CN102574083B - 制备包含一种或多种络合剂盐的粉末的方法 - Google Patents

制备包含一种或多种络合剂盐的粉末的方法 Download PDF

Info

Publication number
CN102574083B
CN102574083B CN201080045832.5A CN201080045832A CN102574083B CN 102574083 B CN102574083 B CN 102574083B CN 201080045832 A CN201080045832 A CN 201080045832A CN 102574083 B CN102574083 B CN 102574083B
Authority
CN
China
Prior art keywords
complexing agent
spray
powder
aqueous solution
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201080045832.5A
Other languages
English (en)
Chinese (zh)
Other versions
CN102574083A (zh
Inventor
F·姆尔泽纳
U·蒙戈
M·舍恩赫尔
T·赫丹弗德
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43499971&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN102574083(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Publication of CN102574083A publication Critical patent/CN102574083A/zh
Application granted granted Critical
Publication of CN102574083B publication Critical patent/CN102574083B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
CN201080045832.5A 2009-10-12 2010-10-11 制备包含一种或多种络合剂盐的粉末的方法 Active CN102574083B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09172810.5 2009-10-12
EP09172810 2009-10-12
PCT/EP2010/065184 WO2011045266A1 (de) 2009-10-12 2010-10-11 Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze

Publications (2)

Publication Number Publication Date
CN102574083A CN102574083A (zh) 2012-07-11
CN102574083B true CN102574083B (zh) 2015-01-28

Family

ID=43499971

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080045832.5A Active CN102574083B (zh) 2009-10-12 2010-10-11 制备包含一种或多种络合剂盐的粉末的方法

Country Status (15)

Country Link
US (1) US9540597B2 (enExample)
EP (1) EP2488291B1 (enExample)
JP (1) JP6243120B2 (enExample)
KR (1) KR20120095390A (enExample)
CN (1) CN102574083B (enExample)
AU (1) AU2010305833A1 (enExample)
BR (1) BR112012008666B1 (enExample)
CA (1) CA2776570A1 (enExample)
ES (1) ES2531306T3 (enExample)
MX (1) MX2012004170A (enExample)
MY (1) MY156376A (enExample)
PL (1) PL2488291T3 (enExample)
RU (1) RU2554932C2 (enExample)
WO (1) WO2011045266A1 (enExample)
ZA (1) ZA201203359B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
US8754026B2 (en) 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB201214558D0 (en) * 2012-08-15 2012-09-26 Reckitt Benckiser Nv Detergent granule
BR112018011578A2 (pt) * 2015-12-11 2018-11-27 Basf Se processo para fabricação de grânulos
BR112018075476B1 (pt) * 2016-06-20 2022-10-04 Basf Se Processo para produção de um pó ou grânulo, pó ou grânulo, e, uso de grânulos e de pós
EP3746535A1 (en) * 2018-01-30 2020-12-09 Eastman Chemical Company Compositions comprising aminocarboxylate chelating agents
WO2019175169A1 (en) * 2018-03-13 2019-09-19 Taminco Bvba Process for drying n,n-dimethyl glycinate salt
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2970057A (en) * 1956-07-06 1961-01-31 Dairy Foods Inc Process for producing crystalline spray dried material
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
WO2009103822A1 (en) * 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid
CN101528907A (zh) * 2006-08-10 2009-09-09 巴斯夫欧洲公司 用于洗碗机的清洁配制物

Family Cites Families (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2728678A (en) 1946-09-19 1955-12-27 Foremost Dairies Inc Process for drying solutions containing crystallizable material, and product produced thereby
DE1261619B (de) * 1962-07-12 1968-02-22 Budenheim Rud A Oetker Chemie Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel
US3615723A (en) * 1970-04-15 1971-10-26 Pillsbury Co Spray-drying apparatus
JPS4924943B1 (enExample) * 1970-06-01 1974-06-26
US3629955A (en) * 1970-07-31 1971-12-28 Procter & Gamble Multilevel spray-drying apparatus
US3717589A (en) * 1970-09-17 1973-02-20 Monsanto Co Sodium nitrilotriacetate and processes for producing same
US3956379A (en) * 1970-10-23 1976-05-11 Ethyl Corporation Process for recovering NTA
JPS5229761B2 (enExample) * 1972-08-17 1977-08-04
JPS52136112A (en) * 1976-05-12 1977-11-14 Nippon Shiryo Kogyo Kk Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose
DE3504896A1 (de) * 1985-02-13 1986-08-14 Basf Ag, 6700 Ludwigshafen Zusaetze fuer wasch- und reinigungsmittel
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DK160809C (da) 1989-01-09 1995-10-02 Niro Holding As Fremgangsmåde og forstøvningstørringsapparat til fremstilling af stabile partikelagglomerater
DE4319935A1 (de) 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
DE19518986A1 (de) 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
JP4711471B2 (ja) * 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19640365A1 (de) * 1996-09-30 1998-04-02 Basf Ag Polymer-Wasserstoffperoxid-Komplexe
DE19649681A1 (de) 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
US5968884A (en) 1997-04-07 1999-10-19 Basf Corporation Concentrated built liquid detergents containing a biodegradable chelant
WO1999061407A1 (en) * 1998-05-27 1999-12-02 Showa Denko K.K. Processes for producing amino acid having secondary or tertiary amino group and three or more carboxyl groups and its salt
US6906215B1 (en) * 1999-04-30 2005-06-14 Mitsubishi Rayon Co., Ltd. Powdery s,s-ethylenediamine-n,n′-disuccinic acid iron complex and process for producing the same
DE19927537A1 (de) * 1999-06-16 2000-12-21 Merck Patent Gmbh Sprühtrocknungsanlage und Verfahren zu ihrer Verwendung
US6451224B1 (en) * 1999-07-21 2002-09-17 The Dow Chemical Company Stable free-flowing solid chelants
DE10161402A1 (de) 2001-12-13 2003-06-18 Merck Patent Gmbh Verfahren zur Herstellung von direkt tablettierbarem beta-Mannit
EP1354939A1 (en) * 2002-04-19 2003-10-22 The Procter & Gamble Company Pouched cleaning compositions
JP4189208B2 (ja) * 2002-11-27 2008-12-03 花王株式会社 界面活性剤担持用粒子群
US7442679B2 (en) * 2004-04-15 2008-10-28 Ecolab Inc. Binding agent for solidification matrix comprising MGDA
DE102005021055A1 (de) 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
EA201001199A1 (ru) * 2008-01-24 2011-02-28 Юнилевер Н.В. Композиции детергентов для посудомоечных машин
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
AU2010251173A1 (en) * 2009-05-20 2012-01-19 Basf Se Method for producing a spray powder containing one or more glycine-N,N-diacetic acid derivatives and use of the spray powder to produce compression agglomerates
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
DE102009060814A1 (de) * 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
US8754026B2 (en) * 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2970057A (en) * 1956-07-06 1961-01-31 Dairy Foods Inc Process for producing crystalline spray dried material
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
CN101528907A (zh) * 2006-08-10 2009-09-09 巴斯夫欧洲公司 用于洗碗机的清洁配制物
WO2009103822A1 (en) * 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid

Also Published As

Publication number Publication date
ZA201203359B (en) 2013-07-31
RU2554932C2 (ru) 2015-07-10
ES2531306T3 (es) 2015-03-12
RU2012119166A (ru) 2013-11-20
US20120202731A1 (en) 2012-08-09
BR112012008666B1 (pt) 2018-09-18
EP2488291B1 (de) 2014-12-10
PL2488291T3 (pl) 2015-05-29
EP2488291A1 (de) 2012-08-22
WO2011045266A1 (de) 2011-04-21
CN102574083A (zh) 2012-07-11
MX2012004170A (es) 2012-05-08
JP6243120B2 (ja) 2017-12-06
CA2776570A1 (en) 2011-04-21
JP2013507499A (ja) 2013-03-04
AU2010305833A1 (en) 2012-04-19
US9540597B2 (en) 2017-01-10
BR112012008666A2 (pt) 2016-04-19
KR20120095390A (ko) 2012-08-28
MY156376A (en) 2016-02-15

Similar Documents

Publication Publication Date Title
CN102574083B (zh) 制备包含一种或多种络合剂盐的粉末的方法
CA2719754C (en) Preparation of free flowing granules of methylglycine diacetic acid
EP2718412B1 (en) Builder granules and process for their preparation
US20030114717A1 (en) Process for the preparation of ss-mannitol for direct compression
JP6827990B2 (ja) ジペプチド含有造粒物の製造方法
CN1365252A (zh) 制备草甘膦铵盐粉末的方法
CN103124720B (zh) 生产包含一种或多种络合剂盐的粒料的方法
CN108368459A (zh) 制造颗粒的方法
US12258541B2 (en) Crumbly phase composition of methylglycine N,N diacetic acid
JP6720356B2 (ja) ジペプチド含有造粒物
CN115916742B (zh) 使用甲基甘氨酸n,n二乙酸盐的易碎相组合物制备甲基甘氨酸n,n二乙酸盐共生颗粒的方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant