MX2012004170A - Metodo para producir un polvo que contiene una o mas sales de agente de complejacion. - Google Patents
Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.Info
- Publication number
- MX2012004170A MX2012004170A MX2012004170A MX2012004170A MX2012004170A MX 2012004170 A MX2012004170 A MX 2012004170A MX 2012004170 A MX2012004170 A MX 2012004170A MX 2012004170 A MX2012004170 A MX 2012004170A MX 2012004170 A MX2012004170 A MX 2012004170A
- Authority
- MX
- Mexico
- Prior art keywords
- complexing agent
- salts
- weight
- aqueous solution
- producing
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C11D11/0088—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
Abstract
La invención se refiere a un método para producir un polvo que contiene una o más sales de agente de complejación de la fórmula general (I), a partir de una solución acuosa, que contiene la una o más sales de agnete de complejación a una concentración de 10 a 80% en peso, en relación al peso total de la solución acuosa, en un proceso de secado por aspersión, que comprende un paso de atomización y un paso de secado, caracterizado además porque el paso de atomización se realiza agregando polvo cristalino fino de la misma sal o sales de agente de complejación que se encuentran en la solución acuosa, o una o más sales de agente de complejación que difieren de ahí, teniendo un límite superior para el diámetro de partícula promedio del polvo cristalino fino que es menos del límite menor del diámetro de partícula promedio del polvo obtenido de conformidad con el método por al menos un factor de 2, a una proporción de 0.1 a 20% en peso, en relación al peso del polvo obtenido de conformidad con el método.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09172810 | 2009-10-12 | ||
PCT/EP2010/065184 WO2011045266A1 (de) | 2009-10-12 | 2010-10-11 | Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere komplexbildnersalze |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2012004170A true MX2012004170A (es) | 2012-05-08 |
Family
ID=43499971
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2012004170A MX2012004170A (es) | 2009-10-12 | 2010-10-11 | Metodo para producir un polvo que contiene una o mas sales de agente de complejacion. |
Country Status (15)
Country | Link |
---|---|
US (1) | US9540597B2 (es) |
EP (1) | EP2488291B1 (es) |
JP (1) | JP6243120B2 (es) |
KR (1) | KR20120095390A (es) |
CN (1) | CN102574083B (es) |
AU (1) | AU2010305833A1 (es) |
BR (1) | BR112012008666B1 (es) |
CA (1) | CA2776570A1 (es) |
ES (1) | ES2531306T3 (es) |
MX (1) | MX2012004170A (es) |
MY (1) | MY156376A (es) |
PL (1) | PL2488291T3 (es) |
RU (1) | RU2554932C2 (es) |
WO (1) | WO2011045266A1 (es) |
ZA (1) | ZA201203359B (es) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
MX2012004170A (es) | 2009-10-12 | 2012-05-08 | Basf Se | Metodo para producir un polvo que contiene una o mas sales de agente de complejacion. |
US8754026B2 (en) | 2010-09-27 | 2014-06-17 | Basf Se | Process for producing granules comprising one or more complexing agent salts |
US8785685B2 (en) | 2011-04-12 | 2014-07-22 | Basf Se | Process for preparing aminopolycarboxylates proceeding from amino acids |
GB201214558D0 (en) * | 2012-08-15 | 2012-09-26 | Reckitt Benckiser Nv | Detergent granule |
WO2017097657A1 (en) * | 2015-12-11 | 2017-06-15 | Basf Se | Process for manufacturing granules |
EP3472294B1 (en) * | 2016-06-20 | 2020-07-22 | Basf Se | Powders and granules and process for making such powders and granules |
EP3746535A1 (en) | 2018-01-30 | 2020-12-09 | Eastman Chemical Company | Compositions comprising aminocarboxylate chelating agents |
EP3765438A1 (en) * | 2018-03-13 | 2021-01-20 | Taminco Bvba | Process for drying n,n-dimethyl glycinate salt |
WO2020127349A1 (en) | 2018-12-21 | 2020-06-25 | Nouryon Chemicals International B.V. | Crumbly phase composition of methylglycine n,n diacetic acid |
Family Cites Families (38)
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US2728678A (en) | 1946-09-19 | 1955-12-27 | Foremost Dairies Inc | Process for drying solutions containing crystallizable material, and product produced thereby |
BE572854A (es) | 1956-07-06 | |||
DE1261619B (de) | 1962-07-12 | 1968-02-22 | Budenheim Rud A Oetker Chemie | Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel |
US3615723A (en) | 1970-04-15 | 1971-10-26 | Pillsbury Co | Spray-drying apparatus |
JPS4924943B1 (es) | 1970-06-01 | 1974-06-26 | ||
US3629955A (en) * | 1970-07-31 | 1971-12-28 | Procter & Gamble | Multilevel spray-drying apparatus |
US3717589A (en) * | 1970-09-17 | 1973-02-20 | Monsanto Co | Sodium nitrilotriacetate and processes for producing same |
US3956379A (en) * | 1970-10-23 | 1976-05-11 | Ethyl Corporation | Process for recovering NTA |
JPS5229761B2 (es) * | 1972-08-17 | 1977-08-04 | ||
JPS52136112A (en) * | 1976-05-12 | 1977-11-14 | Nippon Shiryo Kogyo Kk | Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose |
US4070766A (en) | 1976-09-09 | 1978-01-31 | Stork Friesland B.V. | Method and apparatus for preparing a so-called non-caking powder |
DE3504896A1 (de) * | 1985-02-13 | 1986-08-14 | Basf Ag, 6700 Ludwigshafen | Zusaetze fuer wasch- und reinigungsmittel |
JPH0678225B2 (ja) * | 1985-11-27 | 1994-10-05 | 株式会社林原生物化学研究所 | 脱水医薬品とその製造方法 |
DK160809C (da) | 1989-01-09 | 1995-10-02 | Niro Holding As | Fremgangsmåde og forstøvningstørringsapparat til fremstilling af stabile partikelagglomerater |
DE4319935A1 (de) | 1993-06-16 | 1994-12-22 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen |
DE19518986A1 (de) | 1995-05-29 | 1996-12-05 | Basf Ag | Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium |
JP4711471B2 (ja) * | 1996-07-05 | 2011-06-29 | 三菱商事フードテック株式会社 | 結晶マルチトール及びそれを含有する含蜜結晶の製造方法 |
DE19640365A1 (de) * | 1996-09-30 | 1998-04-02 | Basf Ag | Polymer-Wasserstoffperoxid-Komplexe |
DE19649681A1 (de) | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
US5968884A (en) * | 1997-04-07 | 1999-10-19 | Basf Corporation | Concentrated built liquid detergents containing a biodegradable chelant |
AU3955499A (en) | 1998-05-27 | 1999-12-13 | Chelest Corporation | Processes for producing amino acid having secondary or tertiary amino group and three or more carboxyl groups and its salt |
WO2000066540A1 (fr) * | 1999-04-30 | 2000-11-09 | Mitsubishi Rayon Co., Ltd. | Complexe de fer poudreux de s,s-ethylenediamine-n,n'-acide disuccinique et son procede de production |
DE19927537A1 (de) | 1999-06-16 | 2000-12-21 | Merck Patent Gmbh | Sprühtrocknungsanlage und Verfahren zu ihrer Verwendung |
US6451224B1 (en) * | 1999-07-21 | 2002-09-17 | The Dow Chemical Company | Stable free-flowing solid chelants |
DE10161402A1 (de) | 2001-12-13 | 2003-06-18 | Merck Patent Gmbh | Verfahren zur Herstellung von direkt tablettierbarem beta-Mannit |
EP1354939A1 (en) * | 2002-04-19 | 2003-10-22 | The Procter & Gamble Company | Pouched cleaning compositions |
JP4189208B2 (ja) | 2002-11-27 | 2008-12-03 | 花王株式会社 | 界面活性剤担持用粒子群 |
US7442679B2 (en) * | 2004-04-15 | 2008-10-28 | Ecolab Inc. | Binding agent for solidification matrix comprising MGDA |
DE102005021055A1 (de) | 2005-05-06 | 2006-11-09 | Basf Ag | Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen |
EP2052066A1 (de) * | 2006-08-10 | 2009-04-29 | Basf Se | Reinigungsformulierung für geschirrspülmaschinen |
EP2245129B1 (en) * | 2008-01-24 | 2012-05-09 | Unilever N.V. | Machine dishwash detergent compositions |
EP2257522B1 (en) * | 2008-04-01 | 2016-03-23 | Unilever N.V. | Preparation of free flowing granules of methyglycine diacetic acid |
FR2935383B1 (fr) * | 2008-08-26 | 2010-10-01 | Pancosma Sa Pour L Ind Des Pro | Procede et dispositif pour la fabrication de complexes organometalliques en poudre. |
SG178076A1 (en) * | 2009-05-20 | 2012-03-29 | Basf Se | Process for the preparation of a spray powder comprising one or more glycine-n,n-diacetic acid derivatives and use of the spray powder for producing compression agglomerates |
DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
MX2012004170A (es) | 2009-10-12 | 2012-05-08 | Basf Se | Metodo para producir un polvo que contiene una o mas sales de agente de complejacion. |
DE102009060814A1 (de) * | 2009-12-30 | 2011-07-07 | inprotec AG, 79423 | Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält |
US8754026B2 (en) * | 2010-09-27 | 2014-06-17 | Basf Se | Process for producing granules comprising one or more complexing agent salts |
-
2010
- 2010-10-11 MX MX2012004170A patent/MX2012004170A/es active IP Right Grant
- 2010-10-11 CN CN201080045832.5A patent/CN102574083B/zh active Active
- 2010-10-11 KR KR1020127012330A patent/KR20120095390A/ko not_active Application Discontinuation
- 2010-10-11 ES ES10768453T patent/ES2531306T3/es active Active
- 2010-10-11 EP EP10768453.2A patent/EP2488291B1/de active Active
- 2010-10-11 JP JP2012533597A patent/JP6243120B2/ja active Active
- 2010-10-11 AU AU2010305833A patent/AU2010305833A1/en not_active Abandoned
- 2010-10-11 CA CA2776570A patent/CA2776570A1/en not_active Abandoned
- 2010-10-11 WO PCT/EP2010/065184 patent/WO2011045266A1/de active Application Filing
- 2010-10-11 MY MYPI2012001543A patent/MY156376A/en unknown
- 2010-10-11 PL PL10768453T patent/PL2488291T3/pl unknown
- 2010-10-11 BR BR112012008666A patent/BR112012008666B1/pt active IP Right Grant
- 2010-10-11 RU RU2012119166/04A patent/RU2554932C2/ru active
- 2010-10-11 US US13/501,390 patent/US9540597B2/en active Active
-
2012
- 2012-05-09 ZA ZA2012/03359A patent/ZA201203359B/en unknown
Also Published As
Publication number | Publication date |
---|---|
RU2554932C2 (ru) | 2015-07-10 |
ES2531306T3 (es) | 2015-03-12 |
CA2776570A1 (en) | 2011-04-21 |
KR20120095390A (ko) | 2012-08-28 |
JP2013507499A (ja) | 2013-03-04 |
AU2010305833A1 (en) | 2012-04-19 |
BR112012008666B1 (pt) | 2018-09-18 |
MY156376A (en) | 2016-02-15 |
RU2012119166A (ru) | 2013-11-20 |
BR112012008666A2 (pt) | 2016-04-19 |
CN102574083A (zh) | 2012-07-11 |
WO2011045266A1 (de) | 2011-04-21 |
CN102574083B (zh) | 2015-01-28 |
PL2488291T3 (pl) | 2015-05-29 |
EP2488291B1 (de) | 2014-12-10 |
US9540597B2 (en) | 2017-01-10 |
US20120202731A1 (en) | 2012-08-09 |
JP6243120B2 (ja) | 2017-12-06 |
EP2488291A1 (de) | 2012-08-22 |
ZA201203359B (en) | 2013-07-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |