CN102633924B - 低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法 - Google Patents

低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法 Download PDF

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Publication number
CN102633924B
CN102633924B CN 201210153253 CN201210153253A CN102633924B CN 102633924 B CN102633924 B CN 102633924B CN 201210153253 CN201210153253 CN 201210153253 CN 201210153253 A CN201210153253 A CN 201210153253A CN 102633924 B CN102633924 B CN 102633924B
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vinyl butyrate
aqueous solution
high molecular
homopolymerization
initiator
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Chinese (zh)
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CN102633924A (zh
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王宇
曾阳
吴美玲
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Shanghai Yuang Waterborne New Material Technology Co., Ltd.
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Shanghai Yuang Waterborne New Material Technology Co Ltd
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Priority to CN 201210153253 priority Critical patent/CN102633924B/zh
Priority to PCT/CN2012/079065 priority patent/WO2013170536A1/zh
Priority to IN2324MUN2014 priority patent/IN2014MN02324A/en
Publication of CN102633924A publication Critical patent/CN102633924A/zh
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F4/00—Polymerisation catalysts
    • C08F4/28—Oxygen or compounds releasing free oxygen
    • C08F4/32—Organic compounds
    • C08F4/38—Mixtures of peroxy-compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F126/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen
    • C08F126/06—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen by a heterocyclic ring containing nitrogen
    • C08F126/10—N-Vinyl-pyrrolidone
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/003—Removal of residual monomers by physical means from polymer solutions, suspensions, dispersions or emulsions without recovery of the polymer therefrom

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Polymerisation Methods In General (AREA)
CN 201210153253 2012-05-16 2012-05-16 低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法 Active CN102633924B (zh)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN 201210153253 CN102633924B (zh) 2012-05-16 2012-05-16 低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法
PCT/CN2012/079065 WO2013170536A1 (zh) 2012-05-16 2012-07-23 低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法
IN2324MUN2014 IN2014MN02324A (pt) 2012-05-16 2012-07-23

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Application Number Priority Date Filing Date Title
CN 201210153253 CN102633924B (zh) 2012-05-16 2012-05-16 低残单中高分子量均聚n-乙烯基丁内酰胺k60水溶液的合成方法

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CN102633924A CN102633924A (zh) 2012-08-15
CN102633924B true CN102633924B (zh) 2013-10-23

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CN (1) CN102633924B (pt)
IN (1) IN2014MN02324A (pt)
WO (1) WO2013170536A1 (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106674397A (zh) * 2015-11-11 2017-05-17 上海其福青材料科技有限公司 一种高分子量的聚乙烯吡咯烷酮的制备方法
CN106674388A (zh) * 2015-11-11 2017-05-17 上海其福青材料科技有限公司 一种降低聚乙烯吡咯烷酮中n－乙烯吡咯烷酮的方法
CN109679009A (zh) * 2019-01-02 2019-04-26 黄山邦森新材料有限公司 一种聚维酮k60的制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102093279A (zh) * 2011-01-07 2011-06-15 上海宇昂化工科技发展有限公司 高稳定非离子n-乙烯基丁内酰胺碘及相关制备方法
CN102125053A (zh) * 2011-01-07 2011-07-20 上海宇昂化工科技发展有限公司 高稳定非离子n-乙烯基丁内酰胺碘溶液及相关配制方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101508752A (zh) * 2009-03-14 2009-08-19 博爱新开源制药有限公司 一种聚乙烯吡咯烷酮的聚合方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102093279A (zh) * 2011-01-07 2011-06-15 上海宇昂化工科技发展有限公司 高稳定非离子n-乙烯基丁内酰胺碘及相关制备方法
CN102125053A (zh) * 2011-01-07 2011-07-20 上海宇昂化工科技发展有限公司 高稳定非离子n-乙烯基丁内酰胺碘溶液及相关配制方法

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
N-乙烯基丁内酰胺及其聚合体;李忠福;《高分子学报》;19600120(第01期);全文 *
应琦琮等.聚N-乙烯基丁内酰胺的分子量测定.《高分子学报》.1960,(第01期),
李忠福.N-乙烯基丁内酰胺及其聚合体.《高分子学报》.1960,(第01期),
聚N-乙烯基丁内酰胺的分子量测定;应琦琮等;《高分子学报》;19600120(第01期);全文 *

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Publication number Publication date
CN102633924A (zh) 2012-08-15
IN2014MN02324A (pt) 2015-10-09
WO2013170536A1 (zh) 2013-11-21

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