CN102712735B - 生产硬质聚氨酯泡沫的方法 - Google Patents

生产硬质聚氨酯泡沫的方法 Download PDF

Info

Publication number
CN102712735B
CN102712735B CN201080043579.XA CN201080043579A CN102712735B CN 102712735 B CN102712735 B CN 102712735B CN 201080043579 A CN201080043579 A CN 201080043579A CN 102712735 B CN102712735 B CN 102712735B
Authority
CN
China
Prior art keywords
weight
aethoxy sklerol
components
koh
amount
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201080043579.XA
Other languages
English (en)
Chinese (zh)
Other versions
CN102712735A (zh
Inventor
C·吉斯科尔
J·克拉森
H.塞弗特
M·舒特
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN102712735A publication Critical patent/CN102712735A/zh
Application granted granted Critical
Publication of CN102712735B publication Critical patent/CN102712735B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/36Hydroxylated esters of higher fatty acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/302Water
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40High-molecular-weight compounds
    • C08G18/48Polyethers
    • C08G18/4804Two or more polyethers of different physical or chemical nature
    • C08G18/4816Two or more polyethers of different physical or chemical nature mixtures of two or more polyetherpolyols having at least three hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/66Compounds of groups C08G18/42, C08G18/48, or C08G18/52
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/66Compounds of groups C08G18/42, C08G18/48, or C08G18/52
    • C08G18/6666Compounds of group C08G18/48 or C08G18/52
    • C08G18/6696Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/36 or hydroxylated esters of higher fatty acids of C08G18/38
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • C08J9/12Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent
    • C08J9/125Water, e.g. hydrated salts
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0025Foam properties rigid
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0083Foam properties prepared using water as the sole blowing agent

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN201080043579.XA 2009-09-29 2010-09-22 生产硬质聚氨酯泡沫的方法 Active CN102712735B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09171618.3 2009-09-29
EP09171618 2009-09-29
PCT/EP2010/063935 WO2011039082A1 (de) 2009-09-29 2010-09-22 Verfahren zur herstellung von polyurethan-hartschaumstoffen

Publications (2)

Publication Number Publication Date
CN102712735A CN102712735A (zh) 2012-10-03
CN102712735B true CN102712735B (zh) 2014-01-15

Family

ID=43088379

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080043579.XA Active CN102712735B (zh) 2009-09-29 2010-09-22 生产硬质聚氨酯泡沫的方法

Country Status (12)

Country Link
EP (1) EP2483323B1 (pl)
JP (1) JP5654019B2 (pl)
KR (1) KR101792290B1 (pl)
CN (1) CN102712735B (pl)
AU (1) AU2010300146A1 (pl)
BR (1) BR112012006879A2 (pl)
ES (1) ES2443313T3 (pl)
MX (1) MX2012003659A (pl)
PL (1) PL2483323T3 (pl)
PT (1) PT2483323E (pl)
RU (1) RU2553254C2 (pl)
WO (1) WO2011039082A1 (pl)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9126386B2 (en) 2011-03-04 2015-09-08 Basf Se Composite elements
US9188384B2 (en) 2011-03-31 2015-11-17 Basf Se Dynamically evacuable devices comprising organic aerogels or xerogels
US9896558B2 (en) 2011-08-01 2018-02-20 Basf Se HFO/water-blown rigid foam systems
ES2761816T3 (es) * 2011-08-01 2020-05-21 Basf Se Sistemas de espuma rígida expandida accionados con HFO/agua
US9403963B2 (en) 2011-08-23 2016-08-02 Basf Se Particle-comprising polyether alcohols
JP5554423B2 (ja) * 2012-02-16 2014-07-23 三洋化成工業株式会社 ポリウレタン樹脂製造用ポリオール成分、ポリウレタン樹脂およびその成形品
KR20180020228A (ko) 2015-06-18 2018-02-27 바스프 에스이 강성 폴리우레탄 발포체의 제조 방법
CN105111400A (zh) * 2015-09-21 2015-12-02 河北工业大学 一种二氧化碳基聚碳酸酯聚醚多元醇-蓖麻油聚氨酯弹性体及其制备方法
EA039777B1 (ru) * 2017-03-27 2022-03-11 Басф Се Полиольные компоненты и их применение для получения жестких пенополиуретанов
US11872728B2 (en) * 2017-11-08 2024-01-16 Basf Se Vegetable oil as foam stabilizer in PU boots manufacturing

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1110972A (zh) * 1994-03-17 1995-11-01 拜尔公司 含氨酯、脲及缩二脲基团的硬泡沫塑料的制法及用途
EP0900811A1 (de) * 1997-09-06 1999-03-10 Th. Goldschmidt AG Verwendung von cyclischen organischen Carbonaten bei der Produktion von Polyurethanschäumen
CN101484494A (zh) * 2006-07-04 2009-07-15 亨茨曼国际有限公司 制备粘弹性泡沫塑料的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2639083C2 (de) * 1976-08-31 1983-02-10 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Polyätherpolyolen und ihre Verwendung als Ausgangsmaterialien für Polyurethankunststoffe
CA2132595C (en) 1993-09-22 1999-03-16 Thomas L. Fishback Polyol composition having good flow and water blown rigid polyurethane foams made thereby having good dimensional stability
US6833390B2 (en) 2002-07-22 2004-12-21 Bayer Polymers Llc Process for preparing closed-cell water-blown rigid polyurethane foams having improved mechanical properties
JP4263028B2 (ja) 2003-06-20 2009-05-13 東洋ゴム工業株式会社 硬質ポリウレタンフォーム用ポリオール組成物及び硬質ポリウレタンフォームの製造方法
CN101068843B (zh) 2004-09-30 2011-05-04 东邦化学工业株式会社 硬质聚氨酯泡沫的制造方法
JP2007217648A (ja) 2006-02-20 2007-08-30 Nippon Polyurethane Ind Co Ltd 水発泡硬質ポリイソシアヌレートフォーム形成用組成物、該組成物を用いた水発泡硬質ポリイソシアヌレートフォームの製造方法、及び該製造方法により得られる水発泡硬質ポリイソシアヌレートフォーム
US7671105B2 (en) * 2006-08-22 2010-03-02 Basf Corporation Resin composition and an article formed therefrom

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1110972A (zh) * 1994-03-17 1995-11-01 拜尔公司 含氨酯、脲及缩二脲基团的硬泡沫塑料的制法及用途
EP0900811A1 (de) * 1997-09-06 1999-03-10 Th. Goldschmidt AG Verwendung von cyclischen organischen Carbonaten bei der Produktion von Polyurethanschäumen
CN101484494A (zh) * 2006-07-04 2009-07-15 亨茨曼国际有限公司 制备粘弹性泡沫塑料的方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘益军.聚氨酯原料及助剂手册.《聚氨酯原料及助剂手册》.化学工业出版社,2005,(第一版), *

Also Published As

Publication number Publication date
CN102712735A (zh) 2012-10-03
RU2553254C2 (ru) 2015-06-10
KR101792290B1 (ko) 2017-10-31
JP2013506042A (ja) 2013-02-21
EP2483323B1 (de) 2013-12-04
BR112012006879A2 (pt) 2016-06-07
EP2483323A1 (de) 2012-08-08
PL2483323T3 (pl) 2014-04-30
AU2010300146A1 (en) 2012-04-19
ES2443313T3 (es) 2014-02-18
PT2483323E (pt) 2013-12-19
WO2011039082A1 (de) 2011-04-07
MX2012003659A (es) 2012-04-30
JP5654019B2 (ja) 2015-01-14
RU2012117409A (ru) 2013-11-10
KR20120094921A (ko) 2012-08-27

Similar Documents

Publication Publication Date Title
CN102712735B (zh) 生产硬质聚氨酯泡沫的方法
US11505670B2 (en) Polyurethane foams co-blown with a mixture of a hydrocarbon and a halogenated olefin
CN105940032B (zh) 用于制备硬质聚氨酯或氨基甲酸酯改性聚异氰脲酸酯泡沫体的方法
WO2013030101A1 (en) Polyurethane rigid foams
CN102858832B (zh) 生产硬质聚氨酯泡沫的方法
CN101970534B (zh) 绝热的基于基异氰酸酯的泡沫体
CN101641386A (zh) 顺式和/或反式-邻-环己二胺引发的多元醇及由其制备的硬质聚氨酯泡沫材料
US20110218262A1 (en) Preparing rigid polyurethane foams
CN102781996A (zh) 制备聚氨酯硬质泡沫材料的方法
TR201708752T4 (tr) Köpük izolasyon ünitesi.
CA2988878C (en) Method for producing a rigid polyurethane foam
MX2011010059A (es) Produccion de espumas de poliuretano rigido y uso de las mismas.
CN101652400A (zh) 胺引发的多元醇以及由其制备的硬质聚氨酯泡沫材料
NZ231622A (en) Preparation of rigid closed-cell polyurethane foams in which water comprises at least part of the blowing agent; polyol compositions
CN102947364A (zh) 生产聚氨酯硬质泡沫材料的方法
US5449699A (en) Rigid closed cell polyisocyanate based foams for use as positive flotation materials in watercraft
TW201321426A (zh) 硬質發泡合成樹脂之製造方法
CN102112513B (zh) 亚甲基双(环己胺)-引发的多元醇和从该多元醇制得的硬质聚氨酯泡沫体
SG183523A1 (en) Method for producing polyurethanes
CN102164978A (zh) 基于邻-环己烷二胺引发的多元醇的硬质聚氨酯泡沫体系统
CN109642004B (zh) 聚氨酯泡沫和包含其的聚氨酯复合材料
US5552447A (en) Rigid closed cell polyisocyanate based foams for use as positive flotation materials in watercraft
JP2002515527A (ja) 連続気泡硬質ポリウレタンフォームを製造するためのポリオールブレンド
WO2020046779A1 (en) Methods for formulating polyisocyanurate foam-forming compositions, related polyisocyanurate foam-forming compositions, and foams produced thereby
CN112469752A (zh) 泡沫组合物和由其制成的泡沫复合材料

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant