CN102603408B - Nanometer smectite clay organic compound fertilizer - Google Patents
Nanometer smectite clay organic compound fertilizer Download PDFInfo
- Publication number
- CN102603408B CN102603408B CN 201210085812 CN201210085812A CN102603408B CN 102603408 B CN102603408 B CN 102603408B CN 201210085812 CN201210085812 CN 201210085812 CN 201210085812 A CN201210085812 A CN 201210085812A CN 102603408 B CN102603408 B CN 102603408B
- Authority
- CN
- China
- Prior art keywords
- nanometer
- percent
- smectite clay
- fertilizer
- sulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Fertilizers (AREA)
Abstract
The invention provides a nanometer smectite clay organic compound fertilizer, which is made of the following raw materials in percentage by weight: 5-10 percent of urea, 2-4 percent of monoammonium phosphate, 4-6 percent of potassium sulfate, 4-7 percent of potassium dihydrogen phosphate and the like. During fertilization, a contrast test is conducted to the nutritious fertilizers provided by the invention and commonly used compound fertilizers in the gardening field, planting areas are randomly arranged, each kind of fertilizers is applied in one step and the same field management measures are adopted. According to statistics, after the compound fertilizers provided by the invention are applied, the emergence rate of seeds can reach 93 percent and the absorbing rate of the major elements by plants is increased by 11 percent by applying nanometer additives; the probability of disease infection is reduced by 4 percent and the probability of insect infection is reduced by 4.1 percent; and the yield increase rate reaches 7.5 percent.
Description
Technical field
Patent of the present invention relates to a kind of compound manure, relates in particular to a kind of nanometer smectite clay compoiste fertilizer.
Background technology
The ginseng dish originates in middle part, tropical America, is distributed in the areas such as West Africa, the torrid zone, South America and South East Asia, in the south China many places in wild state, be grown in before the room, stockaded village after eaves, also be common in that to be grown in roof Shang， colony generally more neat, cultivation domestication is easy, and the plantation of production is arranged in Guangzhou at present.The ginseng dish is contained the nutritive substances such as rich in protein, fat, calcium, VITAMIN, the edible part of every 100 grams is containing protein 1.56 grams, fatty 0.18 gram, total acid 0.06 gram, robust fibre 0.66 gram, dry-matter 6.2 grams, reducing sugar 0.44 gram, vitamins C 11.6 grams, total amino acid content 1.33 grams, 28.4 milligrams of iron, 57.17 milligrams of calcium, 3.19 milligrams, zinc.It is dual-purpose that the ginseng dish can make herbal cuisine, but the diseases such as the assisting therapy deficiency of vital energy is weak, the empty spontaneous perspiration of body, diarrhea due to hypofunction of the spleen, xeropulmonary cough, milk rareness have the effects such as promoting lactation, detumescence pain, invigorating the spleen and replenishing QI, moistening lung promote the production of body fluid.Seeding ratio is low, simultaneously due to vegetative period different steps for the demand difference of nutrition, conventional nutritive medium is cultivated and is easy to cause interim element to lack, and causes the defects such as blade is yellow, flower is little, the amount of blooming is few.
At present, fertilizer use some insoluble problems that exist, such as the utilization ratio of fertilizer is lower, too much use Chemical Fertilizer on Environment, pollute etc.; In addition, the solubilized organic carbon is the active substance in soil or aquatic ecosystem, composition and form transformation to the various microorganisms in soil or water body and various nutrients play an important role, and the biogeochemical cycle in the system of hypergene state over the ground and toxicity and the migration of heavy metal simultaneously has profound influence.In view of above problem, the present invention is studied nanometer additive, has made nanometer materials, has both had adsorptivity, dispersiveness, rheological, porousness and surface acidity, has again the surface effects of nano material, many active centre occur.Being conducive to the sorption and desorption to nitrogen, phosphorus, potassium and organic carbon, improving the benefit of using of chemical fertilizer, build good ecotope, is also development and the improvement soil of the friendly type fertilizer of efficient context, increases soil fertility scientific basis is provided.
Summary of the invention
The invention provides a kind of nanometer smectite clay compoiste fertilizer, it is characterized in that: the raw material by following each weight percentages of components forms: urea 5-10%, monoammonium phosphate 2-4%, vitriolate of tartar 4-6%, potassium primary phosphate 4-7%, the nanometer smectite clay 10-20% that the granule diameter is 10-20nm, humic acids 10-15%, BA3-5%, water 5-10%, chitosan 1-5%, borax 3-7%, zinc chloride 0.5-1%, Sodium orthomolybdate 0.05-0.3%, manganous sulfate 0.05-0.1%, Sodium dodecylbenzene sulfonate 0.05-0.3%, ferrous sulfate 0.8-2%, sal epsom 0.03-0.8%, copper sulfate 0.01-0.05%, dimethyl sulfoxide (DMSO) 0.2-2%, field crop stalk 2-10%, fowl and animal excrement 2-3%,
Described fowl and animal excrement is a kind of or any several mixing in pig manure, cow dung, sheep excrement, chicken and duck excrement;
This composite fertilizer is prepared as follows:
(1) choose the raw material of formula ratio by described parts by weight;
(2) by described field crop crushed stalk, be powder;
(3) described fowl and animal excrement, field crop stalk powder are mixed, mix thoroughly, the wet feed of banking up in fermentation vat fermentation, above cover the moisture-heat preservation material, after 60 hours, turning for the first time when in heap, temperature reaches 50-70 ℃, and every turning in 24 hours once, after 3 turnings, fermentation ends;
(4) by tunning and described urea, monoammonium phosphate, vitriolate of tartar, potassium primary phosphate, nanometer smectite clay, nano-sized carbon, humic acids, xylogen, BA, water, chitosan, borax, zinc chloride, Sodium orthomolybdate, manganous sulfate, Sodium dodecylbenzene sulfonate, ferrous sulfate, sal epsom, copper sulfate, reactor is put in the dimethyl sulfoxide (DMSO) mixing, uses water dissolution, is uniformly mixed reaction 2 hours under 100-120 ℃; After technique to be mixed completes, with 200 mesh sieve filtering solutions, remove residue.
(5) add by weight percentage described nanometer smectite clay in filtering solution, stir and obtain the finished product.
Described nanometer smectite clay preparation method is: smectite clay mixing solutions, at 0 ℃ of lower stir-activating 3 h, is added to sodium lauryl sulphate, 4 * 10
4r/min high-shear 4h, reaction soln is cooled to decompress filter after room temperature, and gained is deposited under 105 ℃ and is dried to constant weight, obtains nanometer smectite clay.
Composite fertilizer of the present invention can make fertilizer be utilized to greatest extent, and can not waste fertilizer, reduces the pollution to soil and water source, can guarantee the growth conditions of plant the best, blooms and is guaranteed; Adding of nanometer additive makes plant more easily absorb, increase production; Adding of bio-feritlizer makes fertilizer efficiency alleviate, be conducive to soil protection.
Embodiment
The present invention is implemented by the following method:
1. a nanometer smectite clay compoiste fertilizer, it is characterized in that: the raw material by following each weight percentages of components forms: urea 5-10%, monoammonium phosphate 2-4%, vitriolate of tartar 4-6%, potassium primary phosphate 4-7%, the nanometer smectite clay 10-20% that the granule diameter is 10-20nm, humic acids 10-15%, BA3-5%, water 5-10%, chitosan 1-5%, borax 3-7%, zinc chloride 0.5-1%, Sodium orthomolybdate 0.05-0.3%, manganous sulfate 0.05-0.1%, Sodium dodecylbenzene sulfonate 0.05-0.3%, ferrous sulfate 0.8-2%, sal epsom 0.03-0.8%, copper sulfate 0.01-0.05%, dimethyl sulfoxide (DMSO) 0.2-2%, field crop stalk 2-10%, fowl and animal excrement 2-3%,
Described fowl and animal excrement is a kind of or any several mixing in pig manure, cow dung, sheep excrement, chicken and duck excrement;
This composite fertilizer is prepared as follows:
(1) choose the raw material of formula ratio by described parts by weight;
(2) by described field crop crushed stalk, be powder;
(3) described fowl and animal excrement, field crop stalk powder are mixed, mix thoroughly, the wet feed of banking up in fermentation vat fermentation, above cover the moisture-heat preservation material, after 60 hours, turning for the first time when in heap, temperature reaches 50-70 ℃, and every turning in 24 hours once, after 3 turnings, fermentation ends;
(4) by tunning and described urea, monoammonium phosphate, vitriolate of tartar, potassium primary phosphate, nanometer smectite clay, nano-sized carbon, humic acids, xylogen, BA, water, chitosan, borax, zinc chloride, Sodium orthomolybdate, manganous sulfate, Sodium dodecylbenzene sulfonate, ferrous sulfate, sal epsom, copper sulfate, reactor is put in the dimethyl sulfoxide (DMSO) mixing, uses water dissolution, is uniformly mixed reaction 2 hours under 100-120 ℃; After technique to be mixed completes, with 200 mesh sieve filtering solutions, remove residue.
(5) add by weight percentage described nanometer smectite clay in filtering solution, stir and obtain the finished product.
Described nanometer smectite clay preparation method is: smectite clay mixing solutions, at 0 ℃ of lower stir-activating 3 h, is added to sodium lauryl sulphate, 4 * 10
4r/min high-shear 4h, reaction soln is cooled to decompress filter after room temperature, and gained is deposited under 105 ℃ and is dried to constant weight, obtains nanometer smectite clay.
This composite fertilizer is applied in:
(1) ginseng dish sowing time, by 200 times of described composite fertilizer dilute with waters, spray in soil during from sowing, minute sprays for 2 times, and the timed interval of twice fertilising is 3 days;
(2) ginseng dish seedling stage, by 400 times of described composite fertilizer dilute with waters, spray in soil during from sowing, evenly sprays in blade face 2 times weekly.
(3) ginseng dish is bloomed early stage, by 400 times of described composite fertilizer dilute with waters, when bud occurs, starts minute to have executed for 3 times, and the timed interval of twice fertilising is 2 days, reaches on blade around fertilizer evenly is sprayed to plant;
(4) ginseng dish flowering period, by 500 times of described composite fertilizer dilute with waters, flower occurs spraying 1 time, and fertilizer solution evenly is sprayed at around plant, avoids contacting with petal as far as possible.
In when fertilising, nutritious fertilizer of the present invention and gardening field composite fertilizer commonly used is carried out to simultaneous test, planting area arranges at random, each fertilizer adopts disposable applying, adopt same field management measure, after using by statistics composite fertilizer of the present invention, seeding ratio can reach 93%, uses nanometer additive and has promoted plant to increase to 11% to the absorption width of macroelement element; The ratio of introduced disease reduces 4%, infects insect pest and reduces 4.1%; Stimulation ratio reaches 7.5%.
Claims (1)
1. a nanometer smectite clay compoiste fertilizer, it is characterized in that: the raw material by following each weight percentages of components forms: urea 5-10%, monoammonium phosphate 2-4%, vitriolate of tartar 4-6%, potassium primary phosphate 4-7%, the nanometer smectite clay 10-20% that the granule diameter is 10-20nm, humic acids 10-15%, BA3-5%, water 5-10%, chitosan 1-5%, borax 3-7%, zinc chloride 0.5-1%, Sodium orthomolybdate 0.05-0.3%, manganous sulfate 0.05-0.1%, Sodium dodecylbenzene sulfonate 0.05-0.3%, ferrous sulfate 0.8-2%, sal epsom 0.03-0.8%, copper sulfate 0.01-0.05%, dimethyl sulfoxide (DMSO) 0.2-2%, field crop stalk 2-10%, fowl and animal excrement 2-3%,
Described fowl and animal excrement is a kind of or any several mixing in pig manure, cow dung, sheep excrement, chicken and duck excrement;
This composite fertilizer is prepared as follows:
(1) choose the raw material of formula ratio by described parts by weight;
(2) by described field crop crushed stalk, be powder;
(3) described fowl and animal excrement, field crop stalk powder are mixed, mix thoroughly, the wet feed of banking up in fermentation vat fermentation, above cover the moisture-heat preservation material, after 60 hours, turning for the first time when in heap, temperature reaches 50-70 ℃, and every turning in 24 hours once, after 3 turnings, fermentation ends;
(4) by tunning and described urea, monoammonium phosphate, vitriolate of tartar, potassium primary phosphate, nanometer smectite clay, humic acids, BA, water, chitosan, borax, zinc chloride, Sodium orthomolybdate, manganous sulfate, Sodium dodecylbenzene sulfonate, ferrous sulfate, sal epsom, copper sulfate, reactor is put in the dimethyl sulfoxide (DMSO) mixing, uses water dissolution, is uniformly mixed reaction 2 hours under 100-120 ℃; After technique to be mixed completes, with 200 mesh sieve filtering solutions, remove residue,
(5) add by weight percentage described nanometer smectite clay in filtering solution, stir and obtain the finished product; Described nanometer smectite clay preparation method is: smectite clay mixing solutions, at 0 ℃ of lower stir-activating 3 h, is added to sodium lauryl sulphate, 4 * 10
4r/min high-shear 4h, reaction soln is cooled to decompress filter after room temperature, and gained is deposited under 105 ℃ and is dried to constant weight, obtains nanometer smectite clay.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210085812 CN102603408B (en) | 2012-03-28 | 2012-03-28 | Nanometer smectite clay organic compound fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201210085812 CN102603408B (en) | 2012-03-28 | 2012-03-28 | Nanometer smectite clay organic compound fertilizer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102603408A CN102603408A (en) | 2012-07-25 |
| CN102603408B true CN102603408B (en) | 2013-12-25 |
Family
ID=46521265
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201210085812 Expired - Fee Related CN102603408B (en) | 2012-03-28 | 2012-03-28 | Nanometer smectite clay organic compound fertilizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102603408B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102823355B (en) * | 2012-09-13 | 2015-04-15 | 新疆农业大学 | Soil improvement method |
| CN103772007B (en) * | 2013-12-26 | 2015-06-17 | 杨海涛 | Preparation method of nano cow dung fertilizer |
| CN104072245A (en) * | 2014-06-20 | 2014-10-01 | 裴秀琴 | Composite fertilizer |
| CN105110946A (en) * | 2015-08-31 | 2015-12-02 | 上海创博生态工程有限公司 | Organic fertilizer applicable to culturing of ginseng in farmlands and preparation method of organic fertilizer |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1171948C (en) * | 2002-08-09 | 2004-10-20 | 张夫道 | Production technology of nano-clay-polyester mixed polymer fertilizer coating cementing agent |
| CN1765849A (en) * | 2005-08-26 | 2006-05-03 | 四川大学 | Special-purpose foliage fertilizer for kiwi fruit |
| CN101391919B (en) * | 2008-11-07 | 2012-04-25 | 四川大学 | Foliage fertilizer special for kiwi berry with anti-cold effect |
| CN101774866B (en) * | 2010-02-09 | 2013-06-05 | 常州剑河新材料科技有限公司 | Biological slow-release compound fertilizer |
-
2012
- 2012-03-28 CN CN 201210085812 patent/CN102603408B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN102603408A (en) | 2012-07-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102617214B (en) | Preparation method for nano compound fertilizer | |
| CN102826922B (en) | Fertilizer special for spring corn base fertilizer | |
| CN103265370A (en) | Saline-alkali soil fertilizer | |
| CN102815997B (en) | Special fertilizer for early rice base fertilizer | |
| CN105248209A (en) | Pollution-free paddy rice planting method | |
| CN106673838A (en) | Pest-control organic-inorganic compound fertilizer for peach trees | |
| CN103274843B (en) | A kind of polynary microorganism special fertilizer preventing and treating bacterial soft rot of potato and preparation method thereof | |
| CN103288530B (en) | Pomegranate bark compound fertilizer specially used for peanuts | |
| CN105777233A (en) | Selenium-rich nutrient solution and preparation method thereof | |
| CN106342646A (en) | Grape planting method with soil fertility improving function | |
| CN103621279A (en) | Cucumber cultivation method | |
| CN103319250A (en) | Microbial fertilizer specially used for magnolia officinalis powdery mildew | |
| CN105085093A (en) | Inorganic-organic compound fertilizer dedicated for camellia oleifera and preparation method thereof | |
| CN105367283A (en) | Muskmelon high-yield greenhouse plantation method | |
| CN102559197B (en) | Saline-alkali soil modifying agent and preparation method thereof | |
| CN104355818A (en) | Tomato soilless culture medium | |
| CN109121952A (en) | The implantation methods of integrated control Citrus Huanglongbing pathogen | |
| CN102617232B (en) | Organic compound fertilizer for gynura divaricata | |
| CN102603408B (en) | Nanometer smectite clay organic compound fertilizer | |
| CN104447065A (en) | Environment-friendly chemical fertilizer | |
| CN102826924B (en) | Special base fertilizer for late rice | |
| CN102617234B (en) | Special nano compound fertilizer used for gynura divaricata and fertilizer application method | |
| CN106380313A (en) | Antibacterial and yield-increasing algae fertilizer and preparation method thereof | |
| CN102603390B (en) | Nanometer compound fertilizer | |
| CN106748498A (en) | A kind of fruit tree fertilizer with chicken manure and stalk as matrix and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: TAICANG LINJIANG FARM SPECIALIZED COOPERATIVES Free format text: FORMER OWNER: CHANGSHU NANYANG FERTILIZER CO., LTD. Effective date: 20131119 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 215500 SUZHOU, JIANGSU PROVINCE TO: 215400 SUZHOU, JIANGSU PROVINCE |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20131119 Address after: 215400 Jiangsu city of Suzhou province Taicang City, Huang Jing Zhen Qian Dang Cun Applicant after: Taicang Linjiang Farm Specialized Cooperatives Address before: 215500, Jiangsu, Suzhou province Changshou City Branch Town kiln village Applicant before: Changshu Nanyang Fertilizer Co., Ltd. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131225 Termination date: 20180328 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |