CN102585630A - Water-based glass baking paint and preparation method thereof - Google Patents
Water-based glass baking paint and preparation method thereof Download PDFInfo
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- CN102585630A CN102585630A CN2011104256047A CN201110425604A CN102585630A CN 102585630 A CN102585630 A CN 102585630A CN 2011104256047 A CN2011104256047 A CN 2011104256047A CN 201110425604 A CN201110425604 A CN 201110425604A CN 102585630 A CN102585630 A CN 102585630A
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Abstract
The invention discloses a water-based glass baking paint for glass base materials and a preparation method thereof. The water-based glass baking paint contains the following contents by weight: 30-60 parts of water-soluble resin, 5-10 parts of 325 amino resin, 15-30 parts of pigment, 1-2 parts of adhesion promoters, 0.1-0.5 part of wetting agents, 0.5-1.5 parts of dispersing agents, 0.5-1.5 parts of antifoaming agents, 5-10 parts of propylene glycol and 30-50 parts of water. The preparation method of the water-based glass baking paint for glass base materials is simple in process, and the prepared water-based baking paint has good adhesive force and tinting strength on surfaces of glass products and has the characteristics of high temperature resistance and corrosion resistance.
Description
Technical field
The present invention relates to a kind of water-based stoving paint and preparation method thereof, a kind of specifically water-based stoving paint that is used for glass baseplate and preparation method thereof.
Background technology
Glass become people live in the middle of indispensable finishing material; The texture of glass itself is that other finishing material are irreplaceable; Glass paint lets glass that color has been arranged, and aesthetic feeling has been arranged, and coloured various inspiration produces; Glass is more special material, needs the glass lacquer will have very high performance requriements.The glass lacquer generally can be divided into self-drying type and baking vanish type two big classes, and wherein the performance of baking vanish type is better than self-drying type.The enhancing of Along with people's environmental consciousness, the aqueous glass baking vanish obtains increasing favor.It is painted that the aqueous glass baking vanish is primarily aimed at glasswork, is used to be coated on glass article surface to itself playing the effect that beautifies modification.Owing to be with water as solvent, VOC (organic volatile) belongs to the environment-friendly type coating product in the discharging of air in the prescription thereby reduced greatly.
Summary of the invention
To the deficiency that prior art exists, technical problem to be solved by this invention provides a kind of water-based stoving paint that is used for glass baseplate and preparation method thereof, and this method technology is simple, uses this baking vanish of preparing to possess good clinging power and tinting strength.
For solving the problems of the technologies described above, the technical scheme that the present invention taked is:
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 30-60 part water soluble resin; 5-10 part 325 aminoresin; 15-30 part pigment; 1-2 part adhesion promoter; 0.1-0.5 part wetting agent; 0.5-1.5 part dispersion agent; 0.5-1.5 part skimmer; 5-10 part Ucar 35; 30-50 part water.
Further, described water soluble resin is the water soluble acrylic resin.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
25-45 part water soluble resin, 0.2-0.5 part skimmer, 0.1-0.25 part wetting agent, 0.5-0.8 part dispersion agent, 15-30 part pigment and 15-20 part water are joined in the stirring tank successively, stir 3-5min in the 400-600r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
(1) water, the remainder water soluble resin with 15-20 weight joins in the paint mixing tank, adds the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, and under the 800-1000r/min speed conditions, high-speed stirring is disperseed 30-40min; Add the water of 5-10 part 325 aminoresin, 1-2 part adhesion promoter, 5-10 part Ucar 35 and residual content then, stir the preparation process that 10-15min can accomplish whole baking vanish.
The invention also discloses a kind of method of use that is used for the aqueous glass baking vanish of glass baseplate: may further comprise the steps: take by weighing an amount of water or the ethanolic soln of a certain amount of aqueous glass baking vanish adding and be diluted to working viscosity, coat on the glass baseplate; Dewater to surface drying at 50 ℃ of-60 ℃ of levellings baking 5-8min; Under 80 ℃ of-120 ℃ of conditions, toast 10-20min then, baking-curing gets aqueous glass baking vanish coating.
The disclosed water-based stoving paint preparation method technology that is used for glass baseplate is simple among the present invention, and the water-based stoving paint of preparing has good adherence power, tinting strength, surperficial special decorative effect, high temperature resistant, corrosion-resistant at glass article surface.When the baking vanish of preparing according to the method that the present invention announced is coated on the different glass base material, be easy to generate stronger sticking power, bright-coloured color and luster, favorable mechanical physicals, therefore can play effect such as protection decorations grade glasswork.In addition, above-mentioned aqueous glass baking vanish is in use, and is more or less freely to the allotment of pigment, therefore be easy to control color and with the variation of glossiness, and then satisfy the different appearance needs, promote decorate properties.
Embodiment
Embodiment 1
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 40 parts of water soluble acrylic resins (DT-116, Xi'an Great Sky Science & Technology Co., Ltd.); 7 part of 325 aminoresin (the special company of U.S.'s cyanogen); 30 parts of pigment Green 7s; 1 part of adhesion promoter (kh-470, Nanjing is latitude chemical industry ltd through the sky); 0.5 part wetting agent (OP-10, auxiliary reagent factory, Shanghai); 1.5 part dispersion agent (SN5040, the Ninghua worker of section (China) ltd); 0.5 part skimmer (BYK-051, German Bi Ke chemical company); 5 parts of Ucar 35; 35 parts of water.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
30 parts of water soluble acrylic resins, 0.25 part of skimmer, 0.3 part of wetting agent, 1.0 parts of dispersion agents, 30 parts of pigment Green 7s and 15 parts of water are joined in the stirring tank successively, stir 5min in the 400r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
The water of 15 parts of weight, remaining 10 parts of water soluble acrylic resins are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, under the 800r/min speed conditions, high-speed stirring is disperseed 35min; Add the water of 7 part of 325 aminoresin, 1.0 parts of adhesion promoters, 5 parts of Ucar 35 and residual content then, stir 10min and can accomplish.
Embodiment 2
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 60 parts of water soluble acrylic resins (LZ-7004, the blue bamboo chemical industry in Baoding ltd); 10 part of 325 aminoresin (the special company of U.S.'s cyanogen); 15 parts of pigment violet 1s 9; 1 part of adhesion promoter (DN-630, ltd is learned in Ninghua, road, Nanjing); 0.1 part wetting agent (PE-100, the Ninghua worker of section (China) ltd); 0.5 part dispersion agent (Disperbyk-160, German Bi Ke chemical company); 0.5 part skimmer (BYK-023, German Bi Ke chemical company); 10 parts of Ucar 35; 38 parts of water.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
30 parts of water soluble acrylic resins, 0.25 part of skimmer, 0.05 part of wetting agent, 0.3 part of dispersion agent, 15 parts of pigment violet 1s 9 and 20 parts of water are joined in the stirring tank successively, stir 4min in the 500r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
The water of 15 parts of weight, remaining 30 parts of water soluble acrylic resins are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, under the 800r/min speed conditions, high-speed stirring is disperseed 35min; Add the water of 10 part of 325 aminoresin, 1.0 parts of adhesion promoters, 10 parts of Ucar 35 and residual content then, stir 12min and can accomplish.
Embodiment 3
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 45 parts of water soluble acrylic resins (DT-116, Xi'an Great Sky Science & Technology Co., Ltd.); 5 part of 325 aminoresin (the special company of U.S.'s cyanogen); 20 parts of Pigment greens 17; 2 parts of adhesion promoters (DN-630, ltd is learned in Ninghua, road, Nanjing); 0.3 part wetting agent (OP-10, auxiliary reagent factory, Shanghai); 1.0 part dispersion agent (SN5040, the Ninghua worker of section (China) ltd); 0.8 part skimmer (BYK-051, German Bi Ke chemical company); 7 parts of Ucar 35; 40 parts of water.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
30 parts of water soluble acrylic resins, 0.25 part of skimmer, 0.1 part of wetting agent, 0.3 part of dispersion agent, 20 parts of Pigment greens 17 and 20 parts of water are joined in the stirring tank successively, stir 3min in the 600r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
The water of 15 parts of weight, remaining 15 parts of water soluble acrylic resins are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, under the 800r/min speed conditions, high-speed stirring is disperseed 35min; Add the water of 5 part of 325 aminoresin, 2.0 parts of adhesion promoters, 7 parts of Ucar 35 and residual content then, stir 10min and can accomplish.
Embodiment 4
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 55 parts of water soluble acrylic resins (DT-116, Xi'an Great Sky Science & Technology Co., Ltd.); 10 part of 325 aminoresin (the special company of U.S.'s cyanogen); 25 parts of Pigment blues 28; 2.0 part adhesion promoter (kh-470, Nanjing is latitude chemical industry ltd through the sky); 0.5 part wetting agent (OP-10, auxiliary reagent factory, Shanghai); 1.5 part dispersion agent (Disperbyk-171, German Bi Ke chemical company); 1.0 part skimmer (BYK-053, German Bi Ke chemical company); 10 parts of Ucar 35; 40 parts of water.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
30 parts of water soluble acrylic resins, 0.5 part of skimmer, 0.3 part of wetting agent, 0.8 part of dispersion agent, 25 parts of Pigment blues 28 and 20 parts of water are joined in the stirring tank successively, stir 5min in the 600r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
The water of 15 parts of weight, remaining 25 parts of water soluble acrylic resins are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, under the 800r/min speed conditions, high-speed stirring is disperseed 35min; Add the water of 10 part of 325 aminoresin, 2.0 parts of adhesion promoters, 10 parts of Ucar 35 and residual content then, stir 10min and can accomplish.
Embodiment 5
A kind of aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 40 parts of water soluble acrylic resins (LZ-7004, the blue bamboo chemical industry in Baoding ltd); 8 part of 325 aminoresin (the special company of U.S.'s cyanogen); 20 parts of pigment (Pigment Yellow 73 184); 1.5 part adhesion promoter (DN-630, ltd is learned in Ninghua, road, Nanjing); 0.2 part wetting agent (PE-100, the Ninghua worker of section (China) ltd); 0.6 part dispersion agent (SN5040, the Ninghua worker of section (China) ltd); 0.5 part skimmer (BYK-055, German Bi Ke chemical company); 8 parts of Ucar 35; 35 parts of water.
A kind of preparation method who is used for the aqueous glass baking vanish of glass baseplate is characterized in that, comprises the steps:
(1) preparation pigment slurry
20 parts of water soluble acrylic resins, 0.25 part of skimmer, 0.1 part of wetting agent, 0.3 part of dispersion agent, 20 parts of pigment and 20 parts of water are joined in the stirring tank successively, stir 5min in the 600r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
The water of 10 parts of weight, remaining 20 parts of water soluble acrylic resins are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step 1 prepare successively, under the 800r/min speed conditions, high-speed stirring is disperseed 35min; Add the water of 8 part of 325 aminoresin, 1.5 parts of adhesion promoters, 8 parts of Ucar 35 and residual content then, stir 12min and can accomplish.
After the prepared aqueous glass baking vanish of embodiment 1-5 used according to method of use provided by the invention, the performance index of the paint film that obtains were as shown in the table:
Claims (4)
1. aqueous glass baking vanish that is used for glass baseplate comprises the composition of following weight content: 30-60 part water soluble resin; 5-10 part 325 aminoresin; 15-30 part pigment; 1-2 part adhesion promoter; 0.1-0.5 part wetting agent; 0.5-1.5 part dispersion agent; 0.5-1.5 part skimmer; 5-10 part Ucar 35; 30-50 part water.
2. the aqueous glass baking vanish that is used for glass baseplate according to claim 1 is characterized in that: described water soluble resin is the water soluble acrylic resin.
3. be used for the preparation method of the aqueous glass baking vanish of glass baseplate in the claim 1, it is characterized in that, comprise the steps:
(1) preparation pigment slurry
25-45 part water soluble resin, 0.2-0.5 part skimmer, 0.1-0.25 part wetting agent, 0.5-0.8 part dispersion agent, 15-30 part pigment and 15-20 part water are joined in the stirring tank successively, stir 3-5min in the 400-600r/min speed conditions; After stirring, be ground to suitable fineness, obtain pigment slurry with sand mill.
(2) paint
Water, the remainder water soluble resin of 15-20 part are joined in the paint mixing tank, add the pigment slurry that remaining wetting agent, dispersion agent, skimmer, step (1) prepare successively, under the 800-1000r/min speed conditions, high-speed stirring is disperseed 30-40min; Add the water of 5-10 part 325 aminoresin, 1-2 part adhesion promoter, 5-10 part Ucar 35 and residual content then, stir the preparation process that 10-15min can accomplish whole baking vanish.
4. method of use that is used for the aqueous glass baking vanish of glass baseplate: may further comprise the steps: take by weighing a certain amount of aqueous glass baking vanish and add an amount of water or ethanolic soln and be diluted to working viscosity, coat on the glass baseplate; Dewater to surface drying at 50 ℃ of-60 ℃ of levellings baking 5-8min; Under 80 ℃ of-120 ℃ of conditions, toast 10-20min then, baking-curing gets aqueous glass baking vanish coating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104256047A CN102585630A (en) | 2011-12-19 | 2011-12-19 | Water-based glass baking paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011104256047A CN102585630A (en) | 2011-12-19 | 2011-12-19 | Water-based glass baking paint and preparation method thereof |
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| CN102585630A true CN102585630A (en) | 2012-07-18 |
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| CN2011104256047A Pending CN102585630A (en) | 2011-12-19 | 2011-12-19 | Water-based glass baking paint and preparation method thereof |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102977708A (en) * | 2012-11-16 | 2013-03-20 | 苏州嘉乐威企业发展有限公司 | Water-soluble stoving varnish suitable for craft glass products and preparation method thereof |
| CN103087634A (en) * | 2013-02-19 | 2013-05-08 | 成都市海鲨漆业有限责任公司 | Water-based vessel glaze and preparation method thereof |
| CN103483985A (en) * | 2013-09-18 | 2014-01-01 | 中山蓝海洋水性涂料有限公司 | High-gloss ethanol-tolerance water-based acrylic acid amino glass winebottle stoving varnish as well as preparation method and application thereof |
| CN104293027A (en) * | 2014-09-24 | 2015-01-21 | 晟通科技集团有限公司 | Emulsion-type glass paint |
| CN104312336A (en) * | 2014-11-05 | 2015-01-28 | 德阳森华涂料化工有限公司 | Water-based glass baking paint |
| CN104559557A (en) * | 2014-12-05 | 2015-04-29 | 东来涂料技术（上海）有限公司 | Water based paint with mirror surface effect and preparation method thereof |
| CN104927526A (en) * | 2015-07-08 | 2015-09-23 | 安庆联泰电子科技有限公司 | Water-borne acrylic amino baking varnish special for intelligent ashtray metal shell |
| CN104946049A (en) * | 2015-07-08 | 2015-09-30 | 安庆联泰电子科技有限公司 | Environment-friendly water-based glass baking lacquer |
| CN105693104A (en) * | 2015-09-06 | 2016-06-22 | 广州叶子环保科技有限公司 | Use methods of nano titanium dioxide in ceramics, glass and furniture |
| CN105949914A (en) * | 2016-06-16 | 2016-09-21 | 中山市汉艺涂料有限公司 | Waterborne glass baking paint and preparation method thereof |
| CN106609080A (en) * | 2015-10-26 | 2017-05-03 | 天津市新丽华色材有限责任公司 | Waterborne glass stoving varnish |
| CN106634228A (en) * | 2016-12-18 | 2017-05-10 | 钦州市科学技术开发中心 | Preparation process of anti-cracking paint |
| CN106675271A (en) * | 2017-01-16 | 2017-05-17 | 广东四方威凯新材料有限公司 | Bake type single-layer waterborne flashing paint for aluminum alloy hub and preparation method of waterborne flashing paint |
| CN106675141A (en) * | 2016-12-18 | 2017-05-17 | 钦州市科学技术开发中心 | Novel nickel powder-carbon black conductive paint and preparation method thereof |
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| CN1432612A (en) * | 2003-02-27 | 2003-07-30 | 涿州赛迪化学有限公司 | Aqueous paint |
| CN101928491A (en) * | 2009-11-27 | 2010-12-29 | 广州擎天实业有限公司 | Water-based decorative paint for metal material and preparation method thereof |
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Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102977708B (en) * | 2012-11-16 | 2015-04-01 | 苏州嘉乐威企业发展有限公司 | Water-soluble stoving varnish suitable for craft glass products and preparation method thereof |
| CN102977708A (en) * | 2012-11-16 | 2013-03-20 | 苏州嘉乐威企业发展有限公司 | Water-soluble stoving varnish suitable for craft glass products and preparation method thereof |
| CN103087634B (en) * | 2013-02-19 | 2015-10-28 | 成都市海鲨漆业有限责任公司 | A kind of water-based vessel glaze and preparation method thereof |
| CN103087634A (en) * | 2013-02-19 | 2013-05-08 | 成都市海鲨漆业有限责任公司 | Water-based vessel glaze and preparation method thereof |
| CN103483985A (en) * | 2013-09-18 | 2014-01-01 | 中山蓝海洋水性涂料有限公司 | High-gloss ethanol-tolerance water-based acrylic acid amino glass winebottle stoving varnish as well as preparation method and application thereof |
| CN103483985B (en) * | 2013-09-18 | 2016-03-02 | 中山蓝海洋水性涂料有限公司 | A kind of high gloss acrylic-amino of resistance to ethanol aqueous glass wine bottle baking vanish and its preparation method and application |
| CN104293027A (en) * | 2014-09-24 | 2015-01-21 | 晟通科技集团有限公司 | Emulsion-type glass paint |
| CN104312336A (en) * | 2014-11-05 | 2015-01-28 | 德阳森华涂料化工有限公司 | Water-based glass baking paint |
| CN104559557A (en) * | 2014-12-05 | 2015-04-29 | 东来涂料技术（上海）有限公司 | Water based paint with mirror surface effect and preparation method thereof |
| CN104946049A (en) * | 2015-07-08 | 2015-09-30 | 安庆联泰电子科技有限公司 | Environment-friendly water-based glass baking lacquer |
| CN104927526A (en) * | 2015-07-08 | 2015-09-23 | 安庆联泰电子科技有限公司 | Water-borne acrylic amino baking varnish special for intelligent ashtray metal shell |
| CN105693104A (en) * | 2015-09-06 | 2016-06-22 | 广州叶子环保科技有限公司 | Use methods of nano titanium dioxide in ceramics, glass and furniture |
| CN106609080A (en) * | 2015-10-26 | 2017-05-03 | 天津市新丽华色材有限责任公司 | Waterborne glass stoving varnish |
| CN105949914A (en) * | 2016-06-16 | 2016-09-21 | 中山市汉艺涂料有限公司 | Waterborne glass baking paint and preparation method thereof |
| CN106634228A (en) * | 2016-12-18 | 2017-05-10 | 钦州市科学技术开发中心 | Preparation process of anti-cracking paint |
| CN106675141A (en) * | 2016-12-18 | 2017-05-17 | 钦州市科学技术开发中心 | Novel nickel powder-carbon black conductive paint and preparation method thereof |
| CN106675271A (en) * | 2017-01-16 | 2017-05-17 | 广东四方威凯新材料有限公司 | Bake type single-layer waterborne flashing paint for aluminum alloy hub and preparation method of waterborne flashing paint |
| CN106675271B (en) * | 2017-01-16 | 2019-06-07 | 广东四方威凯新材料有限公司 | A kind of aluminium alloy wheel hub aqueous metallic finishe of baking-type single layer and preparation method thereof |
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Application publication date: 20120718 |