CN104559557A - Water based paint with mirror surface effect and preparation method thereof - Google Patents
Water based paint with mirror surface effect and preparation method thereof Download PDFInfo
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- CN104559557A CN104559557A CN201410742239.6A CN201410742239A CN104559557A CN 104559557 A CN104559557 A CN 104559557A CN 201410742239 A CN201410742239 A CN 201410742239A CN 104559557 A CN104559557 A CN 104559557A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/47—Levelling agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
Abstract
The invention relates to water based paint with a mirror surface effect and a preparation method thereof. The water based paint is composed of the following components in parts by weight: 50-70 parts of water-based acrylic resin A, 10-20 parts of water-based amino resin B, 5-10 parts of cosolvent, 0.1-0.5 part of defoaming agent, 0.5-1 part of leveling agent, 5-10 parts of effect pigment, 0.05-0.1 part of amine neutralizer and 10-20 parts of deionized water. The preparation method comprises the following steps: sequentially adding the water-based acrylic resin A, the water-based amino resin B, 50% of deionized water, the defoaming agent and the cosolvent into a container, and stirring uniformly to obtain a mixture A; uniformly mixing and stirring the residual deionized water, the leveling agent and the effect pigment to obtain a component B; adding the component B into the component A while stirring, uniformly stirring and finally regulating the pH to 7.0-7.5 by use of the amine neutralizer. Compared with the prior art, the water based paint provided by the invention has the advantages of low VOC emission, environmental friendliness, excellent adhesive force, high hardness and scratch resistance, and the like.
Description
Technical field
The present invention relates to a kind of paint and preparation method thereof, especially relate to a kind of water-miscible paint with mirror effect and preparation method thereof.
Background technology
Use field at industrial paint, mainly solvent based coating is adopted for the coating with mirror effect, and outward appearance unfairness, require high to painting environments, yield is low.Along with deepening continuously of countries in the world environmental consciousness, more and more pay close attention to the pollution of organic solvent during painting dressing automobiles, various countries have formulated the VOC of corresponding regulation to car paint one after another and have controlled.Concerning coating industry, Water-borne modification is Main way.
Chinese patent CN103923511A provides a kind of waterborne metallic paint, comprises first component and component B; Described first component comprises: 3 ~ 50g/L metal-salt, 5 ~ 60g/L complexing agent, 0.1 ~ 5g/L stablizer and water; Described component B comprises: 5 ~ 50g/L reductive agent and water.This patent adopts water-borne coatings, and VOC free discharges, more environmental protection; Meanwhile, utilize redox reaction, use metal-salt is raw material, simplifies production technique, and makes the obtained waterborne metallic paint quality guaranteed period longer, providing covalent linkage and ionic linkage, making water-borne coatings make metallic mirror surface effect by adding complexing agent.
The waterborne metallic paint of above-mentioned patent is that a kind of electroplating technology prepares, it is a kind of electrochemical reaction, main by the metal ion in first component, with the reductive agent in component B, under electric current, pass through redox reaction, metal ion is cemented out, is deposited on substrate surface, thus have stronger metal sense, at metal, the substrate surfaces such as plastics carry out the coated of a kind of metal effect.As zinc-plated, copper facing, nickel plating etc.But this electrochemical processing mode is more complicated, needs chemical immersion trough, stable electric current etc., most importantly can produce the waste water containing heavy metal, just current environmental requirement, the waste water of process containing heavy metal needs sizable cost.
Summary of the invention
Object of the present invention be exactly in order to overcome above-mentioned prior art exist defect and a kind of low VOC discharge, environmental protection, the water-miscible paint with mirror effect with sticking power excellence, high rigidity and resistance to marring and preparation method thereof are provided.
Object of the present invention can be achieved through the following technical solutions:
Have a water-miscible paint for mirror effect, by weight, this paint is made up of following component:
Described water-borne acrylic resin A is selected from aqueous acrylic emulsion Bayhydrol 2470 or RCS1554;
Described water-compatible amino resin B is selected from the high imino-resin of CYMEL 385;
Described solubility promoter is selected from tripropylene glycol butyl ether, propylene glycol phenylate, butyl or butyl glycol ether.
Described defoamer is selected from commercially available BYK-182;
Described flow agent is selected from commercially available BYK-333;
Described effect pigment is selected from Shu Lunke Aquamet HR-BG/7800, this effect pigment is that water-based imitates electrosilvering, there is very high mirror effect, because the sheet structure of aluminium paste is for this reason thinner, and edge is mellow and full, silver dollar type, coated by silicon-dioxide capsule again, therefore there is good water-based stability and higher mirror effect;
Described amine neutralizing agent is selected from the modest chemical industry DMAE of moral.
The method comprises the following steps:
(1) water-borne acrylic resin A, water-compatible amino resin B and solubility promoter are mixed, stir 20min with 300r/min, obtain mixture;
(2) under whipped state, defoamer is slowly added step (1) gained mixture, and continue with 500r/min rotating speed, dispersion 20min, is prepared into component A;
(3) portions of de-ionized water, effect pigment and flow agent are mixed, with 300r/min, stir 10min, be prepared into B component;
(4) with under 500r/min rotating speed, component B is slowly added in component A, and with amine neutralizing agent, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) will remain deionized water as thinner, the mixture that dissolving step (4) obtains, and utilize aerial spraying, the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
Residue deionized water described in step (5) is 30 ~ 40% of deionized water gross weight.
Compared with prior art, the present invention is by the water-borne acrylic resin A containing long chain polymer, mix with special effect pigments, emulsion being blown with the form of droplet by air pressure is attached on base material, in substrate surface seasoning film forming, and only can produce water in drying process, thus evaporate in air, can not environment be affected.Metal effect of the present invention is the effect brought by effect pigment itself.The present invention by special resin collocation and auxiliary agent, effect pigment is special chooses, have the following advantages:
(1) water-borne acrylic resin A of the present invention has higher high reactivity, therefore has good levelling property, fullness ratio, high bake is carried out with water-compatible amino resin B, amino is crosslinked with hydroxyl, can form fine and close high-molecular weight compounds, have higher hardness and resistance to marring.
And effect pigment is water-based imitates electrosilvering (2), have very high mirror effect, because the sheet structure of aluminium paste is for this reason thinner, and edge is mellow and full, is silver dollar type, coated by silicon-dioxide capsule again, therefore has good water-based stability and higher mirror effect.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail.
Embodiment 1
Have a water-miscible paint for mirror effect, by weight, this paint is made up of following component:
The above-mentioned preparation method with the water-miscible paint of mirror effect, comprises the following steps:
(1) Bayhydrol 2470, CYMEL 385 and solubility promoter are mixed, stir 20min with 300r/min, obtain mixture;
(2) under whipped state, BYK-182 is slowly added step (1) gained mixture, and continue with 500r/min rotating speed, dispersion 20min, is prepared into component A;
(3) by the deionized water of 10 weight parts, HR-BG/7800 and BYK-333 mixing, with 300r/min, stir 10min, be prepared into B component;
(4) with under 500r/min rotating speed, component B is slowly added in component A, and with DMAE, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) will remain deionized water as thinner, the mixture that dissolving step (4) obtains, and utilize aerial spraying, the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
Embodiment 2
Have a water-miscible paint for mirror effect, by weight, this paint is made up of following component:
The above-mentioned preparation method with the water-miscible paint of mirror effect, comprises the following steps:
(1) Bayhydrol RCS 1554, CYMEL 385 and solubility promoter are mixed, stir 20min with 300r/min, obtain mixture;
(2) under whipped state, BYK-182 is slowly added step (1) gained mixture, and continue with 500r/min rotating speed, dispersion 20min, is prepared into component A;
(3) by 3 parts by weight of deionized water, HR-BG/7800 and BYK-333 mixing, with 300r/min, stir 10min, be prepared into B component;
(4) with under 500r/min rotating speed, component B is slowly added in component A, and with DMAE, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) using remaining deionized water as thinner, the mixture that dissolving step (4) obtains, utilizes aerial spraying, and the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
Above two examples, because used resin types is different with weight part, but all have the features such as sticking power excellence, high rigidity and resistance to marring, but also have difference a little,
The performance of the water-miscible paint that embodiment 1 ~ embodiment 2 obtains
Embodiment 3
Have a water-miscible paint for mirror effect, by weight, this paint is made up of following component:
Water-borne acrylic resin A (Bayer chemical industry Bayhydrol 2470) 50, water-compatible amino resin B (the high imino-resin of cyanogen specialization work CYMEL 385) 10, solubility promoter (butyl) 5, defoamer (Bi Ke chemical industry BYK-182) 0.1, flow agent (Bi Ke chemical industry BYK-333) 0.5, effect pigment (Shu Lunke Aquamet HR-BG/7800) 5, amine neutralizing agent (the modest chemical industry DMAE of moral) 0.05, deionized water 10.
The above-mentioned water-miscible paint preparation method with mirror effect comprises the following steps:
(1) water-borne acrylic resin A, water-compatible amino resin B and solubility promoter are mixed, stir 20min with 300r/min, obtain mixture;
(2) under whipped state, defoamer is slowly added step (1) gained mixture, and continue with 500r/min rotating speed, dispersion 20min, is prepared into component A;
(3) 60-70% deionized water, effect pigment and flow agent are mixed, with 300r/min, stir 10min, be prepared into B component;
(4) with under 500r/min rotating speed, component B is slowly added in component A, and with amine neutralizing agent, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) will remain deionized water as thinner, the mixture that dissolving step (4) obtains, and utilize aerial spraying, the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
Embodiment 4
Have a water-miscible paint for mirror effect, by weight, this paint is made up of following component:
Water-borne acrylic resin A (Bayer chemical industry RCS 1554) 70, water-compatible amino resin B (the high imino-resin of cyanogen specialization work CYMEL 385) 20, solubility promoter (butyl or butyl glycol ether) 10, defoamer (Bi Ke chemical industry BYK-182) 0.5, flow agent (Bi Ke chemical industry BYK-333) 1, effect pigment (Shu Lunke Aquamet HR-BG/7800) 10, amine neutralizing agent (the modest chemical industry DMAE of moral) 0.1, deionized water 20.
The above-mentioned water-miscible paint preparation method with mirror effect comprises the following steps:
(1) water-borne acrylic resin A, water-compatible amino resin B and solubility promoter are mixed, stir 20min with 300r/min, obtain mixture;
(2) under whipped state, defoamer is slowly added step (1) gained mixture, and continue with 500r/min rotating speed, dispersion 20min, is prepared into component A;
(3) 70% deionized water, effect pigment and flow agent are mixed, with 300r/min, stir 10min, be prepared into B component;
(4) with under 500r/min rotating speed, component B is slowly added in component A, and with amine neutralizing agent, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) will remain deionized water as thinner, the mixture that dissolving step (4) obtains, and utilize aerial spraying, the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
Above-mentioned is can understand and use invention for ease of those skilled in the art to the description of embodiment.Person skilled in the art obviously easily can make various amendment to these embodiments, and General Principle described herein is applied in other embodiments and need not through performing creative labour.Therefore, the invention is not restricted to above-described embodiment, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (10)
1. have a water-miscible paint for mirror effect, it is characterized in that, by weight, this paint is made up of following component:
2. a kind of water-miscible paint with mirror effect according to claim 1, is characterized in that, described water-borne acrylic resin A is selected from Bayer water-base resin Bayhydrol 2470 or RCS 1554.
3. a kind of water-miscible paint with mirror effect according to claim 1, is characterized in that, described water-compatible amino resin B is selected from the high imino-resin of cyanogen specialization work CYMEL 385.
4. a kind of water-miscible paint with mirror effect according to claim 1, is characterized in that, described solubility promoter is commercially available tripropylene glycol butyl ether, propylene glycol phenylate, butyl or butyl glycol ether.
5. a kind of water-miscible paint with mirror effect according to claim 1, it is characterized in that, described defoamer is selected from commercially available BYK-182.
6. a kind of water-miscible paint with mirror effect according to claim 1, it is characterized in that, described flow agent is selected from commercially available BYK-333.
7. a kind of water-miscible paint with mirror effect according to claim 1, is characterized in that, described effect pigment is selected from Shu Lunke Aquamet HR-BG/7800.
8. a kind of water-miscible paint with mirror effect according to claim 1, is characterized in that, described amine neutralizing agent is selected from commercially available DMAE.
9. have a preparation method for the water-miscible paint of mirror effect as claimed in claim 1, it is characterized in that, the method comprises the following steps:
(1) water-borne acrylic resin A, water-compatible amino resin B and solubility promoter are mixed, stir and obtain mixture;
(2) under whipped state, defoamer is added step (1) gained mixture, and continue to stir, be prepared into component A;
(3) portions of de-ionized water, effect pigment and flow agent are mixed, stir, be prepared into B component;
(4) under high-speed stirring, component B is slowly added in component A, and with amine neutralizing agent, mixture is adjusted to pH value 7.0 ~ 7.5;
(5) will remain deionized water as thinner, the mixture that dissolving step (4) obtains, and utilize aerial spraying, obtain wet film, the wet film obtained toasts after 1 hour at 140 DEG C, namely obtains the water-miscible paint with mirror effect.
10. a kind of preparation method with the water-miscible paint of mirror effect according to claim 9, is characterized in that, the residue deionized water described in step (5) is 30 ~ 40% of deionized water gross weight.
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| CN201410742239.6A CN104559557B (en) | 2014-12-05 | 2014-12-05 | A kind of water paint with mirror effect and preparation method thereof |
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| CN201410742239.6A CN104559557B (en) | 2014-12-05 | 2014-12-05 | A kind of water paint with mirror effect and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106967322A (en) * | 2017-05-18 | 2017-07-21 | 聂超 | A kind of nanometer water powder environment-friendly materials and preparation method thereof |
| CN107083131A (en) * | 2017-05-25 | 2017-08-22 | 重庆汉宝水性漆有限公司 | Engine fire resistant water-based paint and preparation method thereof |
| CN107151503A (en) * | 2017-05-24 | 2017-09-12 | 贝内克-长顺汽车内饰材料（张家港）有限公司 | It is a kind of for hot water resistance paint of PVC interior decoration leathers and preparation method thereof |
| CN107216748A (en) * | 2017-08-04 | 2017-09-29 | 浙江喜泽荣制漆有限公司 | A kind of aqueous emulation copper coating and preparation method thereof |
| CN110157271A (en) * | 2019-06-05 | 2019-08-23 | 立邦涂料（中国）有限公司 | A kind of aqueous polymeric coating composition of automobile |
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| CN102618133A (en) * | 2012-03-31 | 2012-08-01 | 广州集泰化工有限公司 | High-temperature resistant and strong corrosive resistant water-based baking varnish for metal and preparation method for baking varnish |
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| CN101698771A (en) * | 2009-09-24 | 2010-04-28 | 中国海洋石油总公司 | Water-based primer-topcoat braking paint and preparation method thereof |
| CN102585630A (en) * | 2011-12-19 | 2012-07-18 | 青岛爱尔家佳新材料有限公司 | Water-based glass baking paint and preparation method thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106967322A (en) * | 2017-05-18 | 2017-07-21 | 聂超 | A kind of nanometer water powder environment-friendly materials and preparation method thereof |
| CN107151503A (en) * | 2017-05-24 | 2017-09-12 | 贝内克-长顺汽车内饰材料（张家港）有限公司 | It is a kind of for hot water resistance paint of PVC interior decoration leathers and preparation method thereof |
| CN107083131A (en) * | 2017-05-25 | 2017-08-22 | 重庆汉宝水性漆有限公司 | Engine fire resistant water-based paint and preparation method thereof |
| CN107216748A (en) * | 2017-08-04 | 2017-09-29 | 浙江喜泽荣制漆有限公司 | A kind of aqueous emulation copper coating and preparation method thereof |
| CN107216748B (en) * | 2017-08-04 | 2019-03-29 | 浙江喜泽荣制漆有限公司 | Aqueous emulation copper coating of one kind and preparation method thereof |
| CN110157271A (en) * | 2019-06-05 | 2019-08-23 | 立邦涂料（中国）有限公司 | A kind of aqueous polymeric coating composition of automobile |
| CN110157271B (en) * | 2019-06-05 | 2021-04-13 | 立邦涂料（中国）有限公司 | Water-based polymer coating composition for automobile |
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| CN104559557B (en) | 2017-08-01 |
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Address after: 201807 No. 1221 Xin He Lu, Jiading Industrial Zone, Jiading District, Shanghai. Patentee after: Dong Lai coating technology (Shanghai) Limited by Share Ltd Address before: 201807 No. 1221 Xinhe Road, North District, Jiading District, Shanghai Patentee before: Eastern paint technology (Shanghai) Co., Ltd. |
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