KR20120095390A - 하나 이상의 착화제 염을 포함하는 분말의 제조 방법 - Google Patents

하나 이상의 착화제 염을 포함하는 분말의 제조 방법 Download PDF

Info

Publication number
KR20120095390A
KR20120095390A KR1020127012330A KR20127012330A KR20120095390A KR 20120095390 A KR20120095390 A KR 20120095390A KR 1020127012330 A KR1020127012330 A KR 1020127012330A KR 20127012330 A KR20127012330 A KR 20127012330A KR 20120095390 A KR20120095390 A KR 20120095390A
Authority
KR
South Korea
Prior art keywords
spray
complexing agent
powder
aqueous solution
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
KR1020127012330A
Other languages
English (en)
Korean (ko)
Inventor
프랑크 음르제나
울리히 멘게
미첼 쇠른헤르
토마스 하이덴펠더
Original Assignee
바스프 에스이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43499971&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=KR20120095390(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 바스프 에스이 filed Critical 바스프 에스이
Publication of KR20120095390A publication Critical patent/KR20120095390A/ko
Ceased legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
KR1020127012330A 2009-10-12 2010-10-11 하나 이상의 착화제 염을 포함하는 분말의 제조 방법 Ceased KR20120095390A (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP09172810 2009-10-12
EP09172810.5 2009-10-12

Publications (1)

Publication Number Publication Date
KR20120095390A true KR20120095390A (ko) 2012-08-28

Family

ID=43499971

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127012330A Ceased KR20120095390A (ko) 2009-10-12 2010-10-11 하나 이상의 착화제 염을 포함하는 분말의 제조 방법

Country Status (15)

Country Link
US (1) US9540597B2 (enExample)
EP (1) EP2488291B1 (enExample)
JP (1) JP6243120B2 (enExample)
KR (1) KR20120095390A (enExample)
CN (1) CN102574083B (enExample)
AU (1) AU2010305833A1 (enExample)
BR (1) BR112012008666B1 (enExample)
CA (1) CA2776570A1 (enExample)
ES (1) ES2531306T3 (enExample)
MX (1) MX2012004170A (enExample)
MY (1) MY156376A (enExample)
PL (1) PL2488291T3 (enExample)
RU (1) RU2554932C2 (enExample)
WO (1) WO2011045266A1 (enExample)
ZA (1) ZA201203359B (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
JP6243120B2 (ja) 2009-10-12 2017-12-06 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ １種以上の錯化剤の塩を含む粉末の製造方法
US8754026B2 (en) 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts
US8785685B2 (en) 2011-04-12 2014-07-22 Basf Se Process for preparing aminopolycarboxylates proceeding from amino acids
GB201214558D0 (en) * 2012-08-15 2012-09-26 Reckitt Benckiser Nv Detergent granule
US10975334B2 (en) * 2015-12-11 2021-04-13 Basf Se Process for manufacturing granules
CN109415662A (zh) * 2016-06-20 2019-03-01 巴斯夫欧洲公司 粉末和颗粒以及制备该粉末和颗粒的方法
EP3746535A1 (en) 2018-01-30 2020-12-09 Eastman Chemical Company Compositions comprising aminocarboxylate chelating agents
US11524931B2 (en) * 2018-03-13 2022-12-13 Taminco Bv Process for drying N,N-dimethyl glycinate salte
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物

Family Cites Families (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2728678A (en) 1946-09-19 1955-12-27 Foremost Dairies Inc Process for drying solutions containing crystallizable material, and product produced thereby
BE572854A (enExample) * 1956-07-06
DE1261619B (de) * 1962-07-12 1968-02-22 Budenheim Rud A Oetker Chemie Verfahren zur Herstellung grobkoerniger Wasch- und Reinigungsmittel
US3615723A (en) * 1970-04-15 1971-10-26 Pillsbury Co Spray-drying apparatus
JPS4924943B1 (enExample) * 1970-06-01 1974-06-26
US3629955A (en) * 1970-07-31 1971-12-28 Procter & Gamble Multilevel spray-drying apparatus
US3717589A (en) * 1970-09-17 1973-02-20 Monsanto Co Sodium nitrilotriacetate and processes for producing same
US3956379A (en) * 1970-10-23 1976-05-11 Ethyl Corporation Process for recovering NTA
JPS5229761B2 (enExample) * 1972-08-17 1977-08-04
JPS52136112A (en) * 1976-05-12 1977-11-14 Nippon Shiryo Kogyo Kk Method of producing saccharified powder containing large amount of difficultly hygroscopic maltose
US4070766A (en) * 1976-09-09 1978-01-31 Stork Friesland B.V. Method and apparatus for preparing a so-called non-caking powder
DE3504896A1 (de) * 1985-02-13 1986-08-14 Basf Ag, 6700 Ludwigshafen Zusaetze fuer wasch- und reinigungsmittel
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DK160809C (da) 1989-01-09 1995-10-02 Niro Holding As Fremgangsmåde og forstøvningstørringsapparat til fremstilling af stabile partikelagglomerater
DE4319935A1 (de) * 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
DE19518986A1 (de) 1995-05-29 1996-12-05 Basf Ag Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium
JP4711471B2 (ja) * 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19640365A1 (de) * 1996-09-30 1998-04-02 Basf Ag Polymer-Wasserstoffperoxid-Komplexe
DE19649681A1 (de) 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
US5968884A (en) * 1997-04-07 1999-10-19 Basf Corporation Concentrated built liquid detergents containing a biodegradable chelant
WO1999061407A1 (en) * 1998-05-27 1999-12-02 Showa Denko K.K. Processes for producing amino acid having secondary or tertiary amino group and three or more carboxyl groups and its salt
EP1176137B1 (en) * 1999-04-30 2004-06-30 Mitsubishi Rayon Co., Ltd. Powdery s,s-ethylenediamine-n,n'-disuccinic acid iron complex and process for producing the same
DE19927537A1 (de) * 1999-06-16 2000-12-21 Merck Patent Gmbh Sprühtrocknungsanlage und Verfahren zu ihrer Verwendung
US6451224B1 (en) * 1999-07-21 2002-09-17 The Dow Chemical Company Stable free-flowing solid chelants
DE10161402A1 (de) 2001-12-13 2003-06-18 Merck Patent Gmbh Verfahren zur Herstellung von direkt tablettierbarem beta-Mannit
EP1354939A1 (en) * 2002-04-19 2003-10-22 The Procter & Gamble Company Pouched cleaning compositions
JP4189208B2 (ja) 2002-11-27 2008-12-03 花王株式会社 界面活性剤担持用粒子群
US7442679B2 (en) * 2004-04-15 2008-10-28 Ecolab Inc. Binding agent for solidification matrix comprising MGDA
DE102005021055A1 (de) 2005-05-06 2006-11-09 Basf Ag Verfahren zur Herstellung von nebenproduktarmen Methylglycin-N,N-diessigsäure-Trialkalimetallsalzen
CN101528907A (zh) * 2006-08-10 2009-09-09 巴斯夫欧洲公司 用于洗碗机的清洁配制物
WO2009092699A1 (en) 2008-01-24 2009-07-30 Unilever Nv Machine dishwash detergent compositions
PL3061744T3 (pl) * 2008-04-01 2018-10-31 Unilever N.V. Wytwarzanie sypkich granul kwasu metyloglicynodioctowego
FR2935383B1 (fr) * 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
WO2010133617A1 (de) * 2009-05-20 2010-11-25 Basf Se Verfahren zur herstellung eines sprühpulvers enthaltend ein oder mehrere glycin-n,n-diessigsäure-derivate und verwendung des sprühpulvers zur herstellung von pressagglomeraten
DE102009038951A1 (de) 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
JP6243120B2 (ja) 2009-10-12 2017-12-06 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ １種以上の錯化剤の塩を含む粉末の製造方法
DE102009060814A1 (de) * 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
US8754026B2 (en) * 2010-09-27 2014-06-17 Basf Se Process for producing granules comprising one or more complexing agent salts

Also Published As

Publication number Publication date
EP2488291A1 (de) 2012-08-22
CA2776570A1 (en) 2011-04-21
ES2531306T3 (es) 2015-03-12
CN102574083B (zh) 2015-01-28
AU2010305833A1 (en) 2012-04-19
PL2488291T3 (pl) 2015-05-29
BR112012008666A2 (pt) 2016-04-19
RU2012119166A (ru) 2013-11-20
JP6243120B2 (ja) 2017-12-06
MX2012004170A (es) 2012-05-08
US9540597B2 (en) 2017-01-10
MY156376A (en) 2016-02-15
US20120202731A1 (en) 2012-08-09
JP2013507499A (ja) 2013-03-04
CN102574083A (zh) 2012-07-11
ZA201203359B (en) 2013-07-31
WO2011045266A1 (de) 2011-04-21
EP2488291B1 (de) 2014-12-10
BR112012008666B1 (pt) 2018-09-18
RU2554932C2 (ru) 2015-07-10

Similar Documents

Publication Publication Date Title
US9540597B2 (en) Process for the preparation of a powder comprising one or more complexing agent salts
CA2719754C (en) Preparation of free flowing granules of methylglycine diacetic acid
EP2718412B1 (en) Builder granules and process for their preparation
CA2762507C (en) Process for the preparation of a powder comprising one or more derivatives of glycine-n,n-diacetic acid and/or one or more derivatives of glutamine-n,n-diacetic acid and methylglycine-n,n-diacetic acid trisodium salt powder
CN102725389B (zh) 包含谷氨酸-n,n-二乙酸(glda)或其衍生物的固体及其制备方法
CN109593000B (zh) 含二肽的颗粒体的生产方法
US8748366B2 (en) Process for the preparation of a spray powder comprising one or more glycine-N,N-diacetic acid derivatives and use of the spray powder for producing compression agglomerates
RU2728876C2 (ru) Способ получения гранул
US9562213B2 (en) Process for producing granules comprising one or more complexing agent salts
EP2621892B1 (de) Verfahren zur herstellung eines granulates enthaltend eines oder mehrere komplexbildnersalze
SE452975B (sv) Forfarande for framstellning av granulert stabiliserat natriumperkarbonat

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20120511

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
A201 Request for examination
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20151005

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20170215

Patent event code: PE09021S01D

E601 Decision to refuse application
PE0601 Decision on rejection of patent

Patent event date: 20170821

Comment text: Decision to Refuse Application

Patent event code: PE06012S01D

Patent event date: 20170215

Comment text: Notification of reason for refusal

Patent event code: PE06011S01I