CN103201253B - 纯化由气相加氢获得的苯胺的方法 - Google Patents

纯化由气相加氢获得的苯胺的方法 Download PDF

Info

Publication number
CN103201253B
CN103201253B CN201180050920.9A CN201180050920A CN103201253B CN 103201253 B CN103201253 B CN 103201253B CN 201180050920 A CN201180050920 A CN 201180050920A CN 103201253 B CN103201253 B CN 103201253B
Authority
CN
China
Prior art keywords
water
stream
aniline
product
distillation tower
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201180050920.9A
Other languages
English (en)
Chinese (zh)
Other versions
CN103201253A (zh
Inventor
P·莱纳
K·萨默
A·S·穆萨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covestro Deutschland AG
Original Assignee
Bayer Pharma AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Pharma AG filed Critical Bayer Pharma AG
Publication of CN103201253A publication Critical patent/CN103201253A/zh
Application granted granted Critical
Publication of CN103201253B publication Critical patent/CN103201253B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/86Separation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/45Monoamines
    • C07C211/46Aniline

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201180050920.9A 2010-10-21 2011-10-17 纯化由气相加氢获得的苯胺的方法 Active CN103201253B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010042731A DE102010042731A1 (de) 2010-10-21 2010-10-21 Verfahren zur Reinigung von Anilin aus Gasphasenhydrierungen
DE102010042731.4 2010-10-21
PCT/EP2011/068122 WO2012052407A1 (de) 2010-10-21 2011-10-17 Verfahren zur reinigung von anilin aus gasphasenhydrierungen

Publications (2)

Publication Number Publication Date
CN103201253A CN103201253A (zh) 2013-07-10
CN103201253B true CN103201253B (zh) 2014-12-03

Family

ID=44860336

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201180050920.9A Active CN103201253B (zh) 2010-10-21 2011-10-17 纯化由气相加氢获得的苯胺的方法

Country Status (9)

Country Link
US (1) US9233910B2 (enExample)
EP (1) EP2630117B1 (enExample)
JP (1) JP5951618B2 (enExample)
KR (1) KR101869996B1 (enExample)
CN (1) CN103201253B (enExample)
DE (1) DE102010042731A1 (enExample)
PL (1) PL2630117T3 (enExample)
PT (1) PT2630117E (enExample)
WO (1) WO2012052407A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2641892A1 (de) * 2012-03-23 2013-09-25 Bayer MaterialScience AG Verfahren zur Reinigung von Anilin aus Gasphasenhydrierungen
WO2014057053A1 (de) * 2012-10-11 2014-04-17 Basf Se Verfahren zur gewinnung von rein-anilin
US9115049B2 (en) * 2012-10-11 2015-08-25 Basf Se Process for obtaining pure aniline
CN110627651B (zh) * 2018-06-25 2022-06-14 中国石油化工股份有限公司 一种降低苯胺中苯酚含量的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101024615A (zh) * 2006-02-18 2007-08-29 拜尔材料科学股份公司 制备苯胺的方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2174008A (en) * 1938-01-29 1939-09-26 Nat Aniline & Chem Co Inc Distillation of amines from reduction masses
JPS4935341A (enExample) 1972-07-31 1974-04-01
DE4428017A1 (de) 1994-08-08 1996-02-15 Bayer Ag Verfahren zur Herstellung von aromatischen Aminen
DE4428018A1 (de) * 1994-08-08 1996-02-15 Bayer Ag Verfahren zur Herstellung von aromatischen Aminen
JP3804082B2 (ja) 1995-04-27 2006-08-02 住友化学株式会社 アニリンの精製方法
JPH0935341A (ja) 1995-07-18 1997-02-07 Masayuki Matsuda X線による情報の記録・読み出し方法
JP2001226320A (ja) * 2000-02-14 2001-08-21 Nippon Shokubai Co Ltd アクリル酸の捕集方法およびアクリル酸の精製方法
US7049471B2 (en) 2003-10-10 2006-05-23 E. I. Du Pont De Nemours And Company Separation of amine from a phenolic compound
DE102004026626A1 (de) 2004-06-01 2005-12-29 Bayer Materialscience Ag Verfahren zur destillativen Trennung von wässrigen Aminlösungen
JP2005350388A (ja) 2004-06-10 2005-12-22 Sumitomo Chemical Co Ltd アニリンの製造方法
JP4552941B2 (ja) 2006-01-17 2010-09-29 住友化学株式会社 アニリンの精製方法および製造方法
DE102006007620A1 (de) 2006-02-18 2007-08-23 Bayer Materialscience Ag Verfahren zur Herstellung von Anilin
DE102006035203A1 (de) 2006-07-29 2008-01-31 Bayer Materialscience Ag Verfahren zur Herstellung von aromatischen Aminen
JP2008184409A (ja) * 2007-01-29 2008-08-14 Mitsubishi Rayon Co Ltd アルキルアミン含有混合物の蒸留法及びアルキルアミン類の製造方法
DE102007039091A1 (de) 2007-08-18 2009-02-19 Bayer Materialscience Ag Verfahren zur Reinigung von aromatischen Aminen
WO2012052411A1 (de) * 2010-10-21 2012-04-26 Bayer Technology Services Gmbh Verfahren zur vereinfachten abtrennung eines reaktionsprodukts aus reaktionsgasgemischen mittels mindestens zweimaliger teilweiser kondensation

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101024615A (zh) * 2006-02-18 2007-08-29 拜尔材料科学股份公司 制备苯胺的方法

Also Published As

Publication number Publication date
PL2630117T3 (pl) 2015-03-31
JP5951618B2 (ja) 2016-07-13
PT2630117E (pt) 2015-02-17
EP2630117B1 (de) 2014-10-15
US20140046096A1 (en) 2014-02-13
US9233910B2 (en) 2016-01-12
WO2012052407A1 (de) 2012-04-26
EP2630117A1 (de) 2013-08-28
DE102010042731A1 (de) 2012-04-26
CN103201253A (zh) 2013-07-10
KR101869996B1 (ko) 2018-06-22
KR20130127983A (ko) 2013-11-25
JP2013543517A (ja) 2013-12-05

Similar Documents

Publication Publication Date Title
KR101376940B1 (ko) 아닐린의 제조 방법
JP5204413B2 (ja) アニリンの製造方法
JP2018016628A (ja) 低沸点成分の分離、ならびに部分凝縮によるイソホロンジアミンにおけるアンモニア含分の低下
TW200914403A (en) Process for the purification of aromatic amines
WO2014001461A1 (en) Process for the production of a mixture comprising cyclohexanone and cyclohexanol from phenol
JP2013535478A (ja) ニトロベンゼンの連続製造方法
EA016277B1 (ru) Способ получения циклогексанона с многократной постдистилляцией
JP4773138B2 (ja) アミン水溶液の蒸留分離法
CN103201253B (zh) 纯化由气相加氢获得的苯胺的方法
JP2015522636A (ja) 断熱的ニトロ化によりニトロベンゼンを製造する方法
JP6284933B2 (ja) メチルブチノールの製造方法
JP6165844B2 (ja) 芳香族アミンを含む物質混合物、特に粗製アニリンの物質混合物の処理方法
JP2018527370A (ja) フェノールの精製方法
JP6062527B2 (ja) 気相水素化からのアニリンの精製方法
RU2508287C2 (ru) Химическая установка
JP7663521B2 (ja) アニリンの精製方法
RU2167145C1 (ru) Способ очистки технического нитробензола от серосодержащих, азот- и кислородсодержащих побочных продуктов

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20160525

Address after: Leverkusen, Germany

Patentee after: BAYER MATERIALSCIENCE AG

Address before: German Monheim

Patentee before: Bayer Pharma Aktiengesellschaft