CN102836104B - Bamboo charcoal-cocoon fiber facial mask - Google Patents
Bamboo charcoal-cocoon fiber facial mask Download PDFInfo
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- CN102836104B CN102836104B CN 201210357556 CN201210357556A CN102836104B CN 102836104 B CN102836104 B CN 102836104B CN 201210357556 CN201210357556 CN 201210357556 CN 201210357556 A CN201210357556 A CN 201210357556A CN 102836104 B CN102836104 B CN 102836104B
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Abstract
The invention relates to a bamboo charcoal-cocoon fiber facial mask, which belongs to the living field of cosmetics. The bamboo charcoal-cocoon fiber facial mask consists of the following components in parts by weight: 1-8 parts of bamboo charcoal powder of 8,000-125,000 meshes, 15-20 parts of cucumber juice, 0.5-1.8 parts of squalane, 3-5 parts of fibroin, 30-40 parts of tea liquor, 40-50 parts of water and the balance of decoction, wherein the decoction is obtained by extracting from the following components in parts by weight through a decoction method: 5-10 parts of oat flour, 3-5 parts of black sesame, 5-10 parts of soybean, 4-6 parts of common bletilla pseudobulb and 3-5 parts of Chinese angelica powder. The bamboo charcoal-cocoon fiber facial mask disclosed by the invention can be used for preventing ageing, reducing wrinkles, improving skin elasticity and clearing obstruction in pores.
Description
Technical field
The present invention relates to a kind of bamboo charcoal silkworm silk facial film, belong to the cosmetics sphere of life.
Background technology
Facial film is a kind of cosmetics and skincare product that applies on the face, plays the effect of cleaning, fitness and protection face.Increasing moisture of skin is the basis of beauty and skin care, and the skin that dries out is can be dry coarse, form microgroove, pigmentation, causes many skin problems.Be full of the plant mask of whitening as commercial goods snow, its main component is Radix Ophiopogonis extract, the peach extract, and Flos Carthami extract, the Radix Asparagi extract, Radix Angelicae Sinensis extract, cucurbitaceous plant, green tea extract, Folium Vaccinii vitis-idaeae is general, the effect that having preserves moisture whitens.These groups are advocated and to preserve moisture from antioxidation and are started with, and have certain whitening skin and preserving moisture effect, but a little less than the effect of wrinkle removal.
Bamboo charcoal face pack can be cleared up epidermis, prevent the pore that skin pore stops up and cleaning is stopped up, CN101194885(2010-5-19) disclose a kind of bamboo charcoal face pack, yet its anti-performance that subtracts tamper in wrinkle, enhancing skin elasticity, the unclogging always haves much room for improvement all.
Summary of the invention
The purpose of this invention is to provide a kind of anti-bamboo charcoal silkworm silk facial film that subtracts tamper in wrinkle, enhancing skin elasticity, the energy unclogging always.
Above-mentioned technical purpose of the present invention is achieved by the following technical programs:
A kind of bamboo charcoal silkworm silk facial film, its one-tenth by following weight portion is grouped into: 1-8 part particle diameter 8000-12500 purpose bamboo charcoal powder, Sucus Cucumidis sativi 15-20 part, squalane 0.5-1.8 part, fibroin 3-5 part, tea juice 30-40 part, water 40-50 part and decoction liquor; Described decoction liquor is extracted by decocting method by following compositions in portion by weight and is obtained: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part.
Particle diameter 8000-12500 purpose bamboo charcoal powder has the super large surface area of extremely strong absorption property, is particularly suitable for being used in the beauty and skin care field, if particle diameter order number is too little, then absorption property is not good; If particle diameter order number is too big, then be difficult to play skin effect; Squalane can suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, and to delay skin aging, improvement and elimination eye pouch and black eye all have tangible physiologic effect; The penetration of fibroin hydrolyzed solution is extremely strong, be applied to skin about 10 seconds, fibroin just can infiltrate skin matter layer, the performance insulation effect, it sees through horny layer and is combined with epiderm skin, and by cell as alimentation, participate in and the promotion cellular metabolism, for its metabolism provides essential nutrient, can also repair the skin that has damaged, promote the effect of skin cell regeneration.Sucus Cucumidis sativi and fibroin can strengthen skin elasticity; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in the tea juice can prevent skin aging and recover skin elasticity.
In the decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, especially is fit to the sensitivity skin, and can plays frosted Exfoliating Scrub effect; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium that is rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care can prevent pachylosis and aging, help to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can prevent facial drying, prevents skin aging and recover skin elasticity.According to the decoction liquor that each umber proportioning of the present invention is formed, anti-the effective of wrinkle, enhancing skin elasticity that subtract always.
As preferably, described bamboo charcoal powder makes by the following method:
1., in vertical moving bed, add through blocking the bamboo of splitting broken and preliminarily dried from the top, bamboo relies on gravity to move down gradually, experience dry section, pre-char zone, char zone, calcining zone and cooling zone successively, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged from the top and is entered the Bamboo vinegar solution condenser, and condensation gets Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out the staged intensification, make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., will go up the bamboo charcoal that makes of step and prepare particle diameter 8000-12500 purpose powdered carbon.
More preferably, described bamboo charcoal powder is 5 parts, particle diameter 10000-12000 order.
As preferably, described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 30%-40%; Merge first decocting liquid and second decocting liquid then.
As preferably, include Folium Perillae and Folium Camelliae sinensis that weight ratio is 1:4-9 in the described tea juice.
As preferably, the preparation method of described tea juice is:
(1), earlier Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water fully immersion 2-3 hour, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution carried out vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
More preferably, described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in the described step (2), the solids concentration of first concentrated solution is 15%-20%.
Because the excessive concentration of first concentrated solution is the overlong time of reverse osmosis then, fragrance is worsened, concentration is crossed the low vacuum concentration overlong time that then makes next step, also brown stain and make the fragrance oxidation.
More preferably, in the described step (2), the solids concentration of second concentrated solution is 33%-35%.
The excessive concentration of second concentrated solution is the vacuum concentration overlong time then, and concentration is crossed low enough products that then can not get.
Temperature when more preferably, concentrating with reverse osmosis membrane in the described step (2) is 20-40 ℃.
More preferably, the temperature of vacuum concentration is 40-45 ℃ in the described step (2).
In addition, the present invention also provides a kind of preparation method of bamboo charcoal silkworm silk facial film, and it may further comprise the steps successively:
A, bamboo charcoal powder preparation:
Described bamboo charcoal powder makes by the following method:
1., in vertical moving bed, add through blocking the bamboo of splitting broken and preliminarily dried from the top, bamboo relies on gravity to move down gradually, experience dry section, pre-char zone, char zone, calcining zone and cooling zone successively, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged from the top and is entered the Bamboo vinegar solution condenser, and condensation gets Bamboo vinegar solution; Control the temperature difference of described combustion zone diverse location and carry out the staged intensification, make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., will go up the bamboo charcoal that makes of step and prepare particle diameter 8000-12500 purpose powdered carbon;
The preparation of B, tea juice:
The preparation method of described tea juice is: (1), elder generation clean Folium Perillae and Folium Camelliae sinensis, pulverize, and press the weight ratio of 1:4-9 and mix Folium Perillae and Folium Camelliae sinensis, add abundant the immersion 2-3 hour in the deionized water, pour in the countercurrent extraction machine then and extract, and obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution carried out vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice;
The preparation of C, decoction liquor: take by weighing oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part by weight, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 30%-40%; Merge first decocting liquid then and second decocting liquid obtains described decoction liquor;
The preparation of D, bamboo charcoal silkworm silk facial film: take by weighing the bamboo charcoal powder of steps A gained 1-8 part, tea juice, step C gained decoction liquor and Sucus Cucumidis sativi 15-20 part, squalane 0.5-1.8 part, fibroin 3-5 part and water 40-50 part of step B gained 30-40 part by weight; Handle carrying out microwave vacuum after all substances mixing, pour into then in the facial film mould, bamboo charcoal silkworm silk facial film finished product is prepared in cooling.
As preferably, described step D microwave vacuum treatment conditions are: after all substances are mixed
Send in the microwave vacuum jar, carry out then evacuation handle to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment again, microwave frequency is 245MHz～400MHz, and microwave treatment time is 0.5～1min.
Description of drawings
Fig. 1 is the temperature control system sketch map of the vertical moving bed of bamboo charcoal carbonization of the present invention.
Among the figure, the A-dry section; The pre-char zone of B-; The C-char zone; The D-calcining zone; The E-cooling zone; The temperature sensing device of F-band CPU; D1/d2/d3-oxidizer entrance hole; The t1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed of bamboo charcoal powder preparation use is divided into dry section A, pre-char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D one side is distributed with the many oxidizer entrance holes that can regulate closure or openness, as d1, d2, d3 etc., point for measuring temperature such as t1, t2, the t3s etc. of opposite side to each aperture place should be arranged, each aperture place temperature shows by the temperature sensing device F that is connected with this point for measuring temperature.
Embodiment one
Bamboo charcoal powder preparation: in vertical moving bed dry distillation carbonizing furnace, carry out pilot scale, bamboo chip (being about 36cm) with average moisture content 39%, the temperature of each point for measuring temperature, dry section A is 150 ℃, pre-char zone B is 275 ℃, char zone C is 450 ℃, observe the temperature of D shown in Figure 1 district combustion zone diverse location during intensification, when the temperature of somewhere, combustion zone such as d2 is crossed when low, open the aperture at this place, importing air locally burns, this place temperature is raise, and the combustion zone temperature that experiences in the folding process of control bamboo is warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then is warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min from 700 ℃, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, and drop temperature is 40 ℃.Bamboo charcoal is taken out in running back 10 days (not comprising the warm stove time) continuously.Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.Then the bamboo charcoal that makes is prepared particle diameter 8000-10000 purpose powdered carbon.
The preparation method of tea juice is: (1), elder generation clean Folium Perillae and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is that mass ratio is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water and fully soaked 2 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution be at 40 ℃ of vacuum concentration, obtains solid contents and be 30% second concentrated solution; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing 5 parts of oatmeals, 3 parts of Semen Sesami Nigrums, Semen sojae atricolor 5-10 part, 4 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 3 parts of Radix Angelicae Sinensis powders by weight, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 30%; Merge first decocting liquid then and second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal silkworm silk facial film: take by weighing 40 parts in tea juice, step C gained decoction liquor and 15 parts of Sucus Cucumidis sativis, 0.5 part of squalane, 3 parts of the fibroins of 30 parts of bamboo charcoal powder, the step B gained of 1 part of steps A gained and water by weight; Carry out microwave vacuum after will all substances mixing handles: send in the microwave vacuum jar after will all substances mixing, and carry out evacuation then and handle to vacuum and be-0.09MPaMPa; Carry out microwave treatment again, microwave frequency is 245MHz, and microwave treatment time is 0.5min.All substances after then microwave vacuum being handled are poured in the facial film mould, are cooled to room temperature, prepare bamboo charcoal silkworm silk facial film finished product.
Embodiment two
The preparation of bamboo charcoal powder: in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, carry out pilot scale, ancestor's bamboo chip in the Meng (being about 40cm) with average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃, pre-char zone B is 270 ℃, char zone C is 500 ℃, burn simultaneously from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion during intensification, make combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min, and then be warming up to 1500 ℃ and be incubated 8h with the speed of 15 ℃/min from 750 ℃, spray into steam 60min in 1500 ℃ of districts, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, and drop temperature is 30 ℃.Bamboo charcoal is taken out in running back 8 days (not comprising the warm stove time) continuously, and the solution of the bamboo charcoal that takes out being put into acid content 4% soaks 2h, takes out with clear water and cleans, and puts into oven dry kiln drying 1h then.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.Then the bamboo charcoal that makes is prepared particle diameter 10000-12500 purpose powdered carbon.
The preparation method of tea juice is: (1), elder generation clean Folium Perillae and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water and fully soaked 2.5 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain first concentrated solution of solid contents 20%; Half of getting first concentrated solution is at 45 ℃ of vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing 10 parts of oatmeals, 5 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders by weight, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 40%; Merge first decocting liquid then and second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal silkworm silk facial film: take by weighing 50 parts in tea juice, step C gained decoction liquor and 20 parts of Sucus Cucumidis sativis, 1.8 parts of squalanes, 5 parts of the fibroins of 40 parts of bamboo charcoal powder, the step B gained of steps A gained 1-8 part and water by weight; Carry out microwave vacuum after will all substances mixing handles: send in the microwave vacuum jar after will all substances mixing, and carry out evacuation then and handle to vacuum and be-0.06MPa; Carry out microwave treatment again, microwave frequency is 400MHz, and microwave treatment time is 1min.All substances after then microwave vacuum being handled are poured in the facial film mould, are cooled to room temperature, prepare bamboo charcoal silkworm silk facial film finished product.
Embodiment three
The preparation of bamboo charcoal powder is with embodiment one.Then the bamboo charcoal that makes is prepared particle diameter 8000-9000 purpose powdered carbon.
The preparation method of tea juice is: (1), elder generation clean Folium Perillae and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water and fully soaked 1.5 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain first concentrated solution of solid contents 15%; Half of getting first concentrated solution be at 45 ℃ of vacuum concentration, obtains solid contents and be 35% second concentrated solution; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing 8 parts of oatmeals, 4 parts of Semen Sesami Nigrums, 10 parts of Semen sojae atricolor, 6 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 5 parts of Radix Angelicae Sinensis powders by weight, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 35%; Merge first decocting liquid then and second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal silkworm silk facial film: take by weighing 45 parts in tea juice, step C gained decoction liquor and 18 parts of Sucus Cucumidis sativis, 1 part of squalane, 4 parts of the fibroins of 35 parts of bamboo charcoal powder, the step B gained of steps A gained 1-8 part and water by weight; Carry out microwave vacuum after will all substances mixing handles: send in the microwave vacuum jar after will all substances mixing, and carry out evacuation then and handle to vacuum and be-0.08MPa; Carry out microwave treatment again, microwave frequency is 300MHz, and microwave treatment time is 0.8min.All substances after then microwave vacuum being handled are poured in the facial film mould, are cooled to room temperature, prepare bamboo charcoal silkworm silk facial film finished product.
Embodiment four
The preparation of bamboo charcoal powder is with embodiment two.Then the bamboo charcoal that makes is prepared particle diameter 12000-12500 purpose powdered carbon.
The preparation method of tea juice is: (1), elder generation clean Folium Perillae and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water and fully soaked 2.8 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtain first concentrated solution of solid contents 10%; Half of getting first concentrated solution be at 43 ℃ of vacuum concentration, obtains solid contents and be 34% second concentrated solution; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part by weight, get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 13%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 32%-35%; Merge first decocting liquid then and second decocting liquid obtains described decoction liquor.
The preparation of bamboo charcoal silkworm silk facial film: take by weighing 48 parts in tea juice, step C gained decoction liquor and 16 parts of Sucus Cucumidis sativis, 0.8 part of squalane, 5 parts of the fibroins of 33 parts of bamboo charcoal powder, the step B gained of 5 parts of steps A gained and water by weight; Carry out microwave vacuum after will all substances mixing handles: send in the microwave vacuum jar after will all substances mixing, and carry out evacuation then and handle to vacuum and be-0.07MPa; Carry out microwave treatment again, microwave frequency is 345MHz, and microwave treatment time is 0.5min.All substances after then microwave vacuum being handled are poured in the facial film mould, are cooled to room temperature, prepare bamboo charcoal silkworm silk facial film finished product.
In order to understand the present invention better, will improve by clinical experiment report below the technique effect that the present invention has will be described.
1, user data: select forehead, buccal portion, mouthful week the place or cervical region wrinkle patient 60 examples are arranged, each 30 example of men and women, age 30-45 year.Be divided into two groups at random: use group (Chinese medicine extraction liquid adds the skin nutrient) 30 examples, each 15 example of men and women, 38 ± 7 years old age, matched group (carrageenan adds water) 30 examples, each 15 example of men and women, 36 ± 8 years old age.
Respectively organize sex, age, the skin symptom integration of user before the use there are no significant difference (P〉0.05), have comparability.
2, experiment material:
(1) use group of the present invention:
The use group: contain the skin-nourishing thing in the composition of used facial film, press embodiment 1 preparation, (2) matched group facial film prepares by the following method:
Matched group:
Prescription: carrageenan 11g, ethyl hydroxybenzoate is made 1000g.
Method for making: water adds carrageenan after being heated to 80-90 ℃, and ethyl hydroxybenzoate fully stirred 5 minutes, regulates pH value to 5.5-6.5, film forming, packing, sterilization.
3, experimental technique:
The use group: user is lain on the back, and after washing one's face, spreads on face with facial film of the present invention, flush away behind about 15min.3 times weekly, be 2 weeks the course for the treatment of.
Matched group: the patient lies on the back, and after washing one's face, spreads on face, flush away behind about 15min with matched group facial film (not drug ingredients) and embodiment 1 facial film 1..3 times weekly, be 2 weeks the course for the treatment of.
4, clinical symptoms standards of grading: forehead, the plain wrinkle person of buccal respectively are designated as 2 fens, there is the blackhead forehead, the thick tail stricture of vagina of buccal portion, position, face trigonum the person respectively are designated as 4 fens, forehead, buccal portion, mouthful week the place and cervical region have obvious wrinkle, face and nose region to have the pimple of blackhead and white shape tamper respectively to be designated as 6 fens.Microgroove shoals and is designated as 1 fen, and forehead, the thick tail stricture of vagina of buccal portion shoal and be designated as 2 fens, forehead, buccal portion, mouthful week the place and cervical region have obvious wrinkle, blackhead and tamper pimple to shoal to be designated as 3 fens, wrinkle disappearance, blackhead and tamper pimple disappear and are designated as 0 fen.
5, efficacy assessment standard:
By formula earlier-clinical symptoms integration score value improvement rate=(symptom integral score value before using-use back symptom integral score value)/score value * 100% calculates the improvement rate before using, and adopts following standard rating curative effect then.
Produce effects: symptom integral score value improvement rate 〉=70%;
Effectively: symptom integral score value improvement rate 〉=50%;
Invalid: symptom is not seen obvious improvement or is instead seen deterioration, symptom integral score value improvement rate＜50%.
6, statistical procedures: total data adopts SPSS 13.0 statistics softwares to carry out statistical analysis, measurement data mean ± standard deviation (x ± s) expression.Symptom score more all adopted the t check before and after two groups of experimenters used, and two groups of experimenter's clinical efficacies relatively adopt X
2Check.
7, result of the test
The clinical symptoms scoring relatively saw Table 1 before and after use group and matched group used, and curative effect relatively saw Table 2 before and after use group and matched group used, as known from Table 2, facial film wrinkle removal total effective rate of the present invention is observed nothing through the use group and is found skin heating, flushing up to 83%, the untoward reaction such as itch of edema, convulsion.
Clinical symptoms scoring comparison before and after table 1 use group and matched group use (x ± s)
Table 2 use group and matched group curative effect are relatively
Compare from use group and the matched group of table 1 and table 2, standard variance P＜0.01 illustrates the evident in efficacy of this facial film.
This specific embodiment only is explanation of the invention; it is not limitation of the present invention; those skilled in the art can make the modification that does not have creative contribution to present embodiment as required after reading this description, but as long as all are subjected to the protection of Patent Law in claim scope of the present invention.
Claims (7)
1. bamboo charcoal silkworm silk facial film, it is characterized in that: the one-tenth by following weight portion is grouped into: 1-8 part particle diameter 8000-12500 purpose bamboo charcoal powder, Sucus Cucumidis sativi 15-20 part, squalane 0.5-1.8 part, fibroin 3-5 part, tea juice 30-40 part, water 40-50 part and decoction liquor; Described decoction liquor is extracted by decocting method by following compositions in portion by weight and is obtained: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part;
Described decocting method is: get described oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get described Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate with reverse osmosis membrane, obtain second decocting liquid of solid contents 30%-40%; Merge first decocting liquid and second decocting liquid then.
2. a kind of bamboo charcoal silkworm silk facial film according to claim 1, it is characterized in that: described bamboo charcoal powder makes by the following method:
1., in vertical moving bed, add through blocking the bamboo of splitting broken and preliminarily dried from the top, bamboo relies on gravity to move down gradually, experience dry section, pre-char zone, char zone, calcining zone and cooling zone successively, the pyrolysis gas that char zone produces makes the bamboo drying and reaches carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, pyrolysis gas is discharged from the top and is entered the Bamboo vinegar solution condenser, and condensation gets Bamboo vinegar solution; Control the temperature difference of described calcining zone diverse location and carry out the staged intensification, make the calcining zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min with the speed of 5-15 ℃/min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min; One side of described calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of described calcining zone has the point for measuring temperature at described aperture place;
2., will go up the bamboo charcoal that makes of step and prepare particle diameter 8000-12500 purpose powdered carbon.
3. a kind of bamboo charcoal silkworm silk facial film according to claim 2, it is characterized in that: described bamboo charcoal powder is 5 parts, particle diameter 10000-12000 order.
4. a kind of bamboo charcoal silkworm silk facial film according to claim 3, it is characterized in that: the preparation method of described tea juice is:
(1), earlier Folium Perillae and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Folium Perillae and Folium Camelliae sinensis, add in the deionized water fully immersion 2-3 hour, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution carried out vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; The first remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
5. a kind of bamboo charcoal silkworm silk facial film according to claim 4, it is characterized in that: described Folium Camelliae sinensis is the ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
6. a kind of bamboo charcoal silkworm silk facial film according to claim 5, it is characterized in that: in the described step (2), the solids concentration of first concentrated solution is 15%-20%.
7. a kind of bamboo charcoal silkworm silk facial film according to claim 6 is characterized in that: the temperature when concentrating with reverse osmosis membrane in the described step (2) is 20-40 ℃.
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| CN111000787A (en) * | 2019-12-18 | 2020-04-14 | 宜春大海龟生命科学有限公司 | Facial mask and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101721331A (en) * | 2008-10-22 | 2010-06-09 | 高娜娜 | Moisturizing and skin rejuvenating facial mask |
| CN101961303A (en) * | 2010-09-26 | 2011-02-02 | 郑蓉才 | Facial mask and preparation method thereof |
| CN101991525A (en) * | 2009-08-13 | 2011-03-30 | 常立芝 | Health-care bamboo charcoal mask and preparation technology thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101721331A (en) * | 2008-10-22 | 2010-06-09 | 高娜娜 | Moisturizing and skin rejuvenating facial mask |
| CN101991525A (en) * | 2009-08-13 | 2011-03-30 | 常立芝 | Health-care bamboo charcoal mask and preparation technology thereof |
| CN101961303A (en) * | 2010-09-26 | 2011-02-02 | 郑蓉才 | Facial mask and preparation method thereof |
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