BR112012008666B1 - processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo - Google Patents

processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo Download PDF

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Publication number
BR112012008666B1
BR112012008666B1 BR112012008666-9A BR112012008666A BR112012008666B1 BR 112012008666 B1 BR112012008666 B1 BR 112012008666B1 BR 112012008666 A BR112012008666 A BR 112012008666A BR 112012008666 B1 BR112012008666 B1 BR 112012008666B1
Authority
BR
Brazil
Prior art keywords
powder
complexing agent
salts
spray
weight
Prior art date
Application number
BR112012008666-9A
Other languages
English (en)
Portuguese (pt)
Other versions
BR112012008666A2 (pt
Inventor
Frank Mrzena
Ulrich Menge
Michael Schönherr
Thomas Heidenfelder
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43499971&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BR112012008666(B1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Se filed Critical Basf Se
Publication of BR112012008666A2 publication Critical patent/BR112012008666A2/pt
Publication of BR112012008666B1 publication Critical patent/BR112012008666B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
BR112012008666-9A 2009-10-12 2010-10-11 processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo BR112012008666B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09172810.5 2009-10-12
EP09172810 2009-10-12
PCT/EP2010/065184 WO2011045266A1 (de) 2009-10-12 2010-10-11 Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze

Publications (2)

Publication Number Publication Date
BR112012008666A2 BR112012008666A2 (pt) 2016-04-19
BR112012008666B1 true BR112012008666B1 (pt) 2018-09-18

Family

ID=43499971

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012008666-9A BR112012008666B1 (pt) 2009-10-12 2010-10-11 processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo

Country Status (15)

Country Link
US (1) US9540597B2 (enExample)
EP (1) EP2488291B1 (enExample)
JP (1) JP6243120B2 (enExample)
KR (1) KR20120095390A (enExample)
CN (1) CN102574083B (enExample)
AU (1) AU2010305833A1 (enExample)
BR (1) BR112012008666B1 (enExample)
CA (1) CA2776570A1 (enExample)
ES (1) ES2531306T3 (enExample)
MX (1) MX2012004170A (enExample)
MY (1) MY156376A (enExample)
PL (1) PL2488291T3 (enExample)
RU (1) RU2554932C2 (enExample)
WO (1) WO2011045266A1 (enExample)
ZA (1) ZA201203359B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
US8754026B2 (en) 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB201214558D0 (en) * 2012-08-15 2012-09-26 Reckitt Benckiser Nv Detergent granule
BR112018011578A2 (pt) * 2015-12-11 2018-11-27 Basf Se processo para fabricação de grânulos
BR112018075476B1 (pt) * 2016-06-20 2022-10-04 Basf Se Processo para produção de um pó ou grânulo, pó ou grânulo, e, uso de grânulos e de pós
EP3746535A1 (en) * 2018-01-30 2020-12-09 Eastman Chemical Company Compositions comprising aminocarboxylate chelating agents
WO2019175169A1 (en) * 2018-03-13 2019-09-19 Taminco Bvba Process for drying n,n-dimethyl glycinate salt
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2728678A (en) 1946-09-19 1955-12-27 Foremost Dairies Inc Process for drying solutions containing crystallizable material, and product produced thereby
BE572854A (enExample) * 1956-07-06
DE1261619B (de) * 1962-07-12 1968-02-22 Budenheim Rud A Oetker Chemie Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel
US3615723A (en) * 1970-04-15 1971-10-26 Pillsbury Co Spray-drying apparatus
JPS4924943B1 (enExample) * 1970-06-01 1974-06-26
US3629955A (en) * 1970-07-31 1971-12-28 Procter & Gamble Multilevel spray-drying apparatus
US3717589A (en) * 1970-09-17 1973-02-20 Monsanto Co Sodium nitrilotriacetate and processes for producing same
US3956379A (en) * 1970-10-23 1976-05-11 Ethyl Corporation Process for recovering NTA
JPS5229761B2 (enExample) * 1972-08-17 1977-08-04
JPS52136112A (en) * 1976-05-12 1977-11-14 Nippon Shiryo Kogyo Kk Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
DE3504896A1 (de) * 1985-02-13 1986-08-14 Basf Ag, 6700 Ludwigshafen Zusaetze fuer wasch- und reinigungsmittel
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DK160809C (da) 1989-01-09 1995-10-02 Niro Holding As Fremgangsmåde og forstøvningstørringsapparat til fremstilling af stabile partikelagglomerater
DE4319935A1 (de) 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
DE19518986A1 (de) 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
JP4711471B2 (ja) * 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19640365A1 (de) * 1996-09-30 1998-04-02 Basf Ag Polymer-Wasserstoffperoxid-Komplexe
DE19649681A1 (de) 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
US5968884A (en) 1997-04-07 1999-10-19 Basf Corporation Concentrated built liquid detergents containing a biodegradable chelant
WO1999061407A1 (en) * 1998-05-27 1999-12-02 Showa Denko K.K. Processes for producing amino acid having secondary or tertiary amino group and three or more carboxyl groups and its salt
US6906215B1 (en) * 1999-04-30 2005-06-14 Mitsubishi Rayon Co., Ltd. Powdery s,s-ethylenediamine-n,n′-disuccinic acid iron complex and process for producing the same
DE19927537A1 (de) * 1999-06-16 2000-12-21 Merck Patent Gmbh Sprühtrocknungsanlage und Verfahren zu ihrer Verwendung
US6451224B1 (en) * 1999-07-21 2002-09-17 The Dow Chemical Company Stable free-flowing solid chelants
DE10161402A1 (de) 2001-12-13 2003-06-18 Merck Patent Gmbh Verfahren zur Herstellung von direkt tablettierbarem beta-Mannit
EP1354939A1 (en) * 2002-04-19 2003-10-22 The Procter & Gamble Company Pouched cleaning compositions
JP4189208B2 (ja) * 2002-11-27 2008-12-03 花王株式会社 界面活性剤担持用粒子群
US7442679B2 (en) * 2004-04-15 2008-10-28 Ecolab Inc. Binding agent for solidification matrix comprising MGDA
DE102005021055A1 (de) 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
CA2660193A1 (en) * 2006-08-10 2008-02-14 Basf Se Detergent formulation for machine dishwashers
EA201001199A1 (ru) * 2008-01-24 2011-02-28 Юнилевер Н.В. Композиции детергентов для посудомоечных машин
US8183410B2 (en) 2008-04-01 2012-05-22 Conopco, Inc. Preparation of free flowing granules of methylglycine diacetic acid
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
AU2010251173A1 (en) * 2009-05-20 2012-01-19 Basf Se Method for producing a spray powder containing one or more glycine-N,N-diacetic acid derivatives and use of the spray powder to produce compression agglomerates
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
DE102009060814A1 (de) * 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
US8754026B2 (en) * 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts

Also Published As

Publication number Publication date
ZA201203359B (en) 2013-07-31
RU2554932C2 (ru) 2015-07-10
ES2531306T3 (es) 2015-03-12
RU2012119166A (ru) 2013-11-20
US20120202731A1 (en) 2012-08-09
EP2488291B1 (de) 2014-12-10
PL2488291T3 (pl) 2015-05-29
EP2488291A1 (de) 2012-08-22
WO2011045266A1 (de) 2011-04-21
CN102574083A (zh) 2012-07-11
MX2012004170A (es) 2012-05-08
JP6243120B2 (ja) 2017-12-06
CA2776570A1 (en) 2011-04-21
JP2013507499A (ja) 2013-03-04
AU2010305833A1 (en) 2012-04-19
US9540597B2 (en) 2017-01-10
BR112012008666A2 (pt) 2016-04-19
CN102574083B (zh) 2015-01-28
KR20120095390A (ko) 2012-08-28
MY156376A (en) 2016-02-15

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 11/10/2010, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 15A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2849 DE 12-08-2025 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.