CN102525837A - Astaxanthin-containing bacterial cellulose membrane product - Google Patents
Astaxanthin-containing bacterial cellulose membrane product Download PDFInfo
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- CN102525837A CN102525837A CN2011103500496A CN201110350049A CN102525837A CN 102525837 A CN102525837 A CN 102525837A CN 2011103500496 A CN2011103500496 A CN 2011103500496A CN 201110350049 A CN201110350049 A CN 201110350049A CN 102525837 A CN102525837 A CN 102525837A
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- astaxanthin
- bacterial cellulose
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- cellulose membrane
- arbutin
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Abstract
The invention relates to an astaxanthin-containing bacterial cellulose membrane product. The unique astaxanthin-containing bacterial cellulose membrane product is obtained by uniformly dispersing astaxanthin into a fine mesh-shaped structure of bacterial cellulose. The disadvantage that the astaxanthin cannot be stored for a long time under general preservation conditions is overcome; and meanwhile, a good beauty and skin care product with anti-aging and whitening functions is also provided for consumers. The astaxanthin in the bacterial cellulose membrane product has stable properties, the structure of the astaxanthin cannot be damaged, and the astaxanthin can be slowly and durably released to the applied skin when the product is used, and achieve good effects of resisting senility, oxidization and wrinkles, whitening and protecting sunshine. Meanwhile, the membrane product also has good water supplement and moisturizing effects due to high water retention performance of the bacterial cellulose.
Description
Technical field
The present invention relates to a kind of beauty and skin care product.
Background technology
Astaxanthin is the crayfish shell from the river, a kind of pink group carotene of finding in Concha Ostreae and the salmon, and chemical name is 3; 3 '-dihydroxy-4,4 '-diketo-β, β '-carotene, pigment Aj067-69; CAS No:472-61-7, molecular formula C40H52O4, molecular weight 596.86.Can be blue or green, blue in vivo with protein bound.Antioxidation, defying age, antitumor, the effect of prevention cardiovascular and cerebrovascular disease are arranged.Be the human up to now the strongest antioxidant of nature of finding, its antioxidant activity is considerably beyond existing antioxidant.
The source of astaxanthin mainly is divided into chemosynthesis and natural extract.Commonly used is the natural extract method, normally from processing of aquatic products refuse, cultivation of algae and yeast, extracts astaxanthin, and output is all lower.Astaxanthin can make from carotene with chemical method.Natural astaxanthin is mainly from Haematocoocus Pluvialls.
Astaxanthin is because its antioxidant activity can effectively protect skin to avoid ultraviolet (UVA, infringement UVB).It also has the ability of eliminating free radical, can prevent that Skin Cell from receiving the damage of free radical, reduces the generation of wrinkle and freckle.So it becomes a kind of good novel cosmetic raw material with defying age, whitening function now.
But astaxanthin specific molecule structure has determined also to be easy to receive the effect of light, heat, oxide etc. and has destroyed.Character is unstable, easy loss of activity in the cosmetics goods.
Summary of the invention
To above-mentioned defective, the invention provides a kind of Bacterial cellulose membrane product that contains astaxanthin.
Bacterial cellulose is by the synthetic cellulosic general designation of certain micro-organisms in acetic acid Pseudomonas (Acetobacter), Agrobacterium (Agrobacterium), rhizobium (Rhizobium) and the Sarcina (Sarcina) etc.; It can form unique hyperfine RF through the biosynthesis effect of microorganism.Had a lot of distinguished characteristics, as the elastic modelling quantity of Bacterial cellulose is more than Plant fiber's the several times to ten times, and tensile strength is high; Bacterial fibers have very strong moisture holding capacity.The WRV value of the Bacterial cellulose of undried is up to more than 1000%, and the moisture holding capacity after the lyophilization still surpasses 600%.Suitable through again swelling ability and the cotton linter of 100 ℃ of dried Bacterial cellulose in water; Bacterial fibers have higher biocompatibility, adaptability and good biodegradability.The present invention promptly utilizes the above-mentioned characteristic of Bacterial cellulose, through astaxanthin is dispersed in the meticulous RF of Bacterial cellulose uniformly, has obtained the Bacterial cellulose membrane product of unique astaxanthin-containing.Solved astaxanthin is difficult for long preservation under general preservation condition defective well, offered consumer a kind of extraordinary beauty and skin care product simultaneously again with defying age, whitening function.Astaxanthin character in the said Bacterial cellulose membrane product is highly stable, and structure can not destroyed, and in use can be slowly and muchly astaxanthin be discharged on the deposited skin of institute, play good defying age, antioxidation, crease-resistant, whiten and sun-proof effect.Owing to the high water retention property of Bacterial cellulose, membrane product of the present invention also has extraordinary replenishing water and preserving moisture effect simultaneously.
Employed astaxanthin among the present invention can be natural astaxanthin or synthesizing astaxanthin.Be preferably the astaxanthin of natural extract, effect is best.
In order to play better beautifying skin-protection function, Bacterial cellulose membrane product of the present invention can also contain other an amount of skin care ingredients, and these skin care ingredients include but not limited to have the coenzyme Q10 of crease-resistant effect and/or the arbutin of whitening function.
The method for preparing that contains the Bacterial cellulose membrane product of astaxanthin of the present invention is that the astaxanthin Emulsion with mass concentration 1% is added in the Bacterial cellulose fermentation medium, and making the content astaxanthin in the culture medium is 20-500ppm; Utilize this fermentation medium static fermentation to produce Bacterial cellulose again, obtain the Bacterial cellulose membrane product of astaxanthin-containing.The Bacterial cellulose membrane product that obtains thus can be enclosed in astaxanthin in its meticulous RF, is able to the stable of retention properties; In use, can slowly and muchly discharge again.Adding other skin protection materials if desired, also is it to be added into carry out biosynthesis in the fermentation medium, and as also being added with coenzyme Q10 and/or arbutin in the culture medium, wherein the addition of coenzyme Q10 is that to make the coenzyme Q10 content in the culture medium be 10-100ppm; The addition of arbutin is that to make the arbutin content in the culture medium be 5-50ppm.This kind method is applicable to the skin protection material that molecular weight is moderate, and it is water insoluble generally speaking, or unstable chemcial property.With being added into fermentation medium after its emulsifying, in the biosynthetic process of Bacterial cellulose, it being surrounded wherein, but can not influence its chemical property; And these skin protection materials can not influence the synthetic of Bacterial cellulose yet.
Coenzyme Q10 wherein, Chinese another name: coenzyme; Ubiquinone; Ubidecarenone; Co-ferment Q10; CAS RN.:303-98-0; Molecular formula: C59H90O4; Meeting light is prone to decompose; Can be widely used in industries such as food, cosmetics, dietary supplement.Be a kind of antioxidant and nonspecific immunity strengthening agent.It is water insoluble; The Emulsion that is prepared into debita spissitudo is added in the fermentation medium, in the biosynthetic process of Bacterial cellulose, it is wrapped in RF, in use; Obtain slowly and muchly discharging with astaxanthin, play very effective defying age, crease-resistant effect.
Arbutin wherein, chemical name: right-hydroxy benzenes-β-the D-pyranglucoside, another name: Arbutin, Arbutin, ericalin; Arbutin, Arbutosie, Ursin, Uresol; Arbutus extract, molecular formula: C12H16O7, molecular weight: 272.25, CAS number: 497-76-7.The arbutin extraction is from the leaf of Folium Vaccinii vitis-idaeae, and it can infiltrate skin rapidly, when not influencing cell proliferation concentration; Can suppress the activity of the tryrosinase in the skin effectively, block melanic formation, directly combine with cheese ammonia enzyme through self; Quicken melanic decomposition and drainage, thereby reduce skin pigment deposition, dispelling stain and freckle; And melanocyte do not produced side effect such as toxic, zest, sensitization, also have the effect of antibacterial, antiinflammatory simultaneously.It is a kind of raw material of whitening safely and effectively.Arbutin can be water-soluble, but character is unstable, decomposes easily.The present invention is used arbutin and astaxanthin; The strong anti-oxidation activity of astaxanthin is good protective agent for arbutin; Both ideally merge in the RF of Bacterial cellulose for it, play effectiveness simultaneously, play preserve moisture, whiten, sun-proof, the anti-ageing effect of waiting for a long time.Use the membrane product of arbutin to be preferably in the use at night.
In the above-mentioned method for preparing, the fermented bacterium of Bacterial cellulose is preferably acetobacter xylinum or gluconate pyracetobacillus.Contain the carbon source and the nitrogenous source of the capacity that supplies strain growth in the fermentation medium, carbon source is preferably glucose, fructose, sucrose and/or Sucus Cocois.
Bacterial cellulose membrane product of the present invention is preferred for preparing the facial film goods of human body face.During use it smoothly is attached at face, holds time more than 30 minutes, life-time service, can play extraordinary defying age, antioxidation, crease-resistant, whiten and sun-proof effect.Also can be cut into different shape, be used to be attached at each position of human body, play corresponding effect, as a kind of high-end cosmetics and skincare product.
The specific embodiment
Below in conjunction with embodiment, specific embodiments of the invention describes in further detail.Following examples are used to explain the present invention, but are not used for limiting scope of the present invention.
Embodiment 1:
A kind of anti-ageing face mask product, it is to be cut into corresponding size by the bacteria cellulose film that contains astaxanthin according to the human body face size.
The method for preparing of the above-mentioned bacteria cellulose film that contains astaxanthin is following:
Natural left-handed astaxanthin Emulsion (emulsifying of the Haematocoocus Pluvialls extract) ASTA-W1 (operative norm Q/YSD03-2009) (available from Jingzhou City's natural astaxanthin company limited) of mass concentration 1% is added in the Bacterial cellulose fermentation medium, and making the content astaxanthin in the culture medium is 200ppm; Also contain the carbon source and the nitrogenous source that can supply gluconate pyracetobacillus fully to grow in the fermentation medium; Utilize this fermentation medium inoculation gluconate pyracetobacillus activated seed liquid; Static fermentation at normal temperatures; Can collect bacterial cellulose wet-coating on the culture medium upper strata in about 8-14 days, this wet film promptly is the bacteria cellulose film of astaxanthin-containing.
Embodiment 2:
A kind of defying age, anti-wrinkle face mask product, it is to be cut into corresponding size by the bacteria cellulose film that contains astaxanthin and coenzyme Q10 according to the human body face size.
The method for preparing of the above-mentioned bacteria cellulose film that contains astaxanthin and coenzyme Q10 is following:
Coenzyme Q10 powder (melt rise bio tech ltd available from Xi'an) is prepared into the Emulsion of mass concentration 1% with an amount of emulsifying agent; Be added into together in the Bacterial cellulose fermentation medium with natural left-handed astaxanthin Emulsion (emulsifying of the Haematocoocus Pluvialls extract) ASTA-W1 (operative norm Q/YSD03-2009) (available from Jingzhou City's natural astaxanthin company limited) of mass concentration 1%; Making the content astaxanthin in the culture medium is 100ppm, and coenzyme Q10 content is 50ppm; Also contain the carbon source and the nitrogenous source that can supply gluconate pyracetobacillus fully to grow in the fermentation medium; Utilize this fermentation medium inoculation gluconate pyracetobacillus activated seed liquid; Static fermentation at normal temperatures; Can collect bacterial cellulose wet-coating on the culture medium upper strata in about 8-14 days, this wet film promptly is the bacteria cellulose film of astaxanthin-containing and coenzyme Q10.
Embodiment 3:
A kind ofly whiten, use mask product antidotal night, it is to be cut into corresponding size by the bacteria cellulose film that contains astaxanthin and arbutin according to the human body face size.
The method for preparing of the above-mentioned bacteria cellulose film that contains astaxanthin and arbutin is following:
Arbutin powder (available from Guangzhou alizarin chemical industry company limited in morning) is dissolved in the warm water below 50 degree; Process the solution of mass concentration 2%; Be added into together in the Bacterial cellulose fermentation medium with natural left-handed astaxanthin Emulsion (emulsifying of the Haematocoocus Pluvialls extract) ASTA-W1 (operative norm Q/YSD03-2009) (available from Jingzhou City's natural astaxanthin company limited) of mass concentration 1%; Making the content astaxanthin in the culture medium is 50ppm, and arbutin content is 50ppm; Also contain the carbon source and the nitrogenous source that can supply gluconate pyracetobacillus fully to grow in the fermentation medium; Utilize this fermentation medium inoculation gluconate pyracetobacillus activated seed liquid; Static fermentation at normal temperatures; Can collect bacterial cellulose wet-coating on the culture medium upper strata in about 8-14 days, this wet film promptly is the bacteria cellulose film of astaxanthin-containing and arbutin.
Embodiment 4:
A kind of defying age, crease-resistant body film product, it is to be cut into corresponding size by the bacteria cellulose film that contains astaxanthin according to the human body size, as is used to be attached at the single piece type body film of arms and legs portion and is used to be attached at northern single piece type body film product etc.
The method for preparing of the above-mentioned bacteria cellulose film that contains astaxanthin is following:
The natural left-handed astaxanthin Emulsion of mass concentration 1% (emulsifying of Haematocoocus Pluvialls extract) ASTA-W1 (operative norm Q/YSD03-2009) (available from Jingzhou City's natural astaxanthin company limited) is added in the Bacterial cellulose fermentation medium, and making the content astaxanthin in the culture medium is 500ppm; Also contain the carbon source and the nitrogenous source that can supply gluconate pyracetobacillus fully to grow in the fermentation medium; Utilize this fermentation medium inoculation gluconate pyracetobacillus activated seed liquid; Static fermentation at normal temperatures; Can collect bacterial cellulose wet-coating on the culture medium upper strata in about 8-14 days, this wet film promptly is the bacteria cellulose film of astaxanthin-containing.
Embodiment 5:
A kind ofly whiten, defying age, crease-resistant body film product; It is to be cut into corresponding size by the bacteria cellulose film that contains astaxanthin, coenzyme Q10 and arbutin according to the human body size, as is used to be attached at the single piece type body film of arms and legs portion and is used to be attached at northern single piece type body film product etc.
The method for preparing of above-mentioned bacteria cellulose film is following:
Coenzyme Q10 powder (melt rise bio tech ltd available from Xi'an) is prepared into the Emulsion of mass concentration 1% with an amount of emulsifying agent; Arbutin powder (available from Guangzhou alizarin chemical industry company limited in morning) is dissolved in the warm water below 50 degree; Process the solution of mass concentration 2%; Natural left-handed astaxanthin Emulsion (emulsifying of Haematocoocus Pluvialls extract) ASTA-W1 (operative norm Q/YSD03-2009) (available from Jingzhou City's natural astaxanthin company limited) with mass concentration 1% is added in the Bacterial cellulose fermentation medium; Making the content astaxanthin in the culture medium is 20ppm, and coenzyme Q10 content is 100ppm, and arbutin content is 10ppm; Also contain the carbon source and the nitrogenous source that can supply gluconate pyracetobacillus fully to grow in the fermentation medium; Utilize this fermentation medium inoculation gluconate pyracetobacillus activated seed liquid; Static fermentation at normal temperatures; Can collect bacterial cellulose wet-coating on the culture medium upper strata in about 8-14 days, this wet film promptly is the bacteria cellulose film of astaxanthin-containing, coenzyme Q10 and arbutin.
The product of the foregoing description 1-5 is offered three groups of aspiration experimenters use, every group 12 people, another is organized 12 people and uses the Bacterial cellulose facial film that do not add astaxanthin or body film as matched group, uses every night 1 time, uses for 2 week, and all the other maintenances are normal.Result of the test finds that three groups of experimenters' skin is Paint Gloss flexible with matched group before comparing and using, and also facial wrinkles or body skin fold alleviate the experimenter of the product of use embodiment 2, embodiment 4 and embodiment 5 to some extent to a certain extent; Skin with matched group before the experimenter of use embodiment 3 and the product of embodiment 5 also compares and uses is more pale.
The above only is a preferred implementation of the present invention; Should be pointed out that for those skilled in the art, under the prerequisite that does not break away from know-why of the present invention; Can also make some improvement and retouching, these improvement and retouching also should be regarded as protection scope of the present invention.
Claims (9)
1. Bacterial cellulose membrane product that contains astaxanthin.
2. Bacterial cellulose membrane product according to claim 1 is characterized in that: said astaxanthin is natural astaxanthin or synthesizing astaxanthin.
3. Bacterial cellulose membrane product according to claim 1 is characterized in that: also contain coenzyme Q10 and/or arbutin.
4. method for preparing that contains the Bacterial cellulose membrane product of astaxanthin, it is characterized in that: the astaxanthin Emulsion of mass concentration 1% is added in the Bacterial cellulose fermentation medium, and making the content astaxanthin in the culture medium is 20-500ppm; Utilize this fermentation medium static fermentation to produce Bacterial cellulose again, obtain the Bacterial cellulose membrane product of astaxanthin-containing.
5. method for preparing according to claim 4 is characterized in that: also be added with coenzyme Q10 and/or arbutin in the fermentation medium, wherein the addition of coenzyme Q10 is that to make the coenzyme Q10 content in the culture medium be 10-100ppm; The addition of arbutin is that to make the arbutin content in the culture medium be 5-50ppm.
6. method for preparing according to claim 4 is characterized in that: said fermented bacterium is acetobacter xylinum or gluconate pyracetobacillus.
7. method for preparing according to claim 4 is characterized in that: contain the carbon source and the nitrogenous source of the capacity that supplies strain growth in the said fermentation medium, carbon source is glucose, fructose, sucrose and/or Sucus Cocois.
8. the facial film goods that are used for human body face that prepare with the described Bacterial cellulose membrane product of claim 1.
9. the membrane product that is used for each position of human body for preparing with the described Bacterial cellulose membrane product of claim 1.
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CN103340819A (en) * | 2013-07-23 | 2013-10-09 | 海南光宇生物科技有限公司 | Preparation method of bacterial cellulose facial mask with anti-radiation effect |
CN103385803B (en) * | 2013-07-23 | 2014-11-19 | 海南光宇生物科技有限公司 | Preparation method of bacterial cellulose compound fish collagen protein facial mask |
CN104000773B (en) * | 2014-06-17 | 2016-07-27 | 广州市雅蝶化妆品制造有限公司 | A kind of natural anti-oxidation modularization cosmetic and preparation method thereof |
CN104000773A (en) * | 2014-06-17 | 2014-08-27 | 广州市雅蝶化妆品制造有限公司 | Natural antioxidant composite cosmetic and preparation method thereof |
CN104825347A (en) * | 2015-05-25 | 2015-08-12 | 广西达庆生物科技有限公司 | Medical biological whitening and spot-removing dressing and preparation method thereof |
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CN109674749A (en) * | 2019-01-07 | 2019-04-26 | 东北林业大学 | A kind of high-content coenzyme Q 10 oral nano suspension and its preparation process |
CN111484902A (en) * | 2019-01-28 | 2020-08-04 | 海南光宇生物科技有限公司 | Preparation method of concentrated enzyme-containing laundry beads |
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CN109966189A (en) * | 2019-04-26 | 2019-07-05 | 北京科技大学 | Anti-oxidant moisturizing micro-organisms living cell preparation and the skincare product containing said preparation |
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