CN102836116B - Method for preparing bamboo charcoal eye mask - Google Patents
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- CN102836116B CN102836116B CN2012103575410A CN201210357541A CN102836116B CN 102836116 B CN102836116 B CN 102836116B CN 2012103575410 A CN2012103575410 A CN 2012103575410A CN 201210357541 A CN201210357541 A CN 201210357541A CN 102836116 B CN102836116 B CN 102836116B
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a method for preparing a bamboo charcoal eye mask, which belongs to the life field of cosmetics. The method for preparing bamboo charcoal eye mask is composed of the following components by weight: 1 to 8 parts of nano bamboo charcoal powder, 15 to 20 parts of ganoderma lucidum powder, 0.5 to 1.8 parts of squalane, 3 to 5 parts of ligusticum chuanxiong powder, 30 to 40 parts of tea extract, 40 to 50 parts of water and a decoction; the decoction is obtained by extracting the following components by weight through a decoction process: 5 to 10 parts of oat powder, 3 to 5 parts of semen sesami nigrum, 5 to 10 parts of soybeans, 4 to 6 parts of bletilla striata and 3 to 5 parts of angelica sinensis powder. The bamboo charcoal eye mask provided by the invention is capable of effectively removing eyebags and black eyes.
Description
Technical field
The present invention relates to a kind of preparation method of bamboo charcoal eye mask, belong to the cosmetics sphere of life.
Background technology
Eye mask is a kind of cosmetics and skincare product applied in around eyes, plays effect clean, vigorous and graceful and the protection eye.Increasing moisture of skin is the basis of beauty and skin care, and the skin dried out is can be dry coarse, form microgroove, pigmentation, causes many skin problems.As commercial goods snow is full of whitening plant eye mask, its main component is Radix Ophiopogonis extract, the peach extract, and Flos Carthami extract, the Radix Asparagi extract, Radix Angelicae Sinensis extract, cucurbitaceous plant, green tea extract, Folium Vaccinii vitis-idaeae is general, has the effect of moisturizing whitening.These groups advocate to start with from antioxidation and moisturizing, have certain whitening skin and preserving moisture effect, but a little less than the effect of wrinkle removal.
CN1319511C(2007-6-6) disclose a kind of Wrinkle removing eye patch, yet its performance of removing black eye, enhancing skin elasticity, elimination eye fat granule all haves much room for improvement.
Summary of the invention
The purpose of this invention is to provide and a kind ofly can effectively eliminate eye pouch and black-eyed bamboo charcoal eye mask.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A kind of preparation method of bamboo charcoal eye mask, it comprises the following steps:
The preparation of A, decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, bamboo charcoal eye mask: tea juice and Ganoderma powder 15-20 part, squalane 0.5-1.8 part, Rhizoma Chuanxiong powder 3-5 part and water 40-50 part of taking by weight steps A gained decoction liquor, 1-8 part nano bamboo powdered carbon, 30-40 part; Carry out the microwave vacuum processing after all substances are mixed, then pour in the eye mask mould, cooling, prepare bamboo charcoal eye mask finished product.
The nano bamboo powdered carbon has the super large surface area of extremely strong absorption property, be particularly suitable for being used in the beauty and skin care field, with after other combinations of substances, apply at ocular, can play massage effect, its infrared effect can be played the magnetic therapy radiation effects to eye, help blood circulation promoting, help to eliminate eye pouch and black eye, enhancing skin elasticity, eliminate the eye fat granule; Squalane can suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, to delay skin aging, improves and eliminates eye pouch and black eye all have obvious physiologic effect; The immunoregulation effect of Ganoderma and polysaccharide component thereof, can promote the anabolism of nucleic acid protein, the ability of the division algebraically of resisting oxidation free radical activity and extension body unofficial biography metabolism cell; Ganoderma powder and the combined effect of Rhizoma Chuanxiong powder can strengthen skin elasticity, improve eye pouch and black eye phenomenon; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in tea juice, can prevent skin aging and recover skin elasticity.
In decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, especially is applicable to the sensitivity skin; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium be rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care, can prevent pachylosis and aging, contributes to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can prevent eye dryness, prevents skin aging and recover skin elasticity.The decoction liquor formed according to each umber proportioning of the present invention, can effectively eliminate eye pouch and black eye.
When prepared by eye mask, by microwave vacuum of the present invention, process, heat effect and non-thermal effect occur in each component simultaneously, during carry out microwave radiation heating, electromagnetic field in microwave is with several hundred million even billions of inferior frequency inverted directions of per second, make polarization and this polarization of the different electric charges of material internal not possess the ability of catching up with rapidly alternating electric field, cause the material internal friction and generate heat, i.e. so-called " interior heating ", make each component in eye mask mutually blend, and some reactions may occur, finally make eye mask composition performance of the present invention eliminate eye pouch and black eye, strengthen skin elasticity, eliminate the excellent results of eye fat granule.
Preferably, described step B microwave vacuum treatment conditions are: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
As preferably, described bamboo charcoal powder makes by the following method:
1., add the bamboo of splitting broken and preliminarily dried through blocking from top in vertical moving bed, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged and is entered the Bamboo vinegar solution condenser from top, and condensation obtains Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out the staged intensification, make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., the bamboo charcoal upper step made prepares the nano bamboo powdered carbon.
More preferably, the particle diameter 5-12nm of described bamboo charcoal powder.
As preferably, described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid.
As preferably, Radix Hamamelidis Mollis and Folium Camelliae sinensis that to include weight ratio in described tea juice be 1:4-9.
As preferably, the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtained the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
More preferably, described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in described step (2), the solids concentration of the first concentrated solution is 15%-20%.
Because the excessive concentration of the first concentrated solution is the overlong time of reverse osmosis, fragrance is worsened, the too low vacuum concentration overlong time that makes next step of concentration, also brown stain and make the fragrance oxidation.
More preferably, in described step (2), the solids concentration of the second concentrated solution is 33%-35%.
The excessive concentration of the second concentrated solution is the vacuum concentration overlong time, and concentration is too low can not get enough products.
Temperature while more preferably, concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃.
More preferably, in described step (2), the temperature of vacuum concentration is 40-45 ℃.
The accompanying drawing explanation
Fig. 1 is the temperature control system schematic diagram of the vertical moving bed of bamboo charcoal carbonization of the present invention.
In figure, the A-dry section; The pre-char zone of B-; The C-char zone; The D-calcining zone; The E-cooling zone; F-is with the temperature sensing device of CPU; D1/d2/d3-oxidizer entrance hole; The t1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed that the bamboo charcoal powder preparation is used is divided into dry section A, pre-char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D mono-side is distributed with the many oxidizer entrance holes that can regulate closure or openness, as d1, d2, d3 etc., opposite side is to point for measuring temperature that each aperture place should be arranged as t1, t2, t3 etc., and each aperture place temperature shows by the temperature sensing device F be connected with this point for measuring temperature.
Embodiment mono-
Bamboo charcoal powder preparation: in vertical moving bed dry distillation carbonizing furnace, carry out pilot scale, bamboo chip (being about 36cm) with average moisture content 39%, the temperature of each point for measuring temperature, dry section A is 150 ℃, pre-char zone B is 275 ℃, char zone C is 450 ℃, the temperature of D district combustion zone diverse location shown in observation Fig. 1 during intensification, when the somewhere, combustion zone is as too low as the temperature of d2, open the aperture at this place, importing air locally burns, this place's temperature is raise, control the combustion zone temperature that experiences in the bamboo folding process and be warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then be warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min from 700 ℃, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 40 ℃.Continuous operation takes out bamboo charcoal after 10 days (not comprising the warm stove time).Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.Then prepared by the bamboo charcoal made to the powdered carbon of particle diameter 5nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is that mass ratio is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtained the first concentrated solution of solid contents 5%; Half of getting the first concentrated solution be at 40 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 30%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 5 parts of oatmeals, 3 parts of Semen Sesami Nigrums, Semen sojae atricolor 5-10 part, 4 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 3 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal eye mask: take by weight 40 parts, the bamboo charcoal powder of 1 part, tea juice, gained decoction liquor and 15 parts of Ganoderma powder, 0.5 part of squalane, 3 parts, the Rhizoma Chuanxiong powder of 30 parts and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.09MPaMPa; Carry out microwave treatment, microwave frequency is 245MHz again, and microwave treatment time is 0.5min.Then all substances after microwave vacuum being processed are poured in the eye mask mould, are cooled to room temperature, prepare bamboo charcoal eye mask finished product.
Embodiment bis-
The preparation of bamboo charcoal powder: in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, carry out pilot scale, ancestor's bamboo chip in the Meng (being about 40cm) with average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃, pre-char zone B is 270 ℃, char zone C is 500 ℃, during intensification, from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion, burn simultaneously, make combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min, and then be warming up to 1500 ℃ and be incubated 8h with the speed of 15 ℃/min from 750 ℃, spray into steam 60min in 1500 ℃ of districts, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 30 ℃.Continuous operation takes out bamboo charcoal after 8 days (not comprising the warm stove time), the solution of the bamboo charcoal of taking-up being put into to acid content 4% soaks 2h, takes out with clear water and cleans, and then puts into and dries kiln drying 1h.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.Then prepared by the bamboo charcoal made to the powdered carbon of grain 8nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2.5 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtained the first concentrated solution of solid contents 20%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 33%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 10 parts of oatmeals, 5 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal eye mask: take by weight 50 parts, the bamboo charcoal powder of gained 1-8 part, tea juice, gained decoction liquor and 20 parts of Ganoderma powder, 1.8 parts of squalanes, 5 parts, the Rhizoma Chuanxiong powder of 40 parts and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.06MPa; Carry out microwave treatment, microwave frequency is 400MHz again, and microwave treatment time is 1min.Then all substances after microwave vacuum being processed are poured in the eye mask mould, are cooled to room temperature, prepare bamboo charcoal eye mask finished product.
Embodiment tri-
The preparation of bamboo charcoal powder is with embodiment mono-.Then prepared by the bamboo charcoal made to the bamboo charcoal powder of particle diameter 10nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 1.5 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtained the first concentrated solution of solid contents 15%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 8 parts of oatmeals, 4 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal eye mask: take by weight 45 parts, tea juice, gained decoction liquor and 18 parts of Ganoderma powder, 1 part of squalane, 4 parts, the Rhizoma Chuanxiong powder of 35 parts of bamboo charcoal powder, the gained of 1-8 part and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.08MPa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.8min.Then all substances after microwave vacuum being processed are poured in the eye mask mould, are cooled to room temperature, prepare bamboo charcoal eye mask finished product.
Embodiment tetra-
The preparation of bamboo charcoal powder is with embodiment bis-.Then prepared by the bamboo charcoal made to the bamboo charcoal powder of particle diameter 12nm.
The preparation method of tea juice is: (1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water and fully soak 2.8 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtained the first concentrated solution of solid contents 10%; Half of getting the first concentrated solution be at 43 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 34%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 13%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32%-35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal eye mask: take by weight 48 parts, tea juice, gained decoction liquor and 16 parts of Ganoderma powder, 0.8 part of squalane, 5 parts, the Rhizoma Chuanxiong powder of 33 parts of bamboo charcoal powder, the gained of 5 parts of gained and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.07MPa; Carry out microwave treatment, microwave frequency is 345MHz again, and microwave treatment time is 0.5min.Then all substances after microwave vacuum being processed are poured in the eye mask mould, are cooled to room temperature, prepare bamboo charcoal eye mask finished product.
In order to understand better the present invention, below will improve the technique effect that the present invention has will be described by clinical experiment report.
Number of cases on probation: 18-30 year crowd, women 60 people, male 20 people; 30-45 year crowd, women 60 people, male 20 people; Crowd more than 45 years old, women 60 people, male 20 people.Totally 240 people.
Above-mentioned person on probation, every day each 1 time sooner or later, 20 days on probation continuously.
In 18-30 year crowd, women's 50 people's eye pouch diminish, and 9 people disappear, and it is not obvious that 1 people changes, and male's 15 people's eye pouch diminish, and 4 people disappear, and 1 people changes not obvious.
In 30-45 year crowd, women's 55 people's eye pouch diminish, and 3 people disappear, and it is not obvious that 2 people change, and male 15 people diminish, and 1 people disappears, and 4 people change not obvious.
More than 45 years old, in the crowd, women's 54 people's eye pouch diminish, and it is not obvious that 6 people change, and it is little that male 12 people attenuate, and 6 people change not obvious.
Separately, in above-mentioned 240 triers, have 31 people's eye that the oils and fats grain is arranged, after bamboo charcoal eye mask of the present invention on probation, eye oils and fats grain 2 people disappear, and 23 people obviously reduce, and 6 people change not obvious.In addition, after trial edition bamboo charcoal eye mask, it is more delicate, smooth, flexible that all triers' skin all becomes continuously.All trying out has no adverse reaction per capita.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the modification that there is no creative contribution as required after reading this description, but as long as all are subject to the protection of Patent Law in claim scope of the present invention.
Claims (7)
1. the preparation method of a bamboo charcoal eye mask is characterized in that: comprise the following steps:
The preparation of A, decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, bamboo charcoal eye mask: tea juice and Ganoderma powder 15-20 part, squalane 0.5-1.8 part, Rhizoma Chuanxiong powder 3-5 part and water 40-50 part of taking by weight steps A gained decoction liquor, 1-8 part nano bamboo powdered carbon, 30-40 part; Carry out the microwave vacuum processing after all substances are mixed, then pour in the eye mask mould, cooling, prepare bamboo charcoal eye mask finished product.
2. the preparation method of a kind of bamboo charcoal eye mask according to claim 1, it is characterized in that: described step B microwave vacuum treatment conditions are: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
3. the preparation method of a kind of bamboo charcoal eye mask according to claim 2, is characterized in that: the particle diameter 5-12nm of described bamboo charcoal powder.
4. the preparation method of a kind of bamboo charcoal eye mask according to claim 1, it is characterized in that: the preparation method of described tea juice is:
(1), first Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtained the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
5. the preparation method of a kind of bamboo charcoal eye mask according to claim 4, it is characterized in that: described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
6. the preparation method of a kind of bamboo charcoal eye mask according to claim 4, it is characterized in that: in described step (2), the solids concentration of the first concentrated solution is 15%-20%.
7. the preparation method of a kind of bamboo charcoal eye mask according to claim 4, it is characterized in that: the temperature while concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃.
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| CN103536520A (en) * | 2013-10-18 | 2014-01-29 | 桂林雪芙莲日化有限公司 | Hydrating eye mask |
| CN104146923A (en) * | 2014-08-28 | 2014-11-19 | 桂林市艾康科技有限公司 | Preparation method of bamboo vinegar eye mask |
| CN106539736A (en) * | 2017-01-23 | 2017-03-29 | 钟苏 | A kind of Rosehips oil emollient cream and preparation method thereof |
| CN107412096A (en) * | 2017-05-17 | 2017-12-01 | 太仓新亚逊生物科技有限公司 | A kind of Chinese medicine anti-wrinkle moisturizing eye mask |
| CN108547058B (en) * | 2018-04-18 | 2019-11-26 | 广东柏俐臣生物科技有限公司 | A kind of bamboo charcoal Biofibre facial mask base fabric of high water lock anti-drip and high water lock moisture saver mask |
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| CN1223336C (en) * | 2003-11-27 | 2005-10-19 | 南宁市金赛保健品有限责任公司 | Natural sea salt skin care product |
| CN101194885B (en) * | 2006-12-08 | 2010-05-19 | 何柏军 | Bamboo charcoal face pack |
| CN101518508B (en) * | 2009-03-31 | 2011-11-09 | 东方药林药业有限公司 | Beautifying health composition and facial mask |
| CN101991525A (en) * | 2009-08-13 | 2011-03-30 | 常立芝 | Health-care bamboo charcoal mask and preparation technology thereof |
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