CN106333481B - A kind of nanometer of vitamin bristle and preparation process - Google Patents

A kind of nanometer of vitamin bristle and preparation process Download PDF

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Publication number
CN106333481B
CN106333481B CN201610774981.4A CN201610774981A CN106333481B CN 106333481 B CN106333481 B CN 106333481B CN 201610774981 A CN201610774981 A CN 201610774981A CN 106333481 B CN106333481 B CN 106333481B
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grams
nanometer
vitamin
nano
powder
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CN106333481A (en
Inventor
梁超军
梁超杰
丁胡红
肖问问
肖春晓
闫金丹
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Dongguan City Is Daily Use Products Co Ltd
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Dongguan City Is Daily Use Products Co Ltd
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Classifications

    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/006Antimicrobial, disinfectant bristles, handle, bristle-carrier or packaging
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/02Bristles details
    • A46D1/0207Bristles characterised by the choice of material, e.g. metal
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • A46D1/045Cleaning, e.g. washing, drying
    • AHUMAN NECESSITIES
    • A46BRUSHWARE
    • A46DMANUFACTURE OF BRUSHES
    • A46D1/00Bristles; Selection of materials for bristles
    • A46D1/04Preparing bristles
    • A46D1/06Machines or apparatus for cutting bristles

Abstract

The invention discloses a kind of nanometer of vitamin bristles, by weight, including following component thermoplastic polyester granulate, 40 grams to 60 grams;Nanometer vitamine capsule solution, 25 grams to 30 grams;Crosslinking agent, 5 grams to 10 grams;Nano-magnetic powder, 3 grams to 5 grams;Coral nano powder, 3 grams to 5 grams;Nano pearl powder, 2 grams to 4 grams.Cosmetic brush of the invention its have the effect of that the pitch-dark degree of reduction skin of face of conspicuousness, cosmetic brush of the invention also have anti-aging, antiplaque and other effects.

Description

A kind of nanometer of vitamin bristle and preparation process
Technical field
The present invention relates to bristle preparation process, cosmetic brush technical field more particularly to a kind of nanometer of vitamin bristle and systems Standby technique.
Background technique
The bristle of professional color make-up brushing tool is generally divided into two kinds of hair of animal wool and synthesis.Natural animal felt has complete hair scale Piece, therefore hair quality is soft, eats powder degree saturation, uniform in color can be made docile, and do not stimulate skin.It is well known that vitamin C and Vitamin E can strengthen immunity, beauty and skin care.Since microorganism Vc is a kind of extremely unstable substance, skin is difficult to whole It absorbs.Existing cosmetic brush product, generallys use existing bristle and technique is made, and does not have release dimension in use Raw element arrives the function of skin surface, in use, it is difficult to which timely to skin replenishing vitamins, thus it is difficult to meet more The high market demand, the problems demand solve.
Summary of the invention
A kind of nanometer of vitamin bristle is provided it is an object of the invention to overcome the deficiency of the above-mentioned prior art, the present invention Using the derivative of vitamin V c, the stability of vitamin V c is improved, this vitamin V c derivative is easy to be absorbed by the skin, And Vc form can be changed into again in skin, while vitamin C has attack to pathogen, enhances human immunity, it helps White blood cell as area function center strength works.
To achieve the above object, the present invention provides a kind of nanometer of vitamin bristle, by weight, including following component:
Thermoplastic polyester particle, 40 grams to 60 grams;
Nanometer vitamine capsule solution, 25 grams to 30 grams;
Crosslinking agent, 5 grams to 10 grams;
Nano-magnetic powder, 3 grams to 5 grams;
Coral nano powder, 3 grams to 5 grams;
Nano pearl powder, 2 grams to 4 grams.
Preferably, by weight, it also comprises the following components: hyaluronic acid, 1 gram to 3 grams.
Preferably, by weight, it also comprises the following components: the Chinese herbal medicine extract dry powder with whitening effect, 0.2 gram To 0.5 gram.
Preferably, by weight, it also comprises the following components: natural perfume material, 0.1 gram to 0.2 gram.
Preferably, by weight, it also comprises the following components: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
Preferably, by weight, it also comprises the following components: soft agent, 2 grams to 10 grams.
Preferably, by weight, the thermoplastic polyester particle is PBT particle;The nanometer vitamine capsule solution It is the solution of vitamin nano capsule VCE5788.
The present invention also provides the preparation processes of a kind of nanometer of vitamin bristle, include the following steps:
By weight ratio mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder by S801;Add Enter 30% nanometer vitamine capsule solution;Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;
S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid;
S803 is put into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution after fixation and crosslinking agent passes through High temperature dye vat is warming up to 80 to 110 degree heat preservation 30 minutes;
S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.
Preferably, include the following steps:
S801, by weight ratio, by PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, in Mixer is added in herb extracts dry powder, natural perfume material, polynucleotide extract dry powder, soft agent;30% nanometer vitamin is added Capsule solution mixes 40 minutes;Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;
S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then Subtract material process equipment with laser and further modifies hair peak;
S803 is put into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution after fixation and crosslinking agent passes through High temperature dye vat is warming up to 80 to 110 degree heat preservation 30 minutes;
S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.
The beneficial effects of the present invention are:
1, preparation process of the invention is simple, cheap, the products such as cosmetic brush prepared by this technique its be rich in micro- life Object derivative (or vitamin C), vitamin E (tocopherol), these vitamins make skin health and high resilience and gloss, right The skin of human body has good protective effect, have whitening, delay senescence and other effects.The present invention has excellent moisture absorption and moisture retention Can, regain has the function of hydroscopic fast-drying and antistatic up to 15% or more.Cosmetic brush of the invention has good comfortable Property and taking are small to skin irritation.
It 2, is Microbial biomass C present invention employs vitamin nano capsule, specially vitamin nano capsule VCE5788 The full capsule type Nano capsule of derivative and vitamin E, the arrangement suitable for cotton, hair, silk, fiber crops, chemical & blended fabric and ready-made clothes.It arranges After fabric stress afterwards, microcapsules are impaired, and Microbial biomass C derivative and microorganism E overflow, and by skin absorbed themselves, play skin care Beauty treatment, the function of preventing skin from corrugating etc..Such as without external force, microcapsules are not then damaged, and effect is lasting saves, and never disappear It loses.The capsule of nano in bristle after use, when using cosmetic brush in skin surface brush, microcapsules in bristle, especially It is that the microcapsules of bristle ends are started breakage by external force such as frictional force and pressure, after microcapsules are damaged, content is opened Begin to discharge, in the cell of skin surface.Skin Cell absorbs vitamin, to supplement the micro- of skin surface cell Biology can eliminate intracellular Superoxide radical anion since injection Vitamin B_6 has antioxidation, prolong to have Slow aging, delay color spot such as form at the good beauty, health-care efficacy.During use, with the abrasion of bristle, bristle End face is gradually moved, and discharges content so as to there is microcapsules damaged always.
3, it is proved by statistics, its whitening effect of cosmetic brush of the invention has 99% or more a possibility that be higher than generalization Adornment brush, whitening effect are superior.
4, the used bristle of cosmetic brush is all filling material, made by traditional handicraft currently on the market, with the development of society, Pursuit of the mankind to quality of the life, the attention to safety, we pass through research and development in 2 years, invent nano microbeam bristle, will Suitable for fields such as cosmetic brush, wig makeups tool, accessories.The present invention is widely used in medical treatment, and prove it is safe and efficient, to skin It is nonirritant, it is nontoxic, without allergic reaction.
Detailed description of the invention
Fig. 1 is the initial condition data figure that the present invention tests;
Fig. 2 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group respectively represents hairbrush D Group, hairbrush A group, hairbrush B group, hairbrush C group;Ordinate represents the pitch-dark degree of skin, becomes between pitch-dark degree from 0 to 10 Change;
Fig. 3 is that face test area divides schematic diagram in experimental design of the present invention;
Appended drawing reference:
The area A 10;
The area B 20;
The area C 30;
The area D 40.
Specific embodiment
Embodiment one: formula and preparation process
Preparation process is as follows: S801, by weight ratio, by PBT particle, nano-magnetic powder, coral nano powder, nano-pearl Mixer is added in powder, hyaluronic acid, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent;It is added 30% nanometer vitamine capsule solution mixes 40 minutes;Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;S802, It is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then subtract material processing with laser Equipment further modifies hair peak;S803 is put into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution after fixation 80 to 110 degree heat preservation 30 minutes is warming up to by high temperature dye vat with crosslinking agent;S804 is cleaned again, is dehydrated, into oven 110 Degree baking is dried for 100 minutes.Wherein, organic acid is citric acid.Nanometer vitamine capsule solution is mass concentration expression.
Embodiment two: antibacterial effect experimental design and experimental result
Fig. 1 and Fig. 2 are please referred to, 80 volunteers are randomly choosed, is divided into tetra- groups of A, B, C, D, each group includes 20 members. The face of each volunteer is divided into four regions, is divided into the area A 10, the area B 20, the area C 30, the area D 40.The area A 10 is prepared using prescription A Cosmetic brush, the cosmetic brush that the area B 20 is prepared using prescription B;The cosmetic brush that the area C 30 is prepared using prescription C.Cosmetic brush is used daily To each volunteer's brush face (not brushing cosmetics), brush 5 minutes every time.Continue 15 days, after the 15th day, with Visia skin The pitch-dark degree of skin detector test skin.
The pitch-dark degree under initial conditions is recorded below:
Experimental data after 15 days
Example IV: statistics conclusion
From Fig. 1 it can be found that the pitch-dark degree for 80 volunteer its skin of face chosen is more uniform, meet experiment It is required that.
From Fig. 2 it can be found that by experiment, its pitch-dark degree of control group (D group) does not change substantially, but experimental group (A Group, B group, C group) reduction by a relatively large margin is all presented in its pitch-dark degree, and the reduction amplitude of C group is maximum.
In addition, carrying out statistical test (T inspection):
One, the T of experimental group A group experiment front and back is examined, and P=4.31357E-20 < 0.01 illustrates there is 99% a possibility that, A group The experiment front and back phase, pitch-dark degree had significant difference, and cosmetic brush A has the whitening effect of conspicuousness;
Two, the T of experimental group B group experiment front and back is examined, and P=7.9546E-25 < 0.01 illustrates there is 99% a possibility that, and B group is real Testing front and back phase pitch-dark degree has significant difference, and cosmetic brush B has the whitening effect of conspicuousness;
Three, the T of experimental group C group experiment front and back is examined, and P=2.65403E-27 < 0.01 illustrates there is 99% a possibility that, C group The experiment front and back phase, pitch-dark degree had significant difference, and cosmetic brush C has the whitening effect of conspicuousness;
Four, experimental group C and experimental group A, the T after experiment are examined, and P=2.46199E-24 < 0.01 illustrates there is 99% Possibility, C group, A group pitch-dark degree have significant difference, cosmetic brush C than cosmetic brush A compare with conspicuousness whitening imitate Fruit.
In conclusion statistically, its reduction skin of face with conspicuousness of cosmetic brush of the invention is pitch-dark The effect of degree, that is to say, that its whitening effect with conspicuousness, statistically, conclusion has 99% or more possibility Property is effective.In addition, cosmetic brush of the invention also has anti-aging, antiplaque and other effects.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example Property, it is not considered as limiting the invention, those skilled in the art are not departing from the principle of the present invention and objective In the case where can make changes, modifications, alterations, and variations to the above described embodiments within the scope of the invention.

Claims (9)

1. a kind of nanometer of vitamin bristle, which is characterized in that calculate by weight, including following component:
Thermoplastic polyester particle, 40 grams to 60 grams;
Nanometer vitamine capsule solution, 25 grams to 30 grams;
Crosslinking agent, 5 grams to 10 grams;
Nano-magnetic powder, 3 grams to 5 grams;
Coral nano powder, 3 grams to 5 grams;
Nano pearl powder, 2 grams to 4 grams;
The thermoplastic polyester particle is PBT particle;
It is formulated by weight, mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder;Addition 30% is received Rice vitamine capsule solution;Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;It is cut into chunks according to customization size, utilizes hydroxide Sodium burns a mao peak, is then cleaned using organic acid;It is put into the dyeing of dye vat equipment, adds 30% nanometer of vitamin glue after fixation Capsule solution and crosslinking agent are warming up to 80 to 110 degree by high temperature dye vat and keep the temperature 30 minutes;It cleans, be dehydrated, into oven 110 again Degree baking is dried for 100 minutes.
2. according to claim 1 nanometer of vitamin bristle, which is characterized in that calculate by weight, also comprise the following components: Hyaluronic acid, 1 gram to 3 grams.
3. according to claim 2 nanometer of vitamin bristle, which is characterized in that calculate by weight, also comprise the following components: Chinese herbal medicine extract dry powder with whitening effect, 0.2 gram to 0.5 gram.
4. according to claim 3 nanometer of vitamin bristle, which is characterized in that calculate by weight, also comprise the following components: Natural perfume material, 0.1 gram to 0.2 gram.
5. according to claim 4 nanometer of vitamin bristle, which is characterized in that calculate by weight, also comprise the following components: Polynucleotide extract dry powder, 0 .01 grams to 0 .03 grams.
6. according to claim 5 nanometer of vitamin bristle, which is characterized in that calculate by weight, also comprise the following components: Soft agent, 2 grams to 10 grams.
7. according to claim 1 ~ 6 described in any item nanometers of vitamin bristles, which is characterized in that the nanometer vitamine capsule Solution is the solution of vitamin nano capsule VCE5788.
8. the preparation process of a kind of nanometer of vitamin bristle according to claim 6, which is characterized in that including walking as follows It is rapid:
S801 is formulated by weight, and mixer is added in PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder;It is added 30% nanometer vitamine capsule solution;Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;
S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid;
S803 is put into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution after fixation and crosslinking agent passes through high temperature Dye vat is warming up to 80 to 110 degree heat preservation 30 minutes;
S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.
9. the preparation process of a kind of nanometer of vitamin bristle according to claim 8, which is characterized in that including walking as follows It is rapid:
S801, by weight ratio, by PBT particle, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, Chinese herbal medicine Mixer is added in extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent;30% nanometer vitamine capsule is added Solution mixes 40 minutes;Drying 1.5 hours, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons;
S802 is cut into chunks according to customization size, burns a mao peak using sodium hydroxide, then cleaned using organic acid, then with sharp Light subtracts material process equipment and further modifies hair peak;
S803 is put into the dyeing of dye vat equipment, add after fixation 30% nanometer of vitamine capsule solution and 30% crosslinking agent it is logical It crosses high temperature dye vat and is warming up to 80 to 110 degree heat preservation 30 minutes;
S804 is cleaned again, is dehydrated, toasting 100 minutes and dry into 110 degree of oven.
CN201610774981.4A 2016-08-31 2016-08-31 A kind of nanometer of vitamin bristle and preparation process Active CN106333481B (en)

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018112813A1 (en) * 2016-12-22 2018-06-28 东莞市正和日用制品有限公司 Vitamin nanobristle formula and preparation process
CN110158182A (en) * 2018-02-26 2019-08-23 沧州成浩化妆用具有限公司 A kind of novel artificial hair of the cosmetic brush with antibacterial functions

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1113973A (en) * 1994-06-24 1995-12-27 温一林 Producing method for antibiotic health tooth-brush
JP2009285445A (en) * 2008-04-28 2009-12-10 Fuji Chemical Kk Anti-bacterial make-up brush and method of manufacturing brush bristle
CN102462151A (en) * 2010-11-05 2012-05-23 Hct亚洲有限公司 Brush with magnetic filaments
CN104367247A (en) * 2014-05-04 2015-02-25 爱丽丝·常 Face and body brush with thin and conical bristles, mixture compositions and massage face

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG177474A1 (en) * 2009-07-31 2012-02-28 Colgate Palmolive Co High cleaning dentifrice compositions

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1113973A (en) * 1994-06-24 1995-12-27 温一林 Producing method for antibiotic health tooth-brush
JP2009285445A (en) * 2008-04-28 2009-12-10 Fuji Chemical Kk Anti-bacterial make-up brush and method of manufacturing brush bristle
CN102462151A (en) * 2010-11-05 2012-05-23 Hct亚洲有限公司 Brush with magnetic filaments
CN104367247A (en) * 2014-05-04 2015-02-25 爱丽丝·常 Face and body brush with thin and conical bristles, mixture compositions and massage face

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