BR112012008666A2 - processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo - Google Patents

processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo

Info

Publication number
BR112012008666A2
BR112012008666A2 BR112012008666A BR112012008666A BR112012008666A2 BR 112012008666 A2 BR112012008666 A2 BR 112012008666A2 BR 112012008666 A BR112012008666 A BR 112012008666A BR 112012008666 A BR112012008666 A BR 112012008666A BR 112012008666 A2 BR112012008666 A2 BR 112012008666A2
Authority
BR
Brazil
Prior art keywords
powder
weight
aqueous solution
complexing agent
salts
Prior art date
Application number
BR112012008666A
Other languages
English (en)
Other versions
BR112012008666B1 (pt
Inventor
Frank Mrzena
Michael Schönherr
Thomas Heidenfelder
Ulrich Menge
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43499971&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BR112012008666(A2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Se filed Critical Basf Se
Publication of BR112012008666A2 publication Critical patent/BR112012008666A2/pt
Publication of BR112012008666B1 publication Critical patent/BR112012008666B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Medicinal Preparation (AREA)
  • Detergent Compositions (AREA)
  • Glanulating (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo. a invenção se refere a um processo para a produção de um pó que contém um ou mais sais de agente complexante de fórmula geral (i), partindo de uma solução aquosa, que contém um ou mais sais de agente complexante a uma concentração de 10 a 80% em peso, em relação ao peso total da solução aquosa, em um processo de secagem por pulverização, que compreende uma etapa de atomização e uma etapa de secagem, caracterizado pelo fato de que a etapa de atomização é realizada por adição de pó cristalino fino do mesmo sal ou sais de agente complexante que são encontrados na solução aquosa ou de um ou mais sais de agentes de formação de complexos diferentes dos mesmos, que possuem um limite superior para o diâmetro médio da partícula pó crsitalino fino que é menor do que o limite inferior para o diâmetro médio da partícula do pó obtido de acordo com o processo pelo menos por um fator de 2, a uma proporção de 0,1 a 20% em peso, em relação ao peso do pó obtido de acordo com o processo.
BR112012008666A 2009-10-12 2010-10-11 processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo BR112012008666B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP09172810 2009-10-12
PCT/EP2010/065184 WO2011045266A1 (de) 2009-10-12 2010-10-11 Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze

Publications (2)

Publication Number Publication Date
BR112012008666A2 true BR112012008666A2 (pt) 2016-04-19
BR112012008666B1 BR112012008666B1 (pt) 2018-09-18

Family

ID=43499971

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112012008666A BR112012008666B1 (pt) 2009-10-12 2010-10-11 processo para a preparação de um pó, formulação, e, uso do pó preparado por um processo

Country Status (15)

Country Link
US (1) US9540597B2 (pt)
EP (1) EP2488291B1 (pt)
JP (1) JP6243120B2 (pt)
KR (1) KR20120095390A (pt)
CN (1) CN102574083B (pt)
AU (1) AU2010305833A1 (pt)
BR (1) BR112012008666B1 (pt)
CA (1) CA2776570A1 (pt)
ES (1) ES2531306T3 (pt)
MX (1) MX2012004170A (pt)
MY (1) MY156376A (pt)
PL (1) PL2488291T3 (pt)
RU (1) RU2554932C2 (pt)
WO (1) WO2011045266A1 (pt)
ZA (1) ZA201203359B (pt)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PL2488291T3 (pl) 2009-10-12 2015-05-29 Basf Se Sposób wytwarzania proszku zawierającego jeden lub większą liczbę soli będących czynnikami kompleksującymi
US8754026B2 (en) 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB201214558D0 (en) * 2012-08-15 2012-09-26 Reckitt Benckiser Nv Detergent granule
BR112018011578A2 (pt) * 2015-12-11 2018-11-27 Basf Se processo para fabricação de grânulos
WO2017220308A1 (en) * 2016-06-20 2017-12-28 Basf Se Powders and granules and process for making such powders and granules
WO2019152208A1 (en) * 2018-01-30 2019-08-08 Eastman Chemical Company Compositions comprising aminocarboxylate chelating agents
US11524931B2 (en) * 2018-03-13 2022-12-13 Taminco Bv Process for drying N,N-dimethyl glycinate salte
CN113382980A (zh) 2018-12-21 2021-09-10 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物

Family Cites Families (38)

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BE572854A (pt) * 1956-07-06
DE1261619B (de) * 1962-07-12 1968-02-22 Budenheim Rud A Oetker Chemie Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel
US3615723A (en) * 1970-04-15 1971-10-26 Pillsbury Co Spray-drying apparatus
JPS4924943B1 (pt) * 1970-06-01 1974-06-26
US3629955A (en) * 1970-07-31 1971-12-28 Procter & Gamble Multilevel spray-drying apparatus
US3717589A (en) * 1970-09-17 1973-02-20 Monsanto Co Sodium nitrilotriacetate and processes for producing same
US3956379A (en) * 1970-10-23 1976-05-11 Ethyl Corporation Process for recovering NTA
JPS5229761B2 (pt) * 1972-08-17 1977-08-04
JPS52136112A (en) * 1976-05-12 1977-11-14 Nippon Shiryo Kogyo Kk Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
DE3504896A1 (de) * 1985-02-13 1986-08-14 Basf Ag, 6700 Ludwigshafen Zusaetze fuer wasch- und reinigungsmittel
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
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DE19518986A1 (de) 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
JP4711471B2 (ja) * 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
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RU2533974C2 (ru) 2009-05-20 2014-11-27 Басф Се Способ получения сыпучего порошка, содержащего одно или несколько производных глицин-n,n-диуксусной кислоты, и применение сыпучего порошка для получения прессованных агломератов
DE102009038951A1 (de) 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PL2488291T3 (pl) 2009-10-12 2015-05-29 Basf Se Sposób wytwarzania proszku zawierającego jeden lub większą liczbę soli będących czynnikami kompleksującymi
DE102009060814A1 (de) * 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
US8754026B2 (en) * 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts

Also Published As

Publication number Publication date
CN102574083B (zh) 2015-01-28
BR112012008666B1 (pt) 2018-09-18
WO2011045266A1 (de) 2011-04-21
US9540597B2 (en) 2017-01-10
EP2488291A1 (de) 2012-08-22
AU2010305833A1 (en) 2012-04-19
ZA201203359B (en) 2013-07-31
CA2776570A1 (en) 2011-04-21
EP2488291B1 (de) 2014-12-10
JP2013507499A (ja) 2013-03-04
JP6243120B2 (ja) 2017-12-06
MX2012004170A (es) 2012-05-08
KR20120095390A (ko) 2012-08-28
RU2012119166A (ru) 2013-11-20
CN102574083A (zh) 2012-07-11
ES2531306T3 (es) 2015-03-12
PL2488291T3 (pl) 2015-05-29
RU2554932C2 (ru) 2015-07-10
US20120202731A1 (en) 2012-08-09
MY156376A (en) 2016-02-15

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Legal Events

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B06A Notification to applicant to reply to the report for non-patentability or inadequacy of the application according art. 36 industrial patent law
B09A Decision: intention to grant
B16A Patent or certificate of addition of invention granted

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 11/10/2010, OBSERVADAS AS CONDICOES LEGAIS.