CN102574083B - 制备包含一种或多种络合剂盐的粉末的方法 - Google Patents

制备包含一种或多种络合剂盐的粉末的方法 Download PDF

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Publication number
CN102574083B
CN102574083B CN201080045832.5A CN201080045832A CN102574083B CN 102574083 B CN102574083 B CN 102574083B CN 201080045832 A CN201080045832 A CN 201080045832A CN 102574083 B CN102574083 B CN 102574083B
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China
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complexing agent
spray
powder
aqueous solution
weight
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CN201080045832.5A
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English (en)
Chinese (zh)
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CN102574083A (zh
Inventor
F·姆尔泽纳
U·蒙戈
M·舍恩赫尔
T·赫丹弗德
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
CN201080045832.5A 2009-10-12 2010-10-11 制备包含一种或多种络合剂盐的粉末的方法 Active CN102574083B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09172810 2009-10-12
EP09172810.5 2009-10-12
PCT/EP2010/065184 WO2011045266A1 (de) 2009-10-12 2010-10-11 Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze

Publications (2)

Publication Number Publication Date
CN102574083A CN102574083A (zh) 2012-07-11
CN102574083B true CN102574083B (zh) 2015-01-28

Family

ID=43499971

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201080045832.5A Active CN102574083B (zh) 2009-10-12 2010-10-11 制备包含一种或多种络合剂盐的粉末的方法

Country Status (15)

Country Link
US (1) US9540597B2 (enExample)
EP (1) EP2488291B1 (enExample)
JP (1) JP6243120B2 (enExample)
KR (1) KR20120095390A (enExample)
CN (1) CN102574083B (enExample)
AU (1) AU2010305833A1 (enExample)
BR (1) BR112012008666B1 (enExample)
CA (1) CA2776570A1 (enExample)
ES (1) ES2531306T3 (enExample)
MX (1) MX2012004170A (enExample)
MY (1) MY156376A (enExample)
PL (1) PL2488291T3 (enExample)
RU (1) RU2554932C2 (enExample)
WO (1) WO2011045266A1 (enExample)
ZA (1) ZA201203359B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
JP6243120B2 (ja) 2009-10-12 2017-12-06 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ １種以上の錯化剤の塩を含む粉末の製造方法
US8754026B2 (en) 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB201214558D0 (en) * 2012-08-15 2012-09-26 Reckitt Benckiser Nv Detergent granule
US10975334B2 (en) * 2015-12-11 2021-04-13 Basf Se Process for manufacturing granules
CN109415662A (zh) * 2016-06-20 2019-03-01 巴斯夫欧洲公司 粉末和颗粒以及制备该粉末和颗粒的方法
EP3746535A1 (en) 2018-01-30 2020-12-09 Eastman Chemical Company Compositions comprising aminocarboxylate chelating agents
US11524931B2 (en) * 2018-03-13 2022-12-13 Taminco Bv Process for drying N,N-dimethyl glycinate salte
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物

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US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
WO2009103822A1 (en) * 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid
CN101528907A (zh) * 2006-08-10 2009-09-09 巴斯夫欧洲公司 用于洗碗机的清洁配制物

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DE1261619B (de) * 1962-07-12 1968-02-22 Budenheim Rud A Oetker Chemie Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel
US3615723A (en) * 1970-04-15 1971-10-26 Pillsbury Co Spray-drying apparatus
JPS4924943B1 (enExample) * 1970-06-01 1974-06-26
US3629955A (en) * 1970-07-31 1971-12-28 Procter & Gamble Multilevel spray-drying apparatus
US3717589A (en) * 1970-09-17 1973-02-20 Monsanto Co Sodium nitrilotriacetate and processes for producing same
US3956379A (en) * 1970-10-23 1976-05-11 Ethyl Corporation Process for recovering NTA
JPS5229761B2 (enExample) * 1972-08-17 1977-08-04
JPS52136112A (en) * 1976-05-12 1977-11-14 Nippon Shiryo Kogyo Kk Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose
DE3504896A1 (de) * 1985-02-13 1986-08-14 Basf Ag, 6700 Ludwigshafen Zusaetze fuer wasch- und reinigungsmittel
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DK160809C (da) 1989-01-09 1995-10-02 Niro Holding As Fremgangsmåde og forstøvningstørringsapparat til fremstilling af stabile partikelagglomerater
DE4319935A1 (de) * 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
DE19518986A1 (de) 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
JP4711471B2 (ja) * 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
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EP1176137B1 (en) * 1999-04-30 2004-06-30 Mitsubishi Rayon Co., Ltd. Powdery s,s-ethylenediamine-n,n'-disuccinic acid iron complex and process for producing the same
DE19927537A1 (de) * 1999-06-16 2000-12-21 Merck Patent Gmbh Sprühtrocknungsanlage und Verfahren zu ihrer Verwendung
US6451224B1 (en) * 1999-07-21 2002-09-17 The Dow Chemical Company Stable free-flowing solid chelants
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EP1354939A1 (en) * 2002-04-19 2003-10-22 The Procter & Gamble Company Pouched cleaning compositions
JP4189208B2 (ja) 2002-11-27 2008-12-03 花王株式会社 界面活性剤担持用粒子群
US7442679B2 (en) * 2004-04-15 2008-10-28 Ecolab Inc. Binding agent for solidification matrix comprising MGDA
DE102005021055A1 (de) 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
WO2009092699A1 (en) 2008-01-24 2009-07-30 Unilever Nv Machine dishwash detergent compositions
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
WO2010133617A1 (de) * 2009-05-20 2010-11-25 Basf Se Verfahren zur herstellung eines sprühpulvers enthaltend ein oder mehrere glycin-n,n-diessigsäure-derivate und verwendung des sprühpulvers zur herstellung von pressagglomeraten
DE102009038951A1 (de) 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
JP6243120B2 (ja) 2009-10-12 2017-12-06 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ １種以上の錯化剤の塩を含む粉末の製造方法
DE102009060814A1 (de) * 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
US8754026B2 (en) * 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2970057A (en) * 1956-07-06 1961-01-31 Dairy Foods Inc Process for producing crystalline spray dried material
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
CN101528907A (zh) * 2006-08-10 2009-09-09 巴斯夫欧洲公司 用于洗碗机的清洁配制物
WO2009103822A1 (en) * 2008-04-01 2009-08-27 Unilever Nv Preparation of free flowing granules of methyglycine diacetic acid

Also Published As

Publication number Publication date
EP2488291A1 (de) 2012-08-22
CA2776570A1 (en) 2011-04-21
ES2531306T3 (es) 2015-03-12
AU2010305833A1 (en) 2012-04-19
PL2488291T3 (pl) 2015-05-29
BR112012008666A2 (pt) 2016-04-19
KR20120095390A (ko) 2012-08-28
RU2012119166A (ru) 2013-11-20
JP6243120B2 (ja) 2017-12-06
MX2012004170A (es) 2012-05-08
US9540597B2 (en) 2017-01-10
MY156376A (en) 2016-02-15
US20120202731A1 (en) 2012-08-09
JP2013507499A (ja) 2013-03-04
CN102574083A (zh) 2012-07-11
ZA201203359B (en) 2013-07-31
WO2011045266A1 (de) 2011-04-21
EP2488291B1 (de) 2014-12-10
BR112012008666B1 (pt) 2018-09-18
RU2554932C2 (ru) 2015-07-10

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