CN102836103A - Bamboo charcoal facial cleanser - Google Patents
Bamboo charcoal facial cleanser Download PDFInfo
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- CN102836103A CN102836103A CN2012103575552A CN201210357555A CN102836103A CN 102836103 A CN102836103 A CN 102836103A CN 2012103575552 A CN2012103575552 A CN 2012103575552A CN 201210357555 A CN201210357555 A CN 201210357555A CN 102836103 A CN102836103 A CN 102836103A
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Abstract
The invention relates to a bamboo charcoal facial cleanser, which belongs to the field of life of cosmetics. The bamboo charcoal facial cleanser is composed of the following components by weight: 1 to 8 parts of nano bamboo charcoal powder, 1.5 to 2 parts of sodium alginate, 0.3 to 0.8 parts of alkyl glycoside, 2 to 3 parts of jojoba oil, 0.5 to 1.8 parts of squalane, 0.5 to 0.8 parts of preservative, 3 to 5 parts of glycerol, 30 to 40 parts of tea extract, 40 to 50 parts of de-ionized water and a decoction; the decoction is obtained by extracting the following components by weight through a decoction process, namely 5 to 10 parts of oat powder, 3 to 5 parts of semen sesami nigrum, 5 to 10 parts of soybeans, 4 to 6 parts of bletilla striata and 3 to 5 parts of angelica sinensis powder. The facial cleanser provided by the invention is capable of effectively cleansing the faces, ensuring the skin to keep moist, strengthening oxidation resistance and antianaphylaxis of the skin.
Description
Technical field
The present invention relates to a kind of bamboo charcoal facial milk cleanser, belong to the household chemicals field.
Background technology
If existing in the market cleansing milk such as cleansing milk Bian are processed by the synthetic wetting agent of more single surfactant compound, thereby reach the purpose of decontamination.Owing to used a large amount of surfactants, cause the undue defat of epiderm skin easily, thereby make skin relatively drier, more serious meeting causes the irreversibility infringement to skin, and function singleness, can't satisfy the demand of user to the multiple efficacies of skin care.
CN101427987 (2010-12-15) provide a kind of face cleaning skin lotion product and preparation method thereof; Yet this product is formed by purifying frost and cleaning agent; Use inconvenient, and its clean-up performance, performance of keeping humidity and the effect of skin non-oxidizability and antiallergic property all had much room for improvement.
Summary of the invention
The purpose of this invention is to provide and a kind ofly can effectively clean face, guarantee the bamboo charcoal facial milk cleanser that skin keeps moistening, strengthens skin non-oxidizability and antiallergic property.
Above-mentioned technical purpose of the present invention is achieved through following technical scheme: a kind of bamboo charcoal facial milk cleanser, and its one-tenth by following weight portion is grouped into: 1-8 part bamboo charcoal nano powder, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part, deionized water 40-50 part and decoction liquor; Said decoction liquor is extracted through decocting method by following compositions in portion by weight and is obtained: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part.
Alkyl polyglucoside is a kind of non-ionic surface active agent of gentle environmental protection.Sodium alginate is the polysaccharide-sodium alginate that is derived from Sargassum, is prone to form gel.
The bamboo charcoal nano powder has the super large surface area of extremely strong absorption property; Be particularly suitable for being used in the beauty and skin care field, and apply at facial zone after other combinations of substances, can play massage effect; Its infrared effect can be played the magnetic therapy radiation effects to eye, helps blood circulation promoting; Squalane can suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, to strengthening skin non-oxidizability and elasticity tangible physiologic effect is arranged; The antioxidation of intrinsic tea polyphenols, theanine, tea polysaccharide and radiation-resisting functional in the tea juice can keep skin moistening.The Jojoba oil main component is unsaturated higher alcohol and fatty acid, and good stable property is arranged, and very easily merges with skin, has non-oxidizability free from worldly cares.In addition, Jojoba oil also contains and enriches vitamin, has to nourish softening skin and the effect that keeps skin wet.
In the decoction liquor of the present invention, Herba bromi japonici is rich in microorganism and mineral and various nutrition, can give skin more moisture, mixes the stimulation that can alleviate skin with other materials, especially is fit to the sensitivity skin; Semen Sesami Nigrum is rich in anthocyanidin, has remarkable anti-aging effects, and its selenium that is rich in and various vitamin, can make skin be full of gloss and elasticity; Semen sojae atricolor is rich in dimension E and lecithin, can prevent skin aging and recover skin elasticity; Pseudobulbus Bletillae (Rhizoma Bletillae) convergence granulation promoting, skin care can prevent that pachylosis from aging, helping to recover skin elasticity.Radix Angelicae Sinensis is rich in 17 seed amino acids and 23 kinds of inorganic elementss of abundant dimension A, E, B12 and needed by human, can strengthen skin non-oxidizability and antiallergic property.According to the decoction liquor that each umber proportioning of the present invention is formed, can effectively eliminate eye pouch and black eye.
The present invention fully utilizes the gel emulsification and the moisture-keeping function of sodium alginate and alkyl polyglucoside mixture; And mix with bamboo charcoal nano powder of the present invention, decoction liquor and tea juice; Prove through crowd's trial effect; Can when effectively cleaning face, guarantee that skin keeps moistening, strengthens skin non-oxidizability and antiallergic property.
As preferably, said antiseptic is sorbic acid or sodium diacetate.
As preferably, said bamboo charcoal powder makes through following method:
1., in vertical moving bed, add through blocking the bamboo of splitting broken and preliminarily dried from the top; Bamboo relies on gravity to move down gradually; Experience dry section, preparatory char zone, char zone, calcining zone and cooling zone successively; The pyrolysis gas that char zone produces makes bamboo dry and reach carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, and pyrolysis gas is discharged entering Bamboo vinegar solution condenser from the top, and condensation gets Bamboo vinegar solution; Control the temperature difference of said combustion zone diverse location and carry out the staged intensification; Make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min with the speed of 5-15 ℃/min; One side of said calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of said calcining zone has the point for measuring temperature at said aperture place;
2., will go up the bamboo charcoal that makes of step and prepare the bamboo charcoal nano powder.
More preferably, the particle diameter 100-200nm of said bamboo charcoal powder.
As preferably, said decocting method is: get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate, obtain second decocting liquid of solid contents 30%-40% with reverse osmosis membrane; Merge first decocting liquid and second decocting liquid then.
As preferably, include Radix Hamamelidis Mollis and Folium Camelliae sinensis that weight ratio is 1:4-9 in the said tea juice.
As preferably, the method for preparing of said tea juice is:
(1), earlier Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water fully immersion 2-3 hour, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution carried out vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
Through decocting method of the present invention, can fully utilize the non-oxidizability of Radix Hamamelidis Mollis and tea juice, help skin to mend wet and quiet flesh.
More preferably, said Folium Camelliae sinensis is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
More preferably, in the said step (2), the solids concentration of first concentrated solution is 15%-20%, and the solids concentration of second concentrated solution is 33%-35%.
Because the excessive concentration of first concentrated solution is the overlong time of reverse osmosis then; Fragrance is worsened, and concentration is crossed the low vacuum concentration overlong time that then makes next step, also brown stain and make the fragrance oxidation; The excessive concentration of second concentrated solution is the vacuum concentration overlong time then, and concentration is crossed low enough products that then can not get.
More preferably, the temperature when using reverse osmosis membrane to concentrate in the said step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
The present invention is according to following scheme implementation:
A), the preparation of decoction liquor: take by weighing oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part by weight; Get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor; Add 3-5 times of decocting and boil 4-5h; Filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate, obtain second decocting liquid of solid contents 30%-40% with reverse osmosis membrane; Merge first decocting liquid then and second decocting liquid obtains said decoction liquor;
B), the preparation of bamboo charcoal facial milk cleanser: take by weighing step a) gained decoction liquor, 1-8 part bamboo charcoal nano powder, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part and deionized water 40-50 part by weight; All materials are mixed and stirring and emulsifying, carry out the microwave vacuum processing then and obtain the bamboo charcoal facial milk cleanser.
As preferably, the microwave vacuum treatment conditions of said step b) are: with sending in the microwave vacuum jar behind all material mixing and emulsifyings, carry out then evacuation handle to vacuum for-0.09MPa～-0.06MPa; Carry out microwave treatment again, microwave frequency is 245MHz～400MHz, and microwave treatment time is 0.5～1min.
Handle through microwave vacuum of the present invention, heat effect and non-thermal effect take place in each component simultaneously, during carry out microwave radiation heating; Electromagnetic field in the microwave is with several hundred million times of per second even billions of inferior frequency inverted direction; Make the polarization and this polarization of the different electric charges of material internal not possess the ability of catching up with alternating electric field rapidly, cause the material internal friction and generate heat promptly so-called " internal heating "; Make each component in the facial film blend each other; Emulsifying is uniform and complete more, and some other reactions possibly take place, the function that facial milk cleanser of the present invention is played massage face, effectively cleaning is facial, the maintenance of assurance skin is moistening, strengthens skin non-oxidizability and antiallergic property.
Description of drawings
Fig. 1 is the temperature control system sketch map of the vertical moving bed of bamboo charcoal carbonization of the present invention.
Among the figure, the A-dry section; The preparatory char zone of B-; The C-char zone; The D-calcining zone; The E-cooling zone; The temperature sensing device of F-band CPU; D1/d2/d3-oxidizer entrance hole; The t1/t2/t3-point for measuring temperature.
The specific embodiment
As shown in Figure 1, the vertical moving bed that the bamboo charcoal powder preparation is used is divided into dry section A, preparatory char zone B, char zone C, calcining zone D and cooling zone E.Calcining zone D one side is distributed with the many oxidizer entrance holes that can regulate closure or openness; Like d1, d2, d3 etc.; Opposite side is to point for measuring temperature that each aperture place should be arranged such as t1, t2, t3 etc., and each aperture place temperature shows through the temperature sensing device F that is connected with this point for measuring temperature.
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Embodiment one
Bamboo charcoal powder preparation: in vertical moving bed dry distillation carbonizing furnace, carry out pilot scale, with the bamboo chip (being about 36cm) of average moisture content 39%, the temperature of each point for measuring temperature; Dry section A is 150 ℃, and char zone B is 275 ℃ in advance, and char zone C is 450 ℃; Observe the temperature of D shown in Figure 1 district combustion zone diverse location during intensification, cross when low, open the aperture at this place when the temperature of somewhere, combustion zone such as d2; Importing air locally burns; This place temperature is raise, and the combustion zone temperature that experiences in the folding process of control bamboo is warming up to 700 ℃ and be incubated 40min with the speed of 5 ℃/min, and then is warming up to 1100 ℃ and be incubated 2h with the speed of 5 ℃/min from 700 ℃; Bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, and drop temperature is 40 ℃.Bamboo charcoal is taken out in continuous operation back 10 days (not comprising the warm stove time).Bamboo charcoal quality: average fixed carbon (combustible basis) content 96%, resistance value 0.5 Ω/cm, content of ashes 0.5%, the average 900mg/g of iodine sorption value, pH value 7.The powdered carbon that then bamboo charcoal that makes is prepared particle diameter 100nm.
The method for preparing of tea juice is: (1), elder generation clean Radix Hamamelidis Mollis and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is that mass ratio is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1 mixes; Press the weight ratio of 1:4 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water and fully soaked 2 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 20 ℃, obtain first concentrated solution of solid contents 5%; Get the half the of first concentrated solution, obtain solid contents and be 30% second concentrated solution at 40 ℃ of vacuum concentration; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing oatmeal 5kg, Semen Sesami Nigrum 3kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4kg, Radix Angelicae Sinensis powder 3kg; Get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3 times of decoctings and boil 4h, filter; Filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1 times of decocting and boil 6h, filter, concentrate, obtain second decocting liquid of solid contents 30% with reverse osmosis membrane; Merge first decocting liquid then and second decocting liquid obtains said decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 5kg bamboo charcoal nano powder, sodium alginate 1.9kg, alkyl polyglucoside 0.7kg, Jojoba oil 2.3kg, squalane 0.5kg, sorbic acid 0.5kg, glycerol 3.5kg, tea juice 33kg, deionized water 48kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying is carried out microwave vacuum then and is handled: the material after the stirring and emulsifying sent in the microwave vacuum jar, carried out evacuation then and handle to vacuum and be-0.09MPa; Carry out microwave treatment again, microwave frequency is 245MHz, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Cleansing milk provided by the invention is checked through the PLA Air Force General Hospital, and the experimenter is totally 100 people, wherein male 8 people, women 92 people, age 18-62 one full year of life.Method for using is: the experimenter directly uses and receives trial product; Every day, each used once sooner or later, before using face was drenched with clear water, extruded an amount of cleansing milk according to the invention in the centre of the palm; Add a small amount of clear water and rubbed and enrich foam, massage is moments later clean with flushing with clean water in face.Adhered to using one month, inspection once has or not whole body and local untoward reaction with understanding at least weekly, and the itemized record result.
Use the effect of embodiment 1 compositions:
The experimenter is totally 25 people, wherein male 2 people, women 23 people.Use after one month; The experimenter all representes to use the salubrious non-greasy of face after embodiment 1 compositions, can effectively clean dirt; And that skin keeps for a long time is moistening, clearly compact and high resilience, and the face mask lines use the good in oxidation resistance of back skin than more clear clearly demarcated before using; The local skin untoward reaction appears in the equal end of experimenter, does not also have the little good reactions of whole body such as anorexia, diarrhoea, weak, endocrine regulation, uses the antiallergic property of back skin good.
Embodiment two
The preparation of bamboo charcoal powder: in the tubulation moving bed dry distillation carbonizing furnace of 16 pipe disjunctors, carry out pilot scale; With ancestor's bamboo chip in the Meng (being about 40cm) of average moisture content 30%, the temperature of each point for measuring temperature, dry section A is 200 ℃; Char zone B is 270 ℃ in advance; Char zone C is 500 ℃, burns simultaneously from external-burning lead-in portion combustion gas and the not condensing gas of Bamboo vinegar solution condenser portion during intensification, makes combustion zone temperature be warming up to 750 ℃ and be incubated 80min with the speed of 15 ℃/min; And then be warming up to 1500 ℃ and be incubated 8h from 750 ℃ with the speed of 15 ℃/min; Spray into steam 60min in 1500 ℃ of districts, bamboo charcoal cooling pipe and Bamboo vinegar solution condenser adopt natural cooling, and drop temperature is 30 ℃.Bamboo charcoal is taken out in continuous operation back 8 days (not comprising the warm stove time), and the solution of the bamboo charcoal that takes out being put into acid content 4% soaks 2h, takes out with clear water and cleans, and puts into oven dry kiln drying 1h then.Bamboo charcoal quality: average fixed carbon (combustible basis) content 95%, resistance value 0.4 Ω/cm, content of ashes 0.4%, specific surface area 1200m2/g, the average 800mg/g of iodine sorption value, pH value 7.The powdered carbon that then bamboo charcoal that makes is prepared grain 120nm.
The method for preparing of tea juice is: (1), elder generation clean Radix Hamamelidis Mollis and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:2 mixes; Press the weight ratio of 1:9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water and fully soaked 2.5 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain first concentrated solution of solid contents 20%; Get the half the of first concentrated solution, obtain solid contents and be 33% second concentrated solution at 45 ℃ of vacuum concentration; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing oatmeal 10kg, Semen Sesami Nigrum 5kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg; Get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter; Filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 20%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 2 times of decoctings and boil 7h, filter, concentrate, obtain second decocting liquid of solid contents 40% with reverse osmosis membrane; Merge first decocting liquid then and second decocting liquid obtains said decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 2kg bamboo charcoal nano powder, sodium alginate 1.8kg, alkyl polyglucoside 0.5kg, Jojoba oil 2.5kg, squalane 1kg, sodium diacetate 0.6kg, glycerol 4kg, tea juice 35kg, deionized water 45kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying is carried out microwave vacuum then and is handled: the material after the stirring and emulsifying sent in the microwave vacuum jar, carried out evacuation then and handle to vacuum and be-0.06MPa; Carry out microwave treatment again, microwave frequency is 400MHz, and microwave treatment time is 1min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Test method is used the effect of embodiment 2 compositionss with embodiment one:
The experimenter is totally 25 people, wherein male 2 people, women 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, does not have systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulation yet.Wherein 22 experimenters represent to use the salubrious non-greasy of face after embodiment 2 compositionss, can effectively clean dirt, and skin keeps moistening for a long time, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 3 subject perception have massage and whitening effect when washing one's face, but effect is obvious inadequately.
Embodiment three
The preparation of bamboo charcoal powder is with embodiment one.The bamboo charcoal powder that then bamboo charcoal that makes is prepared particle diameter 150nm.
The method for preparing of tea juice is: (1), elder generation clean Radix Hamamelidis Mollis and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.5 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water and fully soaked 1.5 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate; (2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 40 ℃, obtain first concentrated solution of solid contents 15%; Get the half the of first concentrated solution, obtain solid contents and be 35% second concentrated solution at 45 ℃ of vacuum concentration; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing oatmeal 8kg, Semen Sesami Nigrum 4kg, Semen sojae atricolor 10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 6kg, Radix Angelicae Sinensis powder 5kg; Get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 5 times of decoctings and boil 5h, filter; Filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 20%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.5 times of decoctings and boil 6.5h, filter, concentrate, obtain second decocting liquid of solid contents 35% with reverse osmosis membrane; Merge first decocting liquid then and second decocting liquid obtains said decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 8kg bamboo charcoal nano powder, sodium alginate 2kg, alkyl polyglucoside 0.8kg, Jojoba oil 3kg, squalane 1.8kg, methyl hydroxybenzoate 0.8kg, glycerol 5kg, tea juice 40kg, deionized water 50kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying is carried out microwave vacuum then and is handled: the material after the stirring and emulsifying sent in the microwave vacuum jar, carried out evacuation then and handle to vacuum and be-0.08MPa; Carry out microwave treatment again, microwave frequency is 300MHz, and microwave treatment time is 0.8min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Use the effect of embodiment 3 compositionss:
The experimenter is totally 25 people, wherein male 2 people, women 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, does not have systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulation yet.Wherein 21 experimenters represent to use the salubrious non-greasy of face after embodiment 3 compositionss, can effectively clean dirt, and skin keeps moistening for a long time, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 4 subject perception have massage and whitening effect when washing one's face, but effect is obvious inadequately.
Embodiment four
The preparation of bamboo charcoal powder is with embodiment two.The bamboo charcoal powder that then bamboo charcoal that makes is prepared particle diameter 200nm.
The method for preparing of tea juice is: (1), elder generation clean Radix Hamamelidis Mollis and Folium Camelliae sinensis, pulverize, and wherein, Folium Camelliae sinensis is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1.8 mixes; Press the weight ratio of 1:5 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water and fully soaked 2.8 hours, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane at 25 ℃, obtain first concentrated solution of solid contents 10%; Get the half the of first concentrated solution, obtain solid contents and be 34% second concentrated solution at 43 ℃ of vacuum concentration; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
The preparation of decoction liquor: take by weighing oatmeal 5-10kg, Semen Sesami Nigrum 3-5kg, Semen sojae atricolor 5-10kg, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6kg, Radix Angelicae Sinensis powder 3-5kg; Get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor; Add 3-5 times of decocting and boil 4-5h; Filter, filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 13%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1.1 times of decoctings and boil 6.8h, filter, concentrate, obtain second decocting liquid of solid contents 32%-35% with reverse osmosis membrane; Merge first decocting liquid then and second decocting liquid obtains said decoction liquor.
The preparation of bamboo charcoal facial milk cleanser: 1kg bamboo charcoal nano powder, sodium alginate 1.5kg, alkyl polyglucoside 0.3kg, Jojoba oil 2kg, squalane 0.5kg, propyl hydroxybenzoate 0.5kg, glycerol 3kg, tea juice 30kg, deionized water 40kg and above-mentioned decoction liquor are mixed; Stirring and emulsifying is carried out microwave vacuum then and is handled: the material after the stirring and emulsifying sent in the microwave vacuum jar, carried out evacuation then and handle to vacuum and be-0.07MPa; Carry out microwave treatment again, microwave frequency is 345MHz, and microwave treatment time is 0.5min, and discharging is cooled to room temperature and obtains the bamboo charcoal facial milk cleanser.
Use the effect of embodiment 4 compositionss:
The experimenter is totally 25 people, wherein male 2 people, women 23 people.Use after one month, the local skin untoward reaction does not all appear in the experimenter, does not have systemic adverse reactions such as anorexia, diarrhoea, weak, endocrine regulation yet.Wherein 20 experimenters represent to use the salubrious non-greasy of face after embodiment 4 compositionss, can effectively clean dirt, and skin keeps moistening for a long time, clearly compacts and high resilience, and the face mask lines are than more clear clearly demarcated before using; 5 subject perception have massage and whitening effect when washing one's face, but effect is obvious inadequately.
This specific embodiment only is to explanation of the present invention; It is not a limitation of the present invention; Those skilled in the art can make the modification that does not have creative contribution to present embodiment as required after reading this description, but as long as in claim scope of the present invention, all receive the protection of Patent Law.
Claims (10)
1. bamboo charcoal facial milk cleanser, it is characterized in that: the one-tenth by following weight portion is grouped into: 1-8 part bamboo charcoal nano powder, sodium alginate 1.5-2 part, alkyl polyglucoside 0.3-0.8 part, Jojoba oil 2-3 part, squalane 0.5-1.8 part, antiseptic 0.5-0.8 part, glycerol 3-5 part, tea juice 30-40 part, deionized water 40-50 part and decoction liquor; Said decoction liquor is extracted through decocting method by following compositions in portion by weight and is obtained: oatmeal 5-10 part, Semen Sesami Nigrum 3-5 part, Semen sojae atricolor 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 4-6 part, Radix Angelicae Sinensis powder 3-5 part.
2. a kind of bamboo charcoal facial milk cleanser according to claim 1 is characterized in that: said antiseptic is sorbic acid or sodium diacetate.
3. a kind of bamboo charcoal facial milk cleanser according to claim 2, it is characterized in that: said bamboo charcoal powder makes through following method:
1., in vertical moving bed, add through blocking the bamboo of splitting broken and preliminarily dried from the top; Bamboo relies on gravity to move down gradually; Experience dry section, preparatory char zone, char zone, calcining zone and cooling zone successively; The pyrolysis gas that char zone produces makes bamboo dry and reach carbonization temperature in dry section and bamboo adverse current or cross-flow from bottom to top, and pyrolysis gas is discharged entering Bamboo vinegar solution condenser from the top, and condensation gets Bamboo vinegar solution; Control the temperature difference of said combustion zone diverse location and carry out the staged intensification; Make the combustion zone that experiences in the bamboo folding process be warming up to 700-750 ℃ and be incubated 40-80min, and then be warming up to 1000-1500 ℃ and be incubated 2-8h with the speed of 5-15 ℃/min with the speed of 5-15 ℃/min; One side of said calcining zone is distributed with the aperture of scalable closure or openness, and the opposite side correspondence of said calcining zone has the point for measuring temperature at said aperture place;
2., will go up the bamboo charcoal that makes of step and prepare the bamboo charcoal nano powder.
4. a kind of bamboo charcoal facial milk cleanser according to claim 3 is characterized in that: the particle diameter 100-200nm of said bamboo charcoal powder.
5. a kind of bamboo charcoal facial milk cleanser according to claim 4; It is characterized in that: said decocting method is: get said oatmeal, Semen Sesami Nigrum and Semen sojae atricolor, add 3-5 times of decocting and boil 4-5h, filter; Filtered solution is concentrated with reverse osmosis membrane, obtain first decocting liquid of solid contents 5%-20%; Get said Pseudobulbus Bletillae (Rhizoma Bletillae) and Radix Angelicae Sinensis powder, add 1-2 times of decocting and boil 6-7h, filter, concentrate, obtain second decocting liquid of solid contents 30%-40% with reverse osmosis membrane; Merge first decocting liquid and second decocting liquid then.
6. a kind of bamboo charcoal facial milk cleanser according to claim 5, it is characterized in that: said decocting method is: include Radix Hamamelidis Mollis and Folium Camelliae sinensis that weight ratio is 1:4-9 in the said tea juice.
7. a kind of bamboo charcoal facial milk cleanser according to claim 6, it is characterized in that: said decocting method is: the method for preparing of said tea juice is:
(1), earlier Radix Hamamelidis Mollis and Folium Camelliae sinensis are cleaned, pulverize, press the weight ratio of 1:4-9 and mix Radix Hamamelidis Mollis and Folium Camelliae sinensis, add in the deionized water fully immersion 2-3 hour, pour in the countercurrent extraction machine then and extract, obtain coarse filtration liquid; Coarse filtration liquid is tentatively filtered with the secondary filter film that contains the polypropylene fibre membrane cartridge, remove the fine particle in the coarse filtration liquid, obtain preliminary filtrate;
(2), preliminary filtrate is carried out ultra-filtration filters, again the ultrafiltration permeate is concentrated with reverse osmosis membrane, obtain first concentrated solution of solid contents 5%-20%; Half of getting first concentrated solution carried out vacuum concentration, and obtaining solid contents is second concentrated solution of 30%-35%; First remaining concentrated solution and the mixing of second concentrated solution are obtained tea juice.
8. a kind of bamboo charcoal facial milk cleanser according to claim 7 is characterized in that: said Folium Camelliae sinensis is ripe tea of Folium camelliae assamicae and the Ramulus et Folium Mussaendae Pubescentis that 1:1-2 mixes.
9. a kind of bamboo charcoal facial milk cleanser according to claim 8 is characterized in that: the solids concentration of first concentrated solution is 15%-20%, and the solids concentration of second concentrated solution is 33%-35%.
10. a kind of bamboo charcoal facial milk cleanser according to claim 9 is characterized in that: the temperature when using reverse osmosis membrane to concentrate in the said step (2) is 20-40 ℃, and the temperature of vacuum concentration is 40-45 ℃.
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| CN201210357555.2A CN102836103B (en) | 2012-09-24 | 2012-09-24 | Bamboo charcoal facial cleanser |
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| CN201210357555.2A CN102836103B (en) | 2012-09-24 | 2012-09-24 | Bamboo charcoal facial cleanser |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103239375A (en) * | 2013-05-05 | 2013-08-14 | 洪圣娟 | Cypress charcoal oil absorption washing powder for men |
| CN104434648A (en) * | 2014-11-17 | 2015-03-25 | 青岛厚科信息工程有限公司 | Antibacterial facial cleanser and preparation method thereof |
| CN106309306A (en) * | 2016-08-17 | 2017-01-11 | 倪娟形 | Skin care facial cleanser and preparation method thereof |
| CN111362248A (en) * | 2018-12-25 | 2020-07-03 | 成都易生玄科技有限公司 | Production method of face-cleaning bamboo charcoal |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1723877A (en) * | 2005-05-27 | 2006-01-25 | 徐建国 | Cleansing milk contg. bamboo charcoal |
| CN101245294A (en) * | 2007-09-05 | 2008-08-20 | 江苏隆力奇生物科技股份有限公司 | Perfumed soap |
-
2012
- 2012-09-24 CN CN201210357555.2A patent/CN102836103B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1723877A (en) * | 2005-05-27 | 2006-01-25 | 徐建国 | Cleansing milk contg. bamboo charcoal |
| CN101245294A (en) * | 2007-09-05 | 2008-08-20 | 江苏隆力奇生物科技股份有限公司 | Perfumed soap |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103239375A (en) * | 2013-05-05 | 2013-08-14 | 洪圣娟 | Cypress charcoal oil absorption washing powder for men |
| CN104434648A (en) * | 2014-11-17 | 2015-03-25 | 青岛厚科信息工程有限公司 | Antibacterial facial cleanser and preparation method thereof |
| CN106309306A (en) * | 2016-08-17 | 2017-01-11 | 倪娟形 | Skin care facial cleanser and preparation method thereof |
| CN111362248A (en) * | 2018-12-25 | 2020-07-03 | 成都易生玄科技有限公司 | Production method of face-cleaning bamboo charcoal |
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| CN102836103B (en) | 2014-03-12 |
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