CN102725277B - 制备二乙烯基芳烃二氧化物的方法 - Google Patents

制备二乙烯基芳烃二氧化物的方法 Download PDF

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Publication number
CN102725277B
CN102725277B CN201080058978.3A CN201080058978A CN102725277B CN 102725277 B CN102725277 B CN 102725277B CN 201080058978 A CN201080058978 A CN 201080058978A CN 102725277 B CN102725277 B CN 102725277B
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China
Prior art keywords
divinylarene
reaction
reaction mixture
yield
dvb
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201080058978.3A
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English (en)
Chinese (zh)
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CN102725277A (zh
Inventor
E·B·里普林格尔
D·简
D·L·巴劳
K·T·彭
G·古尔亚斯
B·D·胡克
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Blue Cube Intellectual Property Co Ltd
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Dow Global Technologies LLC
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/19—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02—Polycondensates containing more than one epoxy group per molecule
    • C08G59/027—Polycondensates containing more than one epoxy group per molecule obtained by epoxidation of unsaturated precursor, e.g. polymer or monomer

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)
CN201080058978.3A 2009-12-21 2010-12-17 制备二乙烯基芳烃二氧化物的方法 Expired - Fee Related CN102725277B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US28851109P 2009-12-21 2009-12-21
US61/288,511 2009-12-21
PCT/US2010/061019 WO2011084687A1 (en) 2009-12-21 2010-12-17 Process for preparing divinylarene dioxides

Publications (2)

Publication Number Publication Date
CN102725277A CN102725277A (zh) 2012-10-10
CN102725277B true CN102725277B (zh) 2016-02-03

Family

ID=43513600

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CN201080058978.3A Expired - Fee Related CN102725277B (zh) 2009-12-21 2010-12-17 制备二乙烯基芳烃二氧化物的方法

Country Status (8)

Country Link
US (1) US8674122B2 (enExample)
EP (1) EP2516409B1 (enExample)
JP (1) JP5778691B2 (enExample)
KR (1) KR20120123347A (enExample)
CN (1) CN102725277B (enExample)
BR (1) BR112012015249A2 (enExample)
TW (1) TW201136909A (enExample)
WO (1) WO2011084687A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011119655A2 (en) * 2010-03-24 2011-09-29 Dow Global Technologies Llc Process for preparing divinlylarene dioxides
EP2776412B1 (en) * 2011-11-08 2017-05-03 Blue Cube IP LLC Process for preparing a divinylarene dioxide
US9266849B2 (en) * 2011-12-07 2016-02-23 Blue Cube Ip Llc Process for recovering divinylarene dioxides
EP3010897B1 (en) 2013-06-19 2018-08-22 Blue Cube IP LLC Process and apparatus for producing divinylarene dioxide
US9943839B2 (en) 2014-07-15 2018-04-17 Northwestern University Catalyst composition and process for preparing olefin oxides
DE102018128228A1 (de) 2018-11-12 2020-05-14 Condias Gmbh Verfahren zur Oxidation kohlenstoffhaltiger organischer Verbindungen mit elektrochemisch erzeugten Oxidationsmitteln und Anordnung zur Durchführung des Verfahrens
CN115337913B (zh) * 2022-08-09 2024-03-22 浙江大学杭州国际科创中心 儿茶[9]芳烃及其制备方法和应用

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3053856A (en) * 1958-10-29 1962-09-11 Shell Oil Co Epoxidation of ethylenic compounds with peroxycarboximidic acids
CN1331669A (zh) * 1998-12-22 2002-01-16 罗狄亚化学公司 用于抑制烯属不饱和脂族单体的自由基聚合的组合物和方法
CN1355777A (zh) * 1999-06-11 2002-06-26 Basf公司 防止含烯属不饱和化合物混合物中的不需要聚合反应的方法
CN1764637A (zh) * 2003-02-28 2006-04-26 国际壳牌研究有限公司 方法
EP1307434B1 (en) * 2000-08-11 2006-12-27 Polimeri Europa S.p.A. Integrated process for the preparation of epoxides

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2977374A (en) 1961-03-28 Process for preparing oxirane
US2388235A (en) 1941-07-03 1945-11-06 Heyden Chemical Corp Nitrogen-containing resins and process of exchanging anions in fluid media
US2591573A (en) 1947-07-05 1952-04-01 Rohm & Haas Resinous insoluble reaction products of tertiary amines with haloalkylated vinyl aromatic hydrocarbon copolymers
FR2419938A1 (fr) * 1978-03-13 1979-10-12 Charbonnages Ste Chimique Procede de preparation de l'oxyde de styrene
WO1998014416A1 (en) * 1996-10-04 1998-04-09 Betzdearborn Inc. Compositions and methods for inhibiting vinyl aromatic monomer polymerization

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3053856A (en) * 1958-10-29 1962-09-11 Shell Oil Co Epoxidation of ethylenic compounds with peroxycarboximidic acids
CN1331669A (zh) * 1998-12-22 2002-01-16 罗狄亚化学公司 用于抑制烯属不饱和脂族单体的自由基聚合的组合物和方法
CN1355777A (zh) * 1999-06-11 2002-06-26 Basf公司 防止含烯属不饱和化合物混合物中的不需要聚合反应的方法
EP1307434B1 (en) * 2000-08-11 2006-12-27 Polimeri Europa S.p.A. Integrated process for the preparation of epoxides
CN1764637A (zh) * 2003-02-28 2006-04-26 国际壳牌研究有限公司 方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Influence of Cure Schedule on the Viscoelastic Properties and Thermal Degradation of Crosslinked Mono- and Diepoxides Obtained During the Reaction of Hydrogen Peroxide and Divinylbenzene;Marta Worzakowska;《Journal of Applied Polymer Science》;20071231;第103卷;第463页实验部分 *

Also Published As

Publication number Publication date
CN102725277A (zh) 2012-10-10
WO2011084687A1 (en) 2011-07-14
TW201136909A (en) 2011-11-01
US8674122B2 (en) 2014-03-18
EP2516409B1 (en) 2017-01-25
JP5778691B2 (ja) 2015-09-16
US20120253055A1 (en) 2012-10-04
EP2516409A1 (en) 2012-10-31
BR112012015249A2 (pt) 2015-09-22
JP2013515066A (ja) 2013-05-02
KR20120123347A (ko) 2012-11-08

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Effective date of registration: 20160411

Address after: michigan

Patentee after: BLUE CUBE INTELLECTUAL PROPERTY CO., LTD.

Address before: michigan

Patentee before: Dow Global Technologies Inc.

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160203

Termination date: 20171217

CF01 Termination of patent right due to non-payment of annual fee