CN102860972B - Preparation method of bamboo charcoal mask - Google Patents
Preparation method of bamboo charcoal mask Download PDFInfo
- Publication number
- CN102860972B CN102860972B CN2012103575622A CN201210357562A CN102860972B CN 102860972 B CN102860972 B CN 102860972B CN 2012103575622 A CN2012103575622 A CN 2012103575622A CN 201210357562 A CN201210357562 A CN 201210357562A CN 102860972 B CN102860972 B CN 102860972B
- Authority
- CN
- China
- Prior art keywords
- bamboo charcoal
- parts
- preparation
- decoction
- concentrated solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention relates to a preparation method of a bamboo charcoal mask, which belongs to the life field of cosmetic. The preparation method of the bamboo charcoal mask comprises the steps of: A, a decoction solution preparation: according to the parts by weight, weighing 5 to 10 parts of oat powder, 3 to 5 parts of semen sesami nigrum, 5 to 10 parts of soybean, 4 to 6 parts of bletilla striata and 3 to 5 parts of angelica sinensis powder, adding water into oat powder, semen sesami nigrum and soybeans for decoction, filtration and concentration to obtain a first decoction solution, adding water to bletilla striata and angelica sinensis powder for decoction, filtration and concentration to obtain a second decoction solution, and mixing the first decoction solution and the second decoction solution to obtain the decoction solution; and B, preparation of the bamboo charcoal mask: according to the parts by weight, weighing the decoction, 1 to 8 parts of bamboo charcoal powder with particle size of 8,000 to 12,500 meshes, 30 to 40 parts of tea juice, 15 to 20 parts of cucumber juice, 0.5-1.8 parts of peppermint, 3 to 5 parts of egg white and 40 to 50 parts of water, and carrying out microwave vacuum treatment for the components, then, pouring the mixture into a mask mould for cooling, and obtaining a bamboo charcoal mask finished product. The bamboo charcoal mask provided by the invention is capable of preventing aging and reducing wrinkles, strengthening the skin elasticity and clearing up the blockages in the pores.
Description
Technical field
The present invention relates to a kind of preparation method of bamboo charcoal face pack, belong to the cosmetics sphere of life.
Background technology
Facial film is a kind of cosmetics and skincare product applied on the face, plays effect clean, vigorous and graceful and protection face.Increasing moisture of skin is the basis of beauty and skin care, and the skin dried out is can be dry coarse, form microgroove, pigmentation, causes many skin problems.As commercial goods snow is full of the whitening plant mask, its main component is Radix Ophiopogonis extract, the peach extract, and Flos Carthami extract, the Radix Asparagi extract, Radix Angelicae Sinensis extract, cucurbitaceous plant, green tea extract, Folium Vaccinii vitis-idaeae is general, has the effect of moisturizing whitening.These groups advocate to start with from antioxidation and moisturizing, have certain whitening skin and preserving moisture effect, but a little less than the effect of wrinkle removal.
Bamboo charcoal face pack can be cleared up epidermis, prevent that skin pore from stopping up and clearing up the pore stopped up, CN101194885(2010-5-19) disclose a kind of bamboo charcoal face pack, yet its anti-performance that always subtracts tamper in wrinkle, enhancing skin elasticity, unclogging all haves much room for improvement.
Summary of the invention
The purpose of this invention is to provide a kind of anti-preparation method that always subtracts the bamboo charcoal face pack of tamper in wrinkle, enhancing skin elasticity, energy unclogging.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A kind of preparation method of bamboo charcoal face pack, it comprises the following steps successively:
The preparation of A, decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, bamboo charcoal face pack: tea juice and Sucus Cucumidis sativi 15-20 part, Herba Menthae 0.5-1.8 part, Ovum Gallus domesticus album 3-5 part and water 40-50 part of taking by weight steps A gained decoction liquor, 1-8 part particle diameter 8000-12500 purpose bamboo charcoal powder, 30-40 part; Carry out the microwave vacuum processing after all substances are mixed, then pour in the facial film mould, cooling, prepare the bamboo charcoal face pack finished product.
Particle diameter 8000-12500 purpose bamboo charcoal powder has the super large surface area of extremely strong absorption property, is particularly suitable for being used in the beauty and skin care field, if particle diameter order number is too little, absorption property is not good; If particle diameter order number is too large, be difficult to play skin effect; Herba Menthae is can be calm refrigerant, it is antibiotic to sterilize, pore refining; Sucus Cucumidis sativi and Ovum Gallus domesticus album can strengthen skin elasticity; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in tea juice, can prevent skin aging and recover skin elasticity.
In decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, especially is applicable to the sensitivity skin, and can plays frosted Exfoliating Scrub effect; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium be rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care, can prevent pachylosis and aging, contributes to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can prevent that face is dry, prevent skin aging and recover skin elasticity.The decoction liquor formed according to each umber proportioning of the present invention, anti-the effective of wrinkle, enhancing skin elasticity that always subtract.
When prepared by facial film, by microwave vacuum of the present invention, process, heat effect and non-thermal effect occur in each component simultaneously, during carry out microwave radiation heating, electromagnetic field in microwave is with several hundred million even billions of inferior frequency inverted directions of per second, make polarization and this polarization of the different electric charges of material internal not possess the ability of catching up with rapidly alternating electric field, cause the material internal friction and generate heat, i.e. so-called " interior heating ", make each component in facial film mutually blend, and some reactions may occur, finally make the anti-wrinkle that always subtracts of facial film composition performance of the present invention, strengthen skin elasticity, the excellent results of tamper in unclogging.
As preferably, described step B microwave vacuum treatment conditions are: after all substances are mixed
Send in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
As preferably, described bamboo charcoal powder makes by the following method:
1., add the bamboo of splitting broken and preliminarily dried through blocking from top in vertical moving bed, bamboo relies on gravity to move down gradually, experience successively dry section, pre-char zone, char zone, calcining zone and cooling zone, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged and is entered the Bamboo vinegar solution condenser from top, and condensation obtains Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out the staged intensification, make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., the bamboo charcoal upper step made prepares particle diameter 8000-12500 purpose powdered carbon.
More preferably, described bamboo charcoal powder is 5 parts, particle diameter 10000-12000 order.
As preferably, described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid.
As preferably, Folium Perillae and Folium Camelliae sinensis that to include weight ratio in described tea juice be 1:4-9.
As preferably, the preparation method of described tea juice is:
(1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtained the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
More preferably, described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in described step (2), the solids concentration of the first concentrated solution is 15%-20%.
Because the excessive concentration of the first concentrated solution is the overlong time of reverse osmosis, fragrance is worsened, the too low vacuum concentration overlong time that makes next step of concentration, also brown stain and make the fragrance oxidation.
More preferably, in described step (2), the solids concentration of the second concentrated solution is 33%-35%.
The excessive concentration of the second concentrated solution is the vacuum concentration overlong time, and concentration is too low can not get enough products.
Temperature while more preferably, concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃.
More preferably, in described step (2), the temperature of vacuum concentration is 40-45 ℃.
The accompanying drawing explanation
Fig. 1 is the temperature control system schematic diagram of the vertical moving bed of bamboo charcoal carbonization of the present invention.
In figure, the A-dry section; The pre-char zone of B-; The C-char zone; The D-calcining zone; The E-cooling zone; F-is with the temperature sensing device of CPU; D1/d2/d3-oxidizer entrance hole; The t1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed that the bamboo charcoal powder preparation is used is divided into dry section A, pre-char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D mono-side is distributed with the many oxidizer entrance holes that can regulate closure or openness, as d1, d2, d3 etc., opposite side is to point for measuring temperature that each aperture place should be arranged as t1, t2, t3 etc., and each aperture place temperature shows by the temperature sensing device F be connected with this point for measuring temperature.
Embodiment mono-
Bamboo charcoal powder preparation: in vertical moving bed dry distillation carbonizing furnace, carry out pilot scale, bamboo chip (being about 36cm) with average moisture content 39%, the temperature of each point for measuring temperature, dry section A is 150 ℃, pre-char zone B is 275 ℃, char zone C is 450 ℃, the temperature of D district combustion zone diverse location shown in observation Fig. 1 during intensification, when the somewhere, combustion zone is as too low as the temperature of d2, open the aperture at this place, importing air locally burns, this place's temperature is raise, control the combustion zone temperature that experiences in the bamboo folding process and be warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then be warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min from 700 ℃, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 40 ℃.Continuous operation takes out bamboo charcoal after 10 days (not comprising the warm stove time).Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.Then prepared by the bamboo charcoal made to particle diameter 80000-10000 purpose powdered carbon.
The preparation method of tea juice is: (1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is that mass ratio is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water and fully soak 2 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtained the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution be at 40 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 30%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 5 parts of oatmeals, 3 parts of Semen Sesami Nigrums, Semen sojae atricolor 5-10 part, 4 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 3 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal face pack: take by weight 40 parts, tea juice, step C gained decoction liquor and 15 parts of Sucus Cucumidis sativis, 0.5 part of Herba Menthae, 3 parts of the Ovum Gallus domesticus album of 30 parts of bamboo charcoal powder, the step B gained of 1 part of steps A gained and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.09MPaMPa; Carry out microwave treatment, microwave frequency is 245MHz again, and microwave treatment time is 0.5min.Then all substances after microwave vacuum being processed are poured in the facial film mould, are cooled to room temperature, prepare the bamboo charcoal face pack finished product.
Embodiment bis-
The preparation of bamboo charcoal powder: in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, carry out pilot scale, ancestor's bamboo chip in the Meng (being about 40cm) with average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃, pre-char zone B is 270 ℃, char zone C is 500 ℃, during intensification, from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion, burn simultaneously, make combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min, and then be warming up to 1500 ℃ and be incubated 8h with the speed of 15 ℃/min from 750 ℃, spray into steam 60min in 1500 ℃ of districts, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, drop temperature is 30 ℃.Continuous operation takes out bamboo charcoal after 8 days (not comprising the warm stove time), the solution of the bamboo charcoal of taking-up being put into to acid content 4% soaks 2h, takes out with clear water and cleans, and then puts into and dries kiln drying 1h.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.Then prepared by the bamboo charcoal made to particle diameter 10000-12000 purpose powdered carbon.
The preparation method of tea juice is: (1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water and fully soak 2.5 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtained the first concentrated solution of solid contents 20%; Half of getting the first concentrated solution is at 45 ℃ of vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 10 parts of oatmeals, 5 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal face pack: take by weight 50 parts, tea juice, step C gained decoction liquor and 20 parts of Sucus Cucumidis sativis, 1.8 parts of Herba Menthaes, 5 parts of the Ovum Gallus domesticus album of 40 parts of bamboo charcoal powder, the step B gained of steps A gained 1-8 part and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.06MPa; Carry out microwave treatment, microwave frequency is 400MHz again, and microwave treatment time is 1min.Then all substances after microwave vacuum being processed are poured in the facial film mould, are cooled to room temperature, prepare the bamboo charcoal face pack finished product.
Embodiment tri-
The preparation of bamboo charcoal powder is with embodiment mono-.Then prepared by the bamboo charcoal made to particle diameter 8000-9000 purpose powdered carbon.
The preparation method of tea juice is: (1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water and fully soak 1.5 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtained the first concentrated solution of solid contents 15%; Half of getting the first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight 8 parts of oatmeals, 4 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal face pack: take by weight 45 parts, tea juice, step C gained decoction liquor and 18 parts of Sucus Cucumidis sativis, 1 part of Herba Menthae, 4 parts of the Ovum Gallus domesticus album of 35 parts of bamboo charcoal powder, the step B gained of steps A gained 1-8 part and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.08MPa; Carry out microwave treatment, microwave frequency is 300MHz again, and microwave treatment time is 0.8min.Then all substances after microwave vacuum being processed are poured in the facial film mould, are cooled to room temperature, prepare the bamboo charcoal face pack finished product.
Embodiment tetra-
The preparation of bamboo charcoal powder is with embodiment bis-.Then prepared by the bamboo charcoal made to particle diameter 12000-12500 purpose powdered carbon.
The preparation method of tea juice is: (1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water and fully soak 2.8 hours, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtained the first concentrated solution of solid contents 10%; Half of getting the first concentrated solution be at 43 ℃ of vacuum concentration, obtains solid contents and be the second concentrated solution of 34%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
The preparation of decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 13%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 32%-35%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal face pack: take by weight 48 parts, tea juice, step C gained decoction liquor and 16 parts of Sucus Cucumidis sativis, 0.8 part of Herba Menthae, 5 parts of the Ovum Gallus domesticus album of 33 parts of bamboo charcoal powder, the step B gained of 5 parts of steps A gained and water; Carry out the microwave vacuum processing after will all substances mixing: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum be-0.07MPa; Carry out microwave treatment, microwave frequency is 345MHz again, and microwave treatment time is 0.5min.Then all substances after microwave vacuum being processed are poured in the facial film mould, are cooled to room temperature, prepare the bamboo charcoal face pack finished product.
In order to understand better the present invention, below will improve the technique effect that the present invention has will be described by clinical experiment report.
1, user data: select forehead, buccal section, mouthful week place or cervical region wrinkle patient 60 examples are arranged, each 30 examples of men and women, age 30-45 year.Be divided at random two groups: use group (Chinese medicine extraction liquid adds the skin nutrient) 30 examples, each 15 examples of men and women, 38 ± 7 years old age, matched group (carrageenan adds water) 30 examples, each 15 examples of men and women, 36 ± 8 years old age.
Respectively organize sex, age, the skin symptom integration of user before use there are no significant difference (P > 0.05), there is comparability.
2, experiment material:
(1) use group of the present invention:
The use group: containing the skin-nourishing thing, press embodiment 1 preparation in the composition of facial film used, prepared by (2) matched group facial film by the following method:
Matched group:
Prescription: carrageenan 11g, ethyl hydroxybenzoate, make 1000g.
Method for making: water adds carrageenan after being heated to 80-90 ℃, and ethyl hydroxybenzoate fully stirs 5 minutes, regulates pH value to 5.5-6.5, film forming, packing, sterilizing.
3, experimental technique:
The use group: user is lain on the back, and after washing one's face, with facial film of the present invention, spreads on face, after about 15min, washes away.3 times weekly, be 2 weeks the course for the treatment of.
Matched group: the patient lies on the back, and after washing one's face, with matched group, facial film (not drug ingredients) and embodiment 1 facial film 1. spreads on face, after about 15min, washes away.3 times weekly, be 2 weeks the course for the treatment of.
4, symptom scores standard: forehead, the plain wrinkle person of buccal respectively are designated as 2 minutes, there is the blackhead forehead, the thick tail stricture of vagina of buccal section, position, face trigonum the person respectively are designated as 4 minutes, forehead, buccal section, mouthful week place and cervical region have obvious wrinkle, face and nose region to have the pimple of blackhead and white shape tamper respectively to be designated as 6 minutes.Microgroove shoals and is designated as 1 minute, and forehead, the thick tail stricture of vagina of buccal section shoal and be designated as 2 minutes, forehead, buccal section, mouthful week place and cervical region have obvious wrinkle, blackhead and tamper pimple to shoal to be designated as 3 minutes, wrinkle disappearance, blackhead and tamper pimple disappear and are designated as 0 minute.
5, efficacy assessment standard:
First by formula-clinical symptoms integration score value improvement rate=(symptom integral score value after symptom integral score value before using-uses)/-use front score value * 100% to calculate the improvement rate, then adopt following standard rating curative effect.
Produce effects: symptom integral score value improvement rate >=70%;
Effectively: symptom integral score value improvement rate >=50%;
Invalid: symptom has no obvious improvement or instead sees deterioration, symptom integral score value improvement rate<50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, and mean ± standard deviation for measurement data (x ± s) means.Before and after two groups of experimenters use, symptom score more all adopts the t check, and two groups of experimenter's Clinical efficacy comparisons adopt X
2check.
7, result of the test
Before and after use group and matched group are used, symptom scores is relatively in Table 1, and before and after use group and matched group are used, curative effect is relatively in Table 2, as known from Table 2, facial film wrinkle removal total effective rate of the present invention, up to 83%, is observed without finding skin heating, flushing through the use group, edema, the convulsion untoward reaction such as itch.
Before and after table 1 use group and matched group are used, symptom scores compares (x ± s)
Table 2 use group and matched group curative effect are relatively
From use group and the matched group of table 1 and table 2, compare, standard variance P<0.01, illustrate the evident in efficacy of this facial film.
This specific embodiment is only explanation of the invention; it is not limitation of the present invention; those skilled in the art can make to the present embodiment the modification that there is no creative contribution as required after reading this description, but as long as all are subject to the protection of Patent Law in claim scope of the present invention.
Claims (6)
1. the preparation method of a bamboo charcoal face pack is characterized in that: comprise the following steps:
The preparation of A, decoction liquor: take by weight oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtained the first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrated with reverse osmosis membrane, obtain the second decocting liquid of solid contents 30%-40%; Then merge the first decocting liquid and the second decocting liquid obtains described decoction liquor;
The preparation of B, bamboo charcoal face pack: tea juice and Sucus Cucumidis sativi 15-20 part, Herba Menthae 0.5-1.8 part, Ovum Gallus domesticus album 3-5 part and water 40-50 part of taking by weight steps A gained decoction liquor, 1-8 part particle diameter 8000-12500 purpose bamboo charcoal powder, 30-40 part; Carry out the microwave vacuum processing after all substances are mixed, then pour in the facial film mould, cooling, prepare the bamboo charcoal face pack finished product.
2. the preparation method of a kind of bamboo charcoal face pack according to claim 1, it is characterized in that: described step B microwave vacuum treatment conditions are: after will all substances mixing, send in the microwave vacuum tank, then carry out evacuation process to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment, microwave frequency is 245MHz～400MHz again, and microwave treatment time is 0.5～1min.
3. the preparation method of a kind of bamboo charcoal face pack according to claim 2, it is characterized in that: the preparation method of described tea juice is:
(1), first Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Folium Perillae and Folium Camelliae sinensis, add in deionized water fully immersion 2-3 hour, then pour in countercurrent extraction machine and extracted, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out to ultra-filtration filters, then the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtained the first concentrated solution of solid contents 5%-20%; Half of getting the first concentrated solution carried out vacuum concentration, and obtaining solid contents is the second concentrated solution of 30%-35%; Remaining the first concentrated solution and the second concentrated solution are mixed to get to tea juice.
4. the preparation method of a kind of bamboo charcoal face pack according to claim 3, it is characterized in that: described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
5. the preparation method of a kind of bamboo charcoal face pack according to claim 3, it is characterized in that: in described step (2), the solids concentration of the first concentrated solution is 15%-20%.
6. the preparation method of a kind of bamboo charcoal face pack according to claim 3, it is characterized in that: the temperature while concentrating with reverse osmosis membrane in described step (2) is 20-40 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103575622A CN102860972B (en) | 2012-09-24 | 2012-09-24 | Preparation method of bamboo charcoal mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103575622A CN102860972B (en) | 2012-09-24 | 2012-09-24 | Preparation method of bamboo charcoal mask |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102860972A CN102860972A (en) | 2013-01-09 |
| CN102860972B true CN102860972B (en) | 2013-12-11 |
Family
ID=47440292
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012103575622A Expired - Fee Related CN102860972B (en) | 2012-09-24 | 2012-09-24 | Preparation method of bamboo charcoal mask |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102860972B (en) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101194885B (en) * | 2006-12-08 | 2010-05-19 | 何柏军 | Bamboo charcoal face pack |
| CN101518508B (en) * | 2009-03-31 | 2011-11-09 | 东方药林药业有限公司 | Beautifying health composition and facial mask |
| CN101991525A (en) * | 2009-08-13 | 2011-03-30 | 常立芝 | Health-care bamboo charcoal mask and preparation technology thereof |
-
2012
- 2012-09-24 CN CN2012103575622A patent/CN102860972B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN102860972A (en) | 2013-01-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102836112B (en) | Acne-removing bamboo charcoal facial mask | |
| CN102578339A (en) | Chinese herb tea capable of clearing heat and reducing internal heat, and preparation method thereof | |
| CN104305788A (en) | Wild chrysanthemum soothing tea health-care medicine pillow and preparation method thereof | |
| CN102988264A (en) | Ginkgo leaf freckle removing whitening cream and preparation method thereof | |
| CN102836116B (en) | Method for preparing bamboo charcoal eye mask | |
| CN107372943A (en) | A kind of aid digestion pre- anti-halitosis health protection tea and its preparation method and application | |
| CN102836101B (en) | Method for preparing anti-acne bamboo charcoal mask | |
| CN102526316A (en) | Chinese medicinal formulation for preventing and treating senile dementia and production method thereof | |
| CN102836102B (en) | Method for preparing bamboo charcoal facial cleanser | |
| CN102836103B (en) | Bamboo charcoal facial cleanser | |
| CN102836100B (en) | Method for preparing bamboo charcoal silk mask | |
| CN102836113B (en) | Bamboo charcoal facial mask | |
| CN102836104B (en) | Bamboo charcoal-cocoon fiber facial mask | |
| CN104666896A (en) | Orally-taken medicine for treating alopecia seborrhoeica and preparation method for orally-taken medicine | |
| CN104873433A (en) | Moxa skin cream and preparing method thereof | |
| CN102860972B (en) | Preparation method of bamboo charcoal mask | |
| CN106720637A (en) | One kind is relieved inflammation or internal heat nti-freckle tealeaves and its preparation technology | |
| CN104069144A (en) | Three formula granules for forming Shengmai powder and preparation method thereof | |
| CN104984065A (en) | Traditional Chinese medicine for treating ulcerative colitis | |
| CN105663006A (en) | White poria cocos traditional Chinese medicine facial mask and preparing method | |
| CN102836117B (en) | Bamboo charcoal eye mask | |
| CN103961570B (en) | It is a kind of to treat Chinese medicine preparation of acute and chronic nephritis and preparation method thereof | |
| CN108714176A (en) | It is a kind of to treat Chinese medicine with grey hair | |
| CN1686186A (en) | Eight-Gem capsule and its preparation method | |
| CN103830524A (en) | Traditional Chinese medicine for treating aphtha caused by deficiency of liver-yin and kidney-yin and hyperactivity of deficiency fire and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131211 Termination date: 20140924 |
|
| EXPY | Termination of patent right or utility model |