CN102836103B - Bamboo charcoal facial cleanser - Google Patents
Bamboo charcoal facial cleanser Download PDFInfo
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- CN102836103B CN102836103B CN201210357555.2A CN201210357555A CN102836103B CN 102836103 B CN102836103 B CN 102836103B CN 201210357555 A CN201210357555 A CN 201210357555A CN 102836103 B CN102836103 B CN 102836103B
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Abstract
The invention relates to a bamboo charcoal facial cleanser, which belongs to the field of life of cosmetics. The bamboo charcoal facial cleanser is composed of the following components by weight: 1 to 8 parts of nano bamboo charcoal powder, 1.5 to 2 parts of sodium alginate, 0.3 to 0.8 parts of alkyl glycoside, 2 to 3 parts of jojoba oil, 0.5 to 1.8 parts of squalane, 0.5 to 0.8 parts of preservative, 3 to 5 parts of glycerol, 30 to 40 parts of tea extract, 40 to 50 parts of de-ionized water and a decoction; the decoction is obtained by extracting the following components by weight through a decoction process, namely 5 to 10 parts of oat powder, 3 to 5 parts of semen sesami nigrum, 5 to 10 parts of soybeans, 4 to 6 parts of bletilla striata and 3 to 5 parts of angelica sinensis powder. The facial cleanser provided by the invention is capable of effectively cleansing the faces, ensuring the skin to keep moist, strengthening oxidation resistance and antianaphylaxis of the skin.
Description
Technical field
The present invention relates to a kind of bamboo charcoal facial milk cleanser, belong to household chemicals field.
Background technology
If existing cleansing milk is made by the synthetic wetting agent of more single surfactant compound as cleansing milk Bian in the market, thereby reach the object of decontamination.Owing to having used a large amount of surfactants, easily cause the undue defat of epiderm skin, thereby make skin drier, more serious meeting causes the irreversibility infringement to skin, and function singleness, cannot meet the demand of user to the multiple efficacies of skin care.
CN101427987(2010-12-15) provide a kind of face cleaning skin lotion product and preparation method thereof, yet this product forms by purifying frost and cleaning agent, use inconvenient, and its clean-up performance, performance of keeping humidity and the effect of skin non-oxidizability and antiallergic is all had much room for improvement.
Summary of the invention
The object of this invention is to provide and a kind ofly can effectively clean face, guarantee the bamboo charcoal facial milk cleanser that skin keeps moistening, strengthens skin non-oxidizability and antiallergic.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs: a kind of bamboo charcoal facial milk cleanser, and its one-tenth by following weight portion is grouped into: 1-8 part nano bamboo powdered carbon, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part, deionized water 40-50 part and decoction liquor; Described decoction liquor is extracted and is obtained by decocting method by the composition of following parts by weight: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part.
Alkyl polyglucoside is a kind of non-ionic surface active agent of gentle environmental protection.Sodium alginate is the polysaccharide-sodium alginate that is derived from Sargassum, easily forms gel.
Nano bamboo powdered carbon has the super large surface area of extremely strong absorption property, be particularly suitable for being used in beauty and skin care field, and apply at facial zone after other combinations of substances, can play massage effect, its infrared effect can be played magnetic therapy radiation effects to eye, helps blood circulation promoting; Squalane can suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, to strengthening skin non-oxidizability and elasticity, has obvious physiologic effect; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in tea juice, can keep skin moistening.Jojoba oil main component is unsaturated higher alcohol and fatty acid, has good stability, very easily merges with skin, has non-oxidizability free from worldly cares.In addition, Jojoba oil also contains and enriches vitamin, has the effect of nourishing softening skin and keeping skin wet.
In decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, is especially applicable to sensitivity skin; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium being rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care, can prevent pachylosis and aging, contributes to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can strengthen skin non-oxidizability and antiallergic.The decoction liquor forming according to each umber proportioning of the present invention, can effectively eliminate eye pouch and black eye.
The present invention fully utilizes gel emulsification and the moisture-keeping function of sodium alginate and alkyl polyglucoside mixture, and mix with nano bamboo powdered carbon of the present invention, decoction liquor and tea juice, through crowd's trial effect, prove, can effectively clean facial in, guarantee that skin keeps moistening, strengthens skin non-oxidizability and antiallergic.
As preferably, described antiseptic is sorbic acid or sodium diacetate.
As preferably, described bamboo charcoal powder makes by the following method:
1., in vertical moving bed, from top, add the bamboo of splitting broken and preliminarily dried through blocking, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces is dried bamboo and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged and is entered Bamboo vinegar solution condenser from top, and condensation obtains Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out staged intensification, make the combustion zone that experiences in bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2. the bamboo charcoal, upper step being made is prepared nano bamboo powdered carbon.
More preferably, the particle diameter 100-200nm of described bamboo charcoal powder.
As preferably, described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid.
As preferably, in described tea juice, include Radix Hamamelidis Mollis and Folium Camelliae sinensis that weight ratio is 1:4-9.
As preferably, the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, by the weight ratio of 1:4-9, mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
By decocting method of the present invention, can fully utilize the non-oxidizability of Radix Hamamelidis Mollis and tea juice, help skin to mend wet and quiet flesh.
More preferably, described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in described step (2), the solids concentration of the first concentrated solution is 15%-20%, and the solids concentration of the second concentrated solution is 33%-35%.
Because the excessive concentration of the first concentrated solution is the overlong time of reverse osmosis, fragrance is worsened, the too low vacuum concentration overlong time that makes next step of concentration, also brown stain and fragrance is oxidized, the excessive concentration of the second concentrated solution is vacuum concentration overlong time, and concentration is too low can not get enough products.
More preferably, the temperature while concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
The present invention is according to following scheme implementation:
A), the preparation of decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
B), the preparation of bamboo charcoal facial milk cleanser: take by weight step a) gained decoction liquor, 1-8 part nano bamboo powdered carbon, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part and deionized water 40-50 part; All substances are mixed and stirring and emulsifying, then carry out microwave vacuum processing and obtain bamboo charcoal facial milk cleanser.
As preferably, the microwave vacuum treatment conditions of described step b) are: will after all substances mixing and emulsifying, send in microwave vacuum tank, then carry out evacuation process to vacuum be-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
By microwave vacuum of the present invention, process, there is heat effect and non-thermal effect in each component simultaneously, during carry out microwave radiation heating, electromagnetic field in microwave is with several hundred million even billions of inferior frequency inverted directions per second, make polarization and this polarization of the different electric charges of material internal not possess the ability of catching up with rapidly alternating electric field, cause material internal friction and generate heat, i.e. so-called " interior heating ", each component in facial film is blended mutually, emulsifying is uniform and complete more, and may there are some other reactions, finally make facial milk cleanser of the present invention play massage face, effectively clean face, guarantee that skin keeps moistening, strengthen the function of skin non-oxidizability and antiallergic.
Accompanying drawing explanation
Fig. 1 is the temperature control system schematic diagram of the vertical moving bed of bamboo charcoal carbonization of the present invention.
In figure, A-dry section; The pre-char zone of B-; C-char zone; D-calcining zone; E-cooling zone; F-is with the temperature sensing device of CPU; D1/d2/d3-oxidizer entrance hole; T1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed that bamboo charcoal powder preparation is used is divided into dry section A, pre-char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D mono-side is distributed with many oxidizer entrance holes that can regulate closure or openness, as d1, d2, d3 etc., opposite side is to having the point for measuring temperature at each aperture place as t1, t2, t3 etc., and each aperture place temperature shows by the temperature sensing device F being connected with this point for measuring temperature.
Embodiment mono-
Bamboo charcoal powder preparation: carry out pilot scale in vertical moving bed dry distillation carbonizing furnace, bamboo chip (being about 36cm) with average moisture content 39%, the temperature of each point for measuring temperature, dry section A is 150 ℃, pre-char zone B is 275 ℃, char zone C is 450 ℃, during intensification, observe the temperature of the district of D shown in Fig. 1 combustion zone diverse location, when somewhere, combustion zone is as too low in the temperature of d2, open the aperture at this place, importing air locally burns, this place's temperature is raise, control the combustion zone temperature that experiences in bamboo folding process and be warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then from 700 ℃, be warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 40 ℃.Continuous operation takes out bamboo charcoal after 10 days (not comprising the warm stove time).Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.Then prepared by the bamboo charcoal making to the powdered carbon of particle diameter 100nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is that mass ratio is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtain the first concentrated solution of solid contents 5%; Half of getting the first concentrated solution be at 40 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 30%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take oatmeal 5kg, Semen Sesami Nigrum 3kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4kg, Radix Angelicae Sinensis powder 3kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 30%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 5kg nano bamboo powdered carbon, sodium alginate 1.9kg, alkyl polyglucoside 0.7kg, Jojoba oil 2.3kg, squalane 0.5kg, sorbic acid 0.5kg, glycerol 3.5kg, tea juice 33kg, deionized water 48kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying, then carry out microwave vacuum processing: the material after stirring and emulsifying is sent in microwave vacuum tank, then carry out evacuation process to vacuum be-0.09MPa; Carry out microwave treatment, microwave frequency is 245MHz again, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains bamboo charcoal facial milk cleanser.
Cleansing milk provided by the invention is checked through PLA Air Force General Hospital, and experimenter is totally 100 people, male 8 people wherein, female 92 people, age 18-62 one full year of life.Using method is: experimenter directly uses and is subject to trial product, every day, each used once sooner or later, used Qian Jiang face to drench with clear water, extruded appropriate cleansing milk of the present invention in the centre of the palm, add a small amount of clear water to rub and enrich foam, at face message, with clear water, rinse well in a moment.Adhere to using one month, at least check once and have or not whole body and local untoward reaction to understand weekly, and itemized record result.
Use the effect of embodiment 1 compositions:
Experimenter is totally 25 people, male 2 people wherein, female 23 people.Use after one month; experimenter all represents to use the salubrious non-greasy of face after embodiment 1 compositions, can effectively clean dirt; and that skin keeps is for a long time moistening, clearly compact and high resilience, face mask lines are than more clear clearly demarcated before using, the good in oxidation resistance of skin after using; There is local skin untoward reaction in the equal end of experimenter, also, without little good reactions of whole body such as anorexia, diarrhoea, weak, endocrine regulations, after using, the antiallergic of skin is good.
Embodiment bis-
The preparation of bamboo charcoal powder: carry out pilot scale in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, ancestor's bamboo chip in the Meng (being about 40cm) with average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃, pre-char zone B is 270 ℃, char zone C is 500 ℃, during intensification, from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion, burn simultaneously, make combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min, and then from 750 ℃, be warming up to 1500 ℃ and be incubated 8h with the speed of 15 ℃/min, in 1500 ℃ of districts, spray into steam 60min, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 30 ℃.Continuous operation takes out bamboo charcoal after 8 days (not comprising the warm stove time), the solution of the bamboo charcoal of taking-up being put into acid content 4% soaks 2h, takes out with clear water and cleans, and then puts into and dries kiln drying 1h.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.Then by the powdered carbon of the bamboo charcoal preparation grain 120nm making.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2.5 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain the first concentrated solution of solid contents 20%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 33%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take oatmeal 10kg, Semen Sesami Nigrum 5kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 2kg nano bamboo powdered carbon, sodium alginate 1.8kg, alkyl polyglucoside 0.5kg, Jojoba oil 2.5kg, squalane 1kg, sodium diacetate 0.6kg, glycerol 4kg, tea juice 35kg, deionized water 45kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying, then carry out microwave vacuum processing: the material after stirring and emulsifying is sent in microwave vacuum tank, then carry out evacuation process to vacuum be-0.06MPa; Carry out microwave treatment, microwave frequency is 400MHz again, and microwave treatment time is 1min, and discharging is cooled to room temperature and obtains bamboo charcoal facial milk cleanser.
Test method, with embodiment mono-, is used the effect of embodiment 2 compositionss:
Experimenter is totally 25 people, male 2 people wherein, female 23 people.Using after one month, all there is not local skin untoward reaction in experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 22 experimenters represent to use the salubrious non-greasy of face after embodiment 2 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and face mask lines are than more clear clearly demarcated before using; 3 subject perception have massage and whitening effect while washing one's face, but effect is obvious not.
Embodiment tri-
The preparation of bamboo charcoal powder is with embodiment mono-.Then prepared by the bamboo charcoal making to the bamboo charcoal powder of particle diameter 150nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 1.5 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain the first concentrated solution of solid contents 15%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take oatmeal 8kg, Semen Sesami Nigrum 4kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 8kg nano bamboo powdered carbon, sodium alginate 2kg, alkyl polyglucoside 0.8kg, Jojoba oil 3kg, squalane 1.8kg, methyl hydroxybenzoate 0.8kg, glycerol 5kg, tea juice 40kg, deionized water 50kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying, then carry out microwave vacuum processing: the material after stirring and emulsifying is sent in microwave vacuum tank, then carry out evacuation process to vacuum be-0.08MPa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.8min, and discharging is cooled to room temperature and obtains bamboo charcoal facial milk cleanser.
Use the effect of embodiment 3 compositionss:
Experimenter is totally 25 people, male 2 people wherein, female 23 people.Using after one month, all there is not local skin untoward reaction in experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 21 experimenters represent to use the salubrious non-greasy of face after embodiment 3 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and face mask lines are than more clear clearly demarcated before using; 4 subject perception have massage and whitening effect while washing one's face, but effect is obvious not.
Embodiment tetra-
The preparation of bamboo charcoal powder is with embodiment bis-.Then prepared by the bamboo charcoal making to the bamboo charcoal powder of particle diameter 200nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2.8 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtain the first concentrated solution of solid contents 10%; Half of getting the first concentrated solution be at 43 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 34%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take oatmeal 5-10kg, Semen Sesami Nigrum 3-5kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6kg, Radix Angelicae Sinensis powder 3-5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 13%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 32%-35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 1kg nano bamboo powdered carbon, sodium alginate 1.5kg, alkyl polyglucoside 0.3kg, Jojoba oil 2kg, squalane 0.5kg, propyl hydroxybenzoate 0.5kg, glycerol 3kg, tea juice 30kg, deionized water 40kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying, then carry out microwave vacuum processing: the material after stirring and emulsifying is sent in microwave vacuum tank, then carry out evacuation process to vacuum be-0.07MPa; Carry out microwave treatment, microwave frequency is 345MHz again, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains bamboo charcoal facial milk cleanser.
Use the effect of embodiment 4 compositionss:
Experimenter is totally 25 people, male 2 people wherein, female 23 people.Using after one month, all there is not local skin untoward reaction in experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 20 experimenters represent to use the salubrious non-greasy of face after embodiment 4 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and face mask lines are than more clear clearly demarcated before using; 5 subject perception have massage and whitening effect while washing one's face, but effect is obvious not.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the modification that there is no creative contribution as required after reading this description, but as long as within the scope of claim of the present invention, are all subject to the protection of Patent Law.
Claims (8)
1. a bamboo charcoal facial milk cleanser, is characterized in that: the one-tenth by following weight portion is grouped into: 1-8 part nano bamboo powdered carbon, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part, deionized water 40-50 part and decoction liquor; Described decoction liquor is extracted and is obtained by decocting method by the composition of following parts by weight: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part;
Described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, with reverse osmosis membrane, concentrate, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid.
2. a kind of bamboo charcoal facial milk cleanser according to claim 1, is characterized in that: described antiseptic is sorbic acid or sodium diacetate.
3. a kind of bamboo charcoal facial milk cleanser according to claim 2, is characterized in that: described bamboo charcoal powder makes by the following method:
1., in vertical moving bed, from top, add the bamboo of splitting broken and preliminarily dried through blocking, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces is dried bamboo and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged and is entered Bamboo vinegar solution condenser from top, and condensation obtains Bamboo vinegar solution; Control the temperature difference of described calcining zone diverse location and carry out staged intensification, make the calcining zone that experiences in bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2. the bamboo charcoal, upper step being made is prepared nano bamboo powdered carbon.
4. a kind of bamboo charcoal facial milk cleanser according to claim 3, is characterized in that: the particle diameter 100-200nm of described bamboo charcoal powder.
5. a kind of bamboo charcoal facial milk cleanser according to claim 4, is characterized in that: the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, by the weight ratio of 1:4-9, mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
6. a kind of bamboo charcoal facial milk cleanser according to claim 5, is characterized in that: described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
7. a kind of bamboo charcoal facial milk cleanser according to claim 6, is characterized in that: the solids concentration of the first concentrated solution is 15%-20%, and the solids concentration of the second concentrated solution is 33%-35%.
8. a kind of bamboo charcoal facial milk cleanser according to claim 7, is characterized in that: the temperature while concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210357555.2A CN102836103B (en) | 2012-09-24 | 2012-09-24 | Bamboo charcoal facial cleanser |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210357555.2A CN102836103B (en) | 2012-09-24 | 2012-09-24 | Bamboo charcoal facial cleanser |
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| CN102836103B true CN102836103B (en) | 2014-03-12 |
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| CN103239375A (en) * | 2013-05-05 | 2013-08-14 | 洪圣娟 | Cypress charcoal oil absorption washing powder for men |
| CN104434648A (en) * | 2014-11-17 | 2015-03-25 | 青岛厚科信息工程有限公司 | Antibacterial facial cleanser and preparation method thereof |
| CN106309306A (en) * | 2016-08-17 | 2017-01-11 | 倪娟形 | Skin care facial cleanser and preparation method thereof |
| CN111362248A (en) * | 2018-12-25 | 2020-07-03 | 成都易生玄科技有限公司 | Production method of face-cleaning bamboo charcoal |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1723877A (en) * | 2005-05-27 | 2006-01-25 | 徐建国 | Cleansing milk contg. bamboo charcoal |
| CN101245294B (en) * | 2007-09-05 | 2010-06-09 | 江苏隆力奇生物科技股份有限公司 | Perfumed soap |
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