacturing method thereof, and lithium rechargeable battery

Also Published As

Publication number Publication date
JP6062865B2 (ja) 2017-01-18
CN103221339A (zh) 2013-07-24
TW201231403A (en) 2012-08-01
JP2014503451A (ja) 2014-02-13
KR20130133797A (ko) 2013-12-09
WO2012070012A1 (en) 2012-05-31
KR101963103B1 (ko) 2019-03-28
EP2457873A1 (de) 2012-05-30
EP2457873B1 (de) 2018-10-31

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