CN103044233A - 一种球磨制备硬脂酸盐的工艺 - Google Patents
一种球磨制备硬脂酸盐的工艺 Download PDFInfo
- Publication number
- CN103044233A CN103044233A CN2012105513071A CN201210551307A CN103044233A CN 103044233 A CN103044233 A CN 103044233A CN 2012105513071 A CN2012105513071 A CN 2012105513071A CN 201210551307 A CN201210551307 A CN 201210551307A CN 103044233 A CN103044233 A CN 103044233A
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- CN
- China
- Prior art keywords
- stearate
- ball milling
- oxide
- stearic acid
- technique
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 title claims abstract description 45
- 238000000498 ball milling Methods 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 238000000034 method Methods 0.000 claims abstract description 26
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 16
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000008117 stearic acid Substances 0.000 claims abstract description 16
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 13
- 150000004706 metal oxides Chemical class 0.000 claims abstract description 13
- 229910000000 metal hydroxide Inorganic materials 0.000 claims abstract description 8
- 150000004692 metal hydroxides Chemical class 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 239000003054 catalyst Substances 0.000 claims abstract description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 7
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 229910021518 metal oxyhydroxide Inorganic materials 0.000 claims description 5
- 238000013022 venting Methods 0.000 claims description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims description 4
- -1 hydrated barta Chemical compound 0.000 claims description 4
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 claims description 4
- XXQBEVHPUKOQEO-UHFFFAOYSA-N potassium superoxide Chemical compound [K+].[K+].[O-][O-] XXQBEVHPUKOQEO-UHFFFAOYSA-N 0.000 claims description 4
- 238000012545 processing Methods 0.000 claims description 4
- 229960000583 acetic acid Drugs 0.000 claims description 3
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 3
- 239000000920 calcium hydroxide Substances 0.000 claims description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 3
- 229910021514 lead(II) hydroxide Inorganic materials 0.000 claims description 3
- 239000011787 zinc oxide Substances 0.000 claims description 3
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 2
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 2
- 239000004327 boric acid Substances 0.000 claims description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000292 calcium oxide Substances 0.000 claims description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 2
- 239000012362 glacial acetic acid Substances 0.000 claims description 2
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 2
- 239000000347 magnesium hydroxide Substances 0.000 claims description 2
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 2
- 239000000395 magnesium oxide Substances 0.000 claims description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 2
- PFUVRDFDKPNGAV-UHFFFAOYSA-N sodium peroxide Chemical compound [Na+].[Na+].[O-][O-] PFUVRDFDKPNGAV-UHFFFAOYSA-N 0.000 claims description 2
- UGZADUVQMDAIAO-UHFFFAOYSA-L zinc hydroxide Chemical compound [OH-].[OH-].[Zn+2] UGZADUVQMDAIAO-UHFFFAOYSA-L 0.000 claims description 2
- 229910021511 zinc hydroxide Inorganic materials 0.000 claims description 2
- 229940007718 zinc hydroxide Drugs 0.000 claims description 2
- 238000002156 mixing Methods 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 3
- 230000007547 defect Effects 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 230000004580 weight loss Effects 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000005265 energy consumption Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 229910017053 inorganic salt Inorganic materials 0.000 description 2
- ONUFRYFLRFLSOM-UHFFFAOYSA-N lead;octadecanoic acid Chemical compound [Pb].CCCCCCCCCCCCCCCCCC(O)=O ONUFRYFLRFLSOM-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 239000002351 wastewater Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- AGXUVMPSUKZYDT-UHFFFAOYSA-L barium(2+);octadecanoate Chemical compound [Ba+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O AGXUVMPSUKZYDT-UHFFFAOYSA-L 0.000 description 1
- OTNKRKHMTFRPSK-UHFFFAOYSA-N barium;octadecanoic acid Chemical compound [Ba].CCCCCCCCCCCCCCCCCC(O)=O OTNKRKHMTFRPSK-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000008116 calcium stearate Substances 0.000 description 1
- 235000013539 calcium stearate Nutrition 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000008406 cosmetic ingredient Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 229910000765 intermetallic Inorganic materials 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000001404 mediated effect Effects 0.000 description 1
- 238000005649 metathesis reaction Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- XIVNZHXRIPJOIZ-UHFFFAOYSA-N octadecanoic acid;zinc Chemical compound [Zn].CCCCCCCCCCCCCCCCCC(O)=O XIVNZHXRIPJOIZ-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Lubricants (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CN201210551307.1A CN103044233B (zh) | 2012-12-17 | 2012-12-17 | 一种球磨制备硬脂酸盐的工艺 |
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CN201210551307.1A CN103044233B (zh) | 2012-12-17 | 2012-12-17 | 一种球磨制备硬脂酸盐的工艺 |
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CN103044233A true CN103044233A (zh) | 2013-04-17 |
CN103044233B CN103044233B (zh) | 2014-11-12 |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104387257A (zh) * | 2014-12-11 | 2015-03-04 | 东莞市汉维新材料科技有限公司 | 硬脂酸锂的制备方法 |
CN104910005A (zh) * | 2015-06-17 | 2015-09-16 | 德清县维康生物科技有限公司 | 一种用于药物制剂中的硬脂酸镁及制备方法 |
CN104926640A (zh) * | 2015-06-17 | 2015-09-23 | 德清县维康生物科技有限公司 | 一种硬脂酸锌及制备方法 |
CN104926641A (zh) * | 2015-06-17 | 2015-09-23 | 德清县维康生物科技有限公司 | 一种硬脂酸钙及制备方法 |
CN106278872A (zh) * | 2016-08-24 | 2017-01-04 | 上海制皂(集团)如皋有限公司 | 干法生产硬脂酸锌的新型生产工艺 |
CN110156588A (zh) * | 2019-06-28 | 2019-08-23 | 常州大学 | 一种纳米有机金属羧酸盐的制备方法 |
WO2020248483A1 (zh) * | 2019-06-11 | 2020-12-17 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004072011A1 (en) * | 2003-02-05 | 2004-08-26 | Crompton Corporation | Process for preparing fatty acid zinc salts |
-
2012
- 2012-12-17 CN CN201210551307.1A patent/CN103044233B/zh not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004072011A1 (en) * | 2003-02-05 | 2004-08-26 | Crompton Corporation | Process for preparing fatty acid zinc salts |
Non-Patent Citations (1)
Title |
---|
高喆等: ""高能球磨法制备氧化锆-硬脂酸系相变储能材料"", 《武汉理工大学学报》, vol. 29, no. 10, 31 October 2007 (2007-10-31), pages 83 - 88 * |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104387257A (zh) * | 2014-12-11 | 2015-03-04 | 东莞市汉维新材料科技有限公司 | 硬脂酸锂的制备方法 |
CN104387257B (zh) * | 2014-12-11 | 2017-03-15 | 东莞市汉维科技股份有限公司 | 硬脂酸锂的制备方法 |
CN104910005A (zh) * | 2015-06-17 | 2015-09-16 | 德清县维康生物科技有限公司 | 一种用于药物制剂中的硬脂酸镁及制备方法 |
CN104926640A (zh) * | 2015-06-17 | 2015-09-23 | 德清县维康生物科技有限公司 | 一种硬脂酸锌及制备方法 |
CN104926641A (zh) * | 2015-06-17 | 2015-09-23 | 德清县维康生物科技有限公司 | 一种硬脂酸钙及制备方法 |
CN106278872A (zh) * | 2016-08-24 | 2017-01-04 | 上海制皂(集团)如皋有限公司 | 干法生产硬脂酸锌的新型生产工艺 |
WO2020248483A1 (zh) * | 2019-06-11 | 2020-12-17 | 东莞市汉维科技股份有限公司 | 一种硬脂酸盐的制备工艺 |
CN110156588A (zh) * | 2019-06-28 | 2019-08-23 | 常州大学 | 一种纳米有机金属羧酸盐的制备方法 |
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Publication number | Publication date |
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CN103044233B (zh) | 2014-11-12 |
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Address after: Linjiang Industrial Park in Xiaoshan District of Hangzhou City, Zhejiang Province, on a road 311228 Patentee after: HANGZHOU OLEOCHEMICALS CO.,LTD. Patentee after: ZANYU TECHNOLOGY GROUP CO.,LTD. Address before: Linjiang Industrial Park in Xiaoshan District of Hangzhou City, Zhejiang Province, on a road 311228 Patentee before: HANGZHOU OLEOCHEMICALS CO.,LTD. Patentee before: ZHEJIANG ZANYU TECHNOLOGY Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20141112 |
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CF01 | Termination of patent right due to non-payment of annual fee |