CN102596970B - 用于聚硅亚烷基硅氧烷的生产的方法 - Google Patents

用于聚硅亚烷基硅氧烷的生产的方法 Download PDF

Info

Publication number
CN102596970B
CN102596970B CN201080049875.0A CN201080049875A CN102596970B CN 102596970 B CN102596970 B CN 102596970B CN 201080049875 A CN201080049875 A CN 201080049875A CN 102596970 B CN102596970 B CN 102596970B
Authority
CN
China
Prior art keywords
ring
acid
opening polymerization
polymerization catalyst
monomer mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201080049875.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN102596970A (zh
Inventor
弗朗科斯·格纳奇奥德
F·古贝尔斯
S·罗布里
阿米迪·拉茨米赫蒂
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Publication of CN102596970A publication Critical patent/CN102596970A/zh
Application granted granted Critical
Publication of CN102596970B publication Critical patent/CN102596970B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04Polysiloxanes
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/0834Compounds having one or more O-Si linkage
    • C07F7/0838Compounds with one or more Si-O-Si sequences
    • C07F7/0872Preparation and treatment thereof
    • C07F7/0874Reactions involving a bond of the Si-O-Si linkage
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/20Polysiloxanes containing silicon bound to unsaturated aliphatic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/48Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
    • C08G77/485Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms containing less than 25 silicon atoms
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/48Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
    • C08G77/50Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms by carbon linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Silicon Polymers (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201080049875.0A 2009-11-03 2010-11-02 用于聚硅亚烷基硅氧烷的生产的方法 Expired - Fee Related CN102596970B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09306051 2009-11-03
EP09306051.5 2009-11-03
PCT/EP2010/066661 WO2011054830A1 (en) 2009-11-03 2010-11-02 A process for the production of polysilalkylenesiloxanes

Publications (2)

Publication Number Publication Date
CN102596970A CN102596970A (zh) 2012-07-18
CN102596970B true CN102596970B (zh) 2016-02-10

Family

ID=43499983

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080049875.0A Expired - Fee Related CN102596970B (zh) 2009-11-03 2010-11-02 用于聚硅亚烷基硅氧烷的生产的方法

Country Status (6)

Country Link
US (1) US8586690B2 (enExample)
EP (1) EP2496585A1 (enExample)
JP (1) JP2013510079A (enExample)
KR (1) KR20120080247A (enExample)
CN (1) CN102596970B (enExample)
WO (1) WO2011054830A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5533906B2 (ja) * 2011-02-28 2014-06-25 信越化学工業株式会社 付加反応硬化型オルガノポリシルメチレンシロキサンコポリマー組成物
JP5697160B2 (ja) * 2011-11-10 2015-04-08 信越化学工業株式会社 オルガノポリシロキサン組成物及びその硬化物
KR101939234B1 (ko) 2012-07-23 2019-01-16 삼성전자 주식회사 메모리 장치, 메모리 시스템 및 상기 메모리 장치의 독출 전압의 제어 방법
KR101598325B1 (ko) * 2013-01-09 2016-02-26 주식회사 다이셀 경화성 수지 조성물 및 그의 경화물
CN104817699A (zh) * 2015-04-24 2015-08-05 浙江润禾有机硅新材料有限公司 一种乙烯基硅油及其制备方法
CN104788679A (zh) * 2015-04-24 2015-07-22 浙江润禾有机硅新材料有限公司 含亚烷基结构的乙烯基硅油及其制备方法
EP3153540B8 (en) 2015-10-09 2018-07-25 Dow Silicones Corporation Process for preparing linear carbosiloxane polymers
TWI705598B (zh) * 2019-11-29 2020-09-21 輝能科技股份有限公司 電能供應系統與其封裝結構
CN114634525A (zh) * 2020-12-16 2022-06-17 江西贝特利新材料有限公司 一种四甲基环四硅氧烷的制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999067319A1 (en) * 1998-06-24 1999-12-29 Medtronic, Inc. Silalkylenesiloxane copolymer materials and methods for their preparation

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2229514C3 (de) 1972-06-16 1979-01-04 Wacker-Chemie Gmbh, 8000 Muenchen Verfahren zur Förderung von Kondensations- und/oder Äquilibrierungsreaktionen von Organosiliciumverbindungen
DE3428581A1 (de) 1984-08-02 1986-02-13 Wacker-Chemie GmbH, 8000 München Verfahren zum stabilisieren von organopolysiloxanen
DE3533028A1 (de) 1985-09-16 1987-03-19 Wacker Chemie Gmbh Verfahren zum stabilisieren von organopolysiloxanen
EP0465262B1 (en) * 1990-07-06 1996-06-05 Shin-Etsu Chemical Co., Ltd. Polysilethylenesiloxane
JPH0662773B2 (ja) * 1990-07-06 1994-08-17 信越化学工業株式会社 ポリシルエチレンシロキサン
EP0465263B1 (en) 1990-07-06 1996-10-09 Shin-Etsu Chemical Co., Ltd. Polysilethylenesiloxane
GB9103666D0 (en) 1991-02-21 1991-04-10 Dow Corning Sa Method of making organopolysiloxanes
JPH05222066A (ja) * 1992-02-17 1993-08-31 Shin Etsu Chem Co Ltd 新規有機ケイ素化合物
JP2627383B2 (ja) * 1992-04-01 1997-07-02 信越化学工業株式会社 5員環状シルエチレンシロキサンの製造方法
JPH0770324A (ja) 1993-09-03 1995-03-14 Toray Dow Corning Silicone Co Ltd 有機ケイ素重合体の製造方法
GB9703554D0 (en) 1997-02-20 1997-04-09 Dow Corning Polymerisation of cyclosiloxanes
GB9827069D0 (en) 1998-12-09 1999-02-03 Dow Corning Polymerisation catalyst
JP3793461B2 (ja) * 1999-10-28 2006-07-05 独立行政法人科学技術振興機構 シルアルキレンシロキサンの重合方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999067319A1 (en) * 1998-06-24 1999-12-29 Medtronic, Inc. Silalkylenesiloxane copolymer materials and methods for their preparation

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
Cleavage of cyclogarbosiloxanes in the presence of nucleophilic catalysts;Islamov et al.;<Bulletin the of the Academy of Sicences of the Ussr ,Division of chemical sciences》;19690930;第18卷(第12期);第2576页最后一段 *
Poly(dimethylsilylenemethylene-co-dimethylsiloxane): A Regularly Alternating Copolymer of Poly(dimethylsiloxane) and Poly(dimethylsilylenemethylene);Interrante et al.;《Macromolecules》;20010313;第34卷(第6期);第1545页左栏第3段,右栏第1段,第1546页Scheme1,右栏第2段 *

Also Published As

Publication number Publication date
WO2011054830A1 (en) 2011-05-12
US20120226010A1 (en) 2012-09-06
CN102596970A (zh) 2012-07-18
KR20120080247A (ko) 2012-07-16
US8586690B2 (en) 2013-11-19
JP2013510079A (ja) 2013-03-21
EP2496585A1 (en) 2012-09-12

Similar Documents

Publication Publication Date Title
CN102596970B (zh) 用于聚硅亚烷基硅氧烷的生产的方法
JP6250632B2 (ja) 制御された構造の官能性シロキサンを製造するためのプロセス
JP5196789B2 (ja) カルベンの存在下でのポリオルガノシロキサン(pos)の開環重合及び/又は再分配によるposの製造方法並びに該方法によって製造されたpos化合物
EP0465262B1 (en) Polysilethylenesiloxane
JPH0297529A (ja) パーフルオロアルキル基含有オルガノポリシロキサンの製造方法
JP5278242B2 (ja) 分子鎖両末端トリオルガノシロキシ基封鎖オルガノポリシロキサンの製造方法
JP4787393B2 (ja) シロキサン類の重合
JP2003517072A (ja) トリフル酸又はトリフル酸誘導体を主体とした触媒系で触媒された重合によるポリオルガノシロキサンを製造するための方法
JP3962898B2 (ja) 線状オルガノシロキサンポリマーの製造方法
KR20000057028A (ko) 카보실록산 덴드리머
JP4886772B2 (ja) ジオルガノポリシロキサンの製造方法
JPS6112931B2 (enExample)
US5969173A (en) Method of making dialkali metal silanolates and siloxanolates
Chojnowski et al. Synthesis of linear polysiloxanes with electron-donating organophosphorus pendant groups by kinetically controlled ring-opening polymerization
US10723845B2 (en) Process for preparing linear carbosiloxane polymers
Cao et al. Synthesis and characterization of ladder-like copolymethyl-epoxysilsesquioxane
EP1125939B1 (en) Process for reducing the amount of linear siloxane in a mixture of linear and cyclic siloxanes
JP5716533B2 (ja) 分子鎖両末端トリオルガノシロキシ基封鎖オルガノポリシロキサンの製造方法
CN113087907A (zh) 一种硅醇锂及其制备方法和应用
EP0693520B1 (en) Method for the preparation of organopolysiloxanes
KR20220123422A (ko) 액체 실리케이트 수지
JP6390473B2 (ja) 両末端変性されたシラシクロブタン開環重合物及びその製造方法
JP2018532018A (ja) オルガノポリシロキサンの調製方法
WO2024243126A1 (en) Polymerisation of siloxane polymers
JP3057139B2 (ja) 直鎖状ポリオルガノシロキサン及び製造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160210

Termination date: 20161102