CN102836102B - Method for preparing bamboo charcoal facial cleanser - Google Patents
Method for preparing bamboo charcoal facial cleanser Download PDFInfo
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- CN102836102B CN102836102B CN 201210357554 CN201210357554A CN102836102B CN 102836102 B CN102836102 B CN 102836102B CN 201210357554 CN201210357554 CN 201210357554 CN 201210357554 A CN201210357554 A CN 201210357554A CN 102836102 B CN102836102 B CN 102836102B
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Abstract
The invention relates to a method for preparing a bamboo charcoal facial cleanser, which belongs to the field of life of cosmetics. The method for preparing the bamboo charcoal facial cleanser comprises the steps of: a), preparation of a decoction: weighing oat powder, semen sesami nigrum and soybeans according to the parts by weight, decocting for 4 to 5h, and filtrating and concentrating to obtain a first decoction; decocting bletilla striata and angelica sinensis powder for 6 to 7 hours, and filtrating and concentrating to obtain a second decoction; and then mixing the first decoction and the second decoction to obtain a decoction; and b) preparation of the bamboo charcoal facial cleanser: weighing the obtained decoction, 1 to 8 parts of nano bamboo charcoal powder, 1.5 to 2 parts of sodium alginate, 0.3 to 0.8 parts of alkyl glycoside, 2 to 3 parts of jojoba oil, 0.5 to 1.8 parts of squalane, 0.5 to 0.8 parts of preservative, 3 to 5 parts of glycerol, 30 to 40 parts of tea extract and 40 to 50 parts of de-ionized water according to the parts by weight; and mixing and stirring and emulsifying all substances, and then performing microwave vacuum treatment to obtain the bamboo charcoal facial cleanser. The facial cleanser provided by the invention is capable of effectively cleansing the faces, ensuring the skin to hold in moisture, strengthening oxidation resistance and antianaphylaxis of the skin.
Description
Technical field
The present invention relates to a kind of preparation method of bamboo charcoal facial milk cleanser, belong to the household chemicals field.
Background technology
If existing cleansing milk such as cleansing milk Bian are made by the synthetic wetting agent of more single surfactant compound in the market, thereby reach the purpose of decontamination.Owing to having used a large amount of surfactants, easily cause the undue defat of epiderm skin, thereby make skin drier, more serious meeting causes the irreversibility infringement to skin, and function singleness, can't satisfy user to the demand of the multiple efficacies of skin care.
CN101427987(2010-12-15) provide a kind of face cleaning skin lotion product and preparation method thereof, yet this product forms by purifying frost and cleaning agent, use inconvenient, and its clean-up performance, performance of keeping humidity and the effect of skin non-oxidizability and antiallergic is all had much room for improvement.
Summary of the invention
The purpose of this invention is to provide and a kind ofly can effectively clean face, guarantee the preparation method that skin keeps moistening, strengthens the bamboo charcoal facial milk cleanser of skin non-oxidizability and antiallergic.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A kind of preparation method of bamboo charcoal facial milk cleanser, it comprises step: a), the preparation of decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
B), the preparation of bamboo charcoal facial milk cleanser: take by weight step a) gained decoction liquor, 1-8 part nano bamboo powdered carbon, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part and deionized water 40-50 part; All substances are mixed and stirring and emulsifying, then carry out the microwave vacuum processing and obtain the bamboo charcoal facial milk cleanser.
Alkyl polyglucoside is a kind of non-ionic surface active agent of gentle environmental protection.Sodium alginate is the polysaccharide-sodium alginate that is derived from Sargassum, easily forms gel.
The nano bamboo powdered carbon has the super large surface area of extremely strong absorption property, be particularly suitable for being used in the beauty and skin care field, and apply at facial zone after other combinations of substances, can play massage effect, its infrared effect can be played the magnetic therapy radiation effects to eye, helps blood circulation promoting; Squalane can suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, to strengthening skin non-oxidizability and elasticity, obvious physiologic effect is arranged; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in tea juice can keep skin moistening.The Jojoba oil main component is unsaturated higher alcohol and fatty acid, and good stability is arranged, and very easily merges with skin, has non-oxidizability free from worldly cares.In addition, Jojoba oil also contains and enriches vitamin, has the effect of nourishing softening skin and keeping skin wetness.
In decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, especially is fit to the sensitivity skin; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium that is rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care can prevent pachylosis and aging, help to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can strengthen skin non-oxidizability and antiallergic.According to the decoction liquor that each umber proportioning of the present invention forms, can effectively eliminate eye pouch and black eye.
The present invention fully utilizes gel emulsification and the moisture-keeping function of sodium alginate and alkyl polyglucoside mixture, and mix with nano bamboo powdered carbon of the present invention, decoction liquor and tea juice, prove through crowd's trial effect, can when effectively cleaning face, guarantee that skin keeps moistening, strengthens skin non-oxidizability and antiallergic.
As preferably, the microwave vacuum treatment conditions of described step b) are: will send into after all substances mixing and emulsifying in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
process by microwave vacuum of the present invention, heat effect and non-thermal effect occur in each component simultaneously, during carry out microwave radiation heating, electromagnetic field in microwave is with several hundred million even billions of inferior frequency inverted directions of per second, make polarization and this polarization of the different electric charges of material internal not possess the ability of catching up with rapidly alternating electric field, cause the material internal friction and generate heat, i.e. so-called " interior heating ", make each component in facial film mutually blend, emulsifying is uniform and complete more, and some other reactions may occur, facial milk cleanser of the present invention is played massage face, effectively cleaning is facial, guarantee that skin keeps moistening, strengthen the function of skin non-oxidizability and antiallergic.
As preferably, described antiseptic is sorbic acid or sodium diacetate.
As preferably, described bamboo charcoal powder makes by the following method:
1., add the bamboo of splitting broken and preliminarily dried through blocking from the top in vertical moving bed, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged from the top and is entered the Bamboo vinegar solution condenser, and condensation gets Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out the staged intensification, make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., the bamboo charcoal that the upper step was made prepares the nano bamboo powdered carbon.
More preferably, the particle diameter 100-200nm of described bamboo charcoal powder.
As preferably, described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid.
As preferably, include Radix Hamamelidis Mollis and Folium Camelliae sinensis that weight ratio is 1:4-9 in described tea juice.
As preferably, the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
By decocting method of the present invention, can fully utilize the non-oxidizability of Radix Hamamelidis Mollis and tea juice, help skin to mend wet and quiet flesh.
More preferably, described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in described step (2), the solids concentration of the first concentrated solution is 15%-20%, and the solids concentration of the second concentrated solution is 33%-35%.
Because the excessive concentration of the first concentrated solution is the overlong time of reverse osmosis, fragrance is worsened, the too low vacuum concentration overlong time that makes next step of concentration, also brown stain and make the fragrance oxidation, the excessive concentration of the second concentrated solution is the vacuum concentration overlong time, and concentration is too low can not get enough products.
More preferably, the temperature when concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
Description of drawings
Fig. 1 is the temperature control system schematic diagram of the vertical moving bed of bamboo charcoal carbonization of the present invention.
In figure, the A-dry section; The pre-char zone of B-; The C-char zone; The D-calcining zone; The E-cooling zone; F-is with the temperature sensing device of CPU; D1/d2/d3-oxidizer entrance hole; The t1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed of bamboo charcoal powder preparation use is divided into dry section A, pre-char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D one side is distributed with the many oxidizer entrance holes that can regulate closure or openness, as d1, d2, d3 etc., opposite side be to should have point for measuring temperature such as t1, t2, the t3 etc. at each aperture place, and each aperture place temperature shows by the temperature sensing device F that is connected with this point for measuring temperature.
Embodiment one
bamboo charcoal powder preparation: carry out pilot scale in vertical moving bed dry distillation carbonizing furnace, bamboo chip (being about 36cm) with average moisture content 39%, the temperature of each point for measuring temperature, dry section A is 150 ℃, pre-char zone B is 275 ℃, char zone C is 450 ℃, observe the temperature of D shown in Figure 1 district combustion zone diverse location during intensification, when the temperature of somewhere, combustion zone such as d2 is too low, open the aperture at this place, importing air locally burns, this place's temperature is raise, control the combustion zone temperature that experiences in the bamboo folding process and be warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then be warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min from 700 ℃, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 40 ℃.Continuous operation takes out bamboo charcoal after 10 days (not comprising the warm stove time).Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.Then the bamboo charcoal that makes is prepared the powdered carbon of particle diameter 100nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is that mass ratio is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soaked 2 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtain the first concentrated solution of solid contents 5%; Half of getting the first concentrated solution be at 40 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 30%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
The preparation of decoction liquor: take oatmeal 5kg, Semen Sesami Nigrum 3kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4kg, Radix Angelicae Sinensis powder 3kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 5kg nano bamboo powdered carbon, sodium alginate 1.9kg, alkyl polyglucoside 0.7kg, Jojoba oil 2.3kg, squalane 0.5kg, sorbic acid 0.5kg, glycerol 3.5kg, tea juice 33kg, deionized water 48kg and above-mentioned decoction liquor are mixed; Then stirring and emulsifying is carried out microwave vacuum and is processed: the material after stirring and emulsifying is sent in the microwave vacuum tank, then carried out evacuation and process to vacuum and be-0.09MPa; Carry out microwave treatment, microwave frequency is 245MHz again, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Cleansing milk provided by the invention is checked through the PLA Air Force General Hospital, and the experimenter is totally 100 people, male 8 people wherein, female 92 people, age 18-62 one full year of life.Using method is: the experimenter directly uses and is subjected to trial product, every day, each used once sooner or later, before using, face was drenched with clear water, extruded appropriate cleansing milk of the present invention in the centre of the palm, add a small amount of clear water to rub and enrich foam, clean with flushing with clean water in a moment at face message.Adhered to using one month, and checked at least weekly once to have or not whole body and local untoward reaction with understanding, and the itemized record result.
Use the effect of embodiment 1 compositions:
The experimenter is totally 25 people, male 2 people wherein, female 23 people.Use after one month, the experimenter all represents to use the salubrious non-greasy of face after embodiment 1 compositions, can effectively clean dirt, and that skin keeps for a long time is moistening, clearly compact and high resilience, and the face mask lines are than more clear clearly demarcated before using, the good in oxidation resistance of skin after using; The local skin untoward reaction appears in the equal end of experimenter, and also without little good reactions of whole body such as anorexia, diarrhoea, weak, endocrine regulations, after using, the antiallergic of skin is good.
Embodiment two
the preparation of bamboo charcoal powder: carry out pilot scale in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, ancestor's bamboo chip in the Meng (being about 40cm) with average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃, pre-char zone B is 270 ℃, char zone C is 500 ℃, burn simultaneously from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion during intensification, make combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min, and then be warming up to 1500 ℃ and be incubated 8h with the speed of 15 ℃/min from 750 ℃, spray into steam 60min in 1500 ℃ of districts, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 30 ℃.Continuous operation takes out bamboo charcoal after 8 days (not comprising the warm stove time), the solution of the bamboo charcoal that takes out being put into acid content 4% soaks 2h, takes out with clear water and cleans, and then puts into oven dry kiln drying 1h.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.Then the bamboo charcoal that makes is prepared the powdered carbon of grain 120nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soaked 2.5 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain the first concentrated solution of solid contents 20%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 33%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
The preparation of decoction liquor: take oatmeal 10kg, Semen Sesami Nigrum 5kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 2kg nano bamboo powdered carbon, sodium alginate 1.8kg, alkyl polyglucoside 0.5kg, Jojoba oil 2.5kg, squalane 1kg, sodium diacetate 0.6kg, glycerol 4kg, tea juice 35kg, deionized water 45kg and above-mentioned decoction liquor are mixed; Then stirring and emulsifying is carried out microwave vacuum and is processed: the material after stirring and emulsifying is sent in the microwave vacuum tank, then carried out evacuation and process to vacuum and be-0.06MPa; Carry out microwave treatment, microwave frequency is 400MHz again, and microwave treatment time is 1min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Test method is used the effect of embodiment 2 compositionss with embodiment one:
The experimenter is totally 25 people, male 2 people wherein, female 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 22 experimenters represent to use the salubrious non-greasy of face after embodiment 2 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 3 subject perception have massage and whitening effect when washing one's face, but effect is obvious not.
Embodiment three
The preparation of bamboo charcoal powder is with embodiment one.Then the bamboo charcoal that makes is prepared the bamboo charcoal powder of particle diameter 150nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soaked 1.5 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain the first concentrated solution of solid contents 15%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
The preparation of decoction liquor: take oatmeal 8kg, Semen Sesami Nigrum 4kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 8kg nano bamboo powdered carbon, sodium alginate 2kg, alkyl polyglucoside 0.8kg, Jojoba oil 3kg, squalane 1.8kg, methyl hydroxybenzoate 0.8kg, glycerol 5kg, tea juice 40kg, deionized water 50kg and above-mentioned decoction liquor are mixed; Then stirring and emulsifying is carried out microwave vacuum and is processed: the material after stirring and emulsifying is sent in the microwave vacuum tank, then carried out evacuation and process to vacuum and be-0.08MPa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.8min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Use the effect of embodiment 3 compositionss:
The experimenter is totally 25 people, male 2 people wherein, female 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 21 experimenters represent to use the salubrious non-greasy of face after embodiment 3 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 4 subject perception have massage and whitening effect when washing one's face, but effect is obvious not.
Embodiment four
The preparation of bamboo charcoal powder is with embodiment two.Then the bamboo charcoal that makes is prepared the bamboo charcoal powder of particle diameter 200nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soaked 2.8 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtain the first concentrated solution of solid contents 10%; Half of getting the first concentrated solution be at 43 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 34%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
The preparation of decoction liquor: take oatmeal 5-10kg, Semen Sesami Nigrum 3-5kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6kg, Radix Angelicae Sinensis powder 3-5kg, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 13%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32%-35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 1kg nano bamboo powdered carbon, sodium alginate 1.5kg, alkyl polyglucoside 0.3kg, Jojoba oil 2kg, squalane 0.5kg, propyl hydroxybenzoate 0.5kg, glycerol 3kg, tea juice 30kg, deionized water 40kg and above-mentioned decoction liquor are mixed; Then stirring and emulsifying is carried out microwave vacuum and is processed: the material after stirring and emulsifying is sent in the microwave vacuum tank, then carried out evacuation and process to vacuum and be-0.07MPa; Carry out microwave treatment, microwave frequency is 345MHz again, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Use the effect of embodiment 4 compositionss:
The experimenter is totally 25 people, male 2 people wherein, female 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, without systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulations yet.Wherein 20 experimenters represent to use the salubrious non-greasy of face after embodiment 4 compositionss, can effectively clean dirt, and skin keeps for a long time moistening, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 5 subject perception have massage and whitening effect when washing one's face, but effect is obvious not.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the modification that there is no creative contribution as required after reading this description, but as long as all are subject to the protection of Patent Law in claim scope of the present invention.
Claims (9)
1. the preparation method of a bamboo charcoal facial milk cleanser is characterized in that comprising step:
A), the preparation of decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
B), the preparation of bamboo charcoal facial milk cleanser: take by weight step a) gained decoction liquor, 1-8 part nano bamboo powdered carbon, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part and deionized water 40-50 part; All substances are mixed and stirring and emulsifying, then carry out the microwave vacuum processing and obtain the bamboo charcoal facial milk cleanser.
2. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 1, it is characterized in that: the microwave vacuum treatment conditions of described step b) are: will send into after all substances mixing and emulsifying in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
3. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 2, it is characterized in that: described antiseptic is sorbic acid or sodium diacetate.
4. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 3, it is characterized in that: described bamboo charcoal powder makes by the following method:
1., add the bamboo of splitting broken and preliminarily dried through blocking from the top in vertical moving bed, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged from the top and is entered the Bamboo vinegar solution condenser, and condensation gets Bamboo vinegar solution; Control the temperature difference of described calcining zone diverse location and carry out the staged intensification, make the calcining zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., the bamboo charcoal that the upper step was made prepares the nano bamboo powdered carbon.
5. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 4, is characterized in that: the particle diameter 100-200nm of described bamboo charcoal powder.
6. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 5, it is characterized in that: the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get tea juice.
7. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 6, it is characterized in that: described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
8. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 7, it is characterized in that: the solids concentration of the first concentrated solution is 15%-20%, the solids concentration of the second concentrated solution is 33%-35%.
9. the preparation method of a kind of bamboo charcoal facial milk cleanser according to claim 8, it is characterized in that: the temperature when concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
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| CN103301029B (en) * | 2013-06-18 | 2015-03-04 | 中国日用化学工业研究院 | Facial cleanser capable of balancing oil and moisturizing skin, and preparation method thereof |
| CN109055050A (en) * | 2018-08-13 | 2018-12-21 | 深圳市科迪生物科技有限公司 | A kind of efficient hair follicle cleaning essential oil soap composition |
| CN108904304A (en) * | 2018-09-06 | 2018-11-30 | 黄犟兵 | A kind of face cleaning cream and preparation method thereof containing charcoal |
| CN111362248A (en) * | 2018-12-25 | 2020-07-03 | 成都易生玄科技有限公司 | Production method of face-cleaning bamboo charcoal |
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