CN106333481A - Formula of nanometer vitamin brush bristle and preparation technology - Google Patents
Formula of nanometer vitamin brush bristle and preparation technology Download PDFInfo
- Publication number
- CN106333481A CN106333481A CN201610774981.4A CN201610774981A CN106333481A CN 106333481 A CN106333481 A CN 106333481A CN 201610774981 A CN201610774981 A CN 201610774981A CN 106333481 A CN106333481 A CN 106333481A
- Authority
- CN
- China
- Prior art keywords
- nanometer
- grams
- vitamin
- powder
- nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011782 vitamin Substances 0.000 title claims abstract description 41
- 229940088594 vitamin Drugs 0.000 title claims abstract description 26
- 229930003231 vitamin Natural products 0.000 title claims abstract description 26
- 235000013343 vitamin Nutrition 0.000 title claims abstract description 26
- 150000003722 vitamin derivatives Chemical class 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims description 13
- 238000005516 engineering process Methods 0.000 title claims description 10
- 239000000843 powder Substances 0.000 claims abstract description 23
- 239000002775 capsule Substances 0.000 claims abstract description 18
- 239000006247 magnetic powder Substances 0.000 claims abstract description 9
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 8
- 229920000728 polyester Polymers 0.000 claims abstract description 5
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 5
- 239000004416 thermosoftening plastic Substances 0.000 claims abstract description 5
- WIGIZIANZCJQQY-UHFFFAOYSA-N 4-ethyl-3-methyl-N-[2-[4-[[[(4-methylcyclohexyl)amino]-oxomethyl]sulfamoyl]phenyl]ethyl]-5-oxo-2H-pyrrole-1-carboxamide Chemical compound O=C1C(CC)=C(C)CN1C(=O)NCCC1=CC=C(S(=O)(=O)NC(=O)NC2CCC(C)CC2)C=C1 WIGIZIANZCJQQY-UHFFFAOYSA-N 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000008187 granular material Substances 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 230000002087 whitening effect Effects 0.000 claims description 11
- 241001450685 Corallium japonicum Species 0.000 claims description 8
- 235000005956 Cosmos caudatus Nutrition 0.000 claims description 8
- 244000293323 Cosmos caudatus Species 0.000 claims description 8
- 239000011858 nanopowder Substances 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
- 241000411851 herbal medicine Species 0.000 claims description 6
- 150000007524 organic acids Chemical class 0.000 claims description 6
- 239000002304 perfume Substances 0.000 claims description 6
- 239000002157 polynucleotide Substances 0.000 claims description 6
- 102000040430 polynucleotide Human genes 0.000 claims description 6
- 108091033319 polynucleotide Proteins 0.000 claims description 6
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 5
- 230000018044 dehydration Effects 0.000 claims description 5
- 238000006297 dehydration reaction Methods 0.000 claims description 5
- 238000004043 dyeing Methods 0.000 claims description 5
- 229920002674 hyaluronan Polymers 0.000 claims description 5
- 229960003160 hyaluronic acid Drugs 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- 239000002088 nanocapsule Substances 0.000 claims description 5
- 238000005491 wire drawing Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 3
- 230000008439 repair process Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 2
- 239000002537 cosmetic Substances 0.000 abstract description 20
- 230000000694 effects Effects 0.000 abstract description 6
- 230000032683 aging Effects 0.000 abstract description 3
- 235000014653 Carica parviflora Nutrition 0.000 abstract 1
- 241000243321 Cnidaria Species 0.000 abstract 1
- 230000003247 decreasing effect Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 235000019362 perlite Nutrition 0.000 abstract 1
- 239000010451 perlite Substances 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 21
- 238000002474 experimental method Methods 0.000 description 9
- 210000004209 hair Anatomy 0.000 description 6
- 238000007689 inspection Methods 0.000 description 6
- 239000003094 microcapsule Substances 0.000 description 6
- 244000005700 microbiome Species 0.000 description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- 241001597008 Nomeidae Species 0.000 description 4
- 229960005070 ascorbic acid Drugs 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000001680 brushing effect Effects 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000013401 experimental design Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 206010002198 Anaphylactic reaction Diseases 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- OUUQCZGPVNCOIJ-UHFFFAOYSA-M Superoxide Chemical compound [O-][O] OUUQCZGPVNCOIJ-UHFFFAOYSA-M 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000036783 anaphylactic response Effects 0.000 description 1
- 208000003455 anaphylaxis Diseases 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000002882 anti-plaque Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 210000000265 leukocyte Anatomy 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 230000036559 skin health Effects 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 238000000528 statistical test Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/006—Antimicrobial, disinfectant bristles, handle, bristle-carrier or packaging
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/02—Bristles details
- A46D1/0207—Bristles characterised by the choice of material, e.g. metal
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
- A46D1/045—Cleaning, e.g. washing, drying
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
- A46D1/06—Machines or apparatus for cutting bristles
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a formula of a nanometer vitamin brush bristle. The formula comprises the following components by weight: 40 to 60g of thermoplastic polyester particles, 25 to 30g of nanometer vitamin capsule solution, 5 to 10g of crosslinking agent, 3 to 5g of nanometer magnetic powder, 3 to 5g of coral nanometer powder, and 2 to 4g of nanometer perlite powder. A cosmetic brush has the effects that the dark degree of face skin is obviously decreased, the aging and color spot are resisted, and the like.
Description
Technical field
The present invention relates to bristle preparation technology, cosmetic brush technical field, more particularly, to a kind of nanometer vitamin bristle formula
And preparation technology.
Background technology
The bristle of professional color make-up brushing tool is generally divided into animal wool and two kinds of hair of synthesis.Natural animal felt has complete hair scale
Piece, therefore hair matter are soft, eat powder degree saturation, uniform in color can be made docile, and do not stimulate skin.It is known that vitamin c and
Vitamin e can enhancing immunity, beauty and skin care.Because microorganism vc is a kind of material of extremely unstable, skin is difficult to all
Absorb.Existing cosmetic brush product, it is generally made using existing bristle and technique, does not have release dimension in use
To the function of skin surface, in use it is difficult to timely to skin vitimin supplement, thus it is difficult to meet more raw element
The high market demand, this problems demand solves.
Content of the invention
It is an object of the invention to overcoming the deficiency of above-mentioned prior art and providing a kind of nanometer vitamin bristle formula, this
Invention, using the derivant of vitamin vc, improves the stability of vitamin vc, this vitamin vc derivant is easily by skin
Absorb, and vc form can be changed in skin again, vitamin c has attack to pathogen simultaneously, strengthen body immunity,
Help be operated as the leukocyte of area function center strength.
For achieving the above object, the present invention provides a kind of nanometer vitamin bristle formula, by weight, including such as the following group
Point:
Thermoplastic polyester granule, 40 grams to 60 grams；
Nanometer vitamine capsule solution, 25 grams to 30 grams；
Cross-linking agent, 5 grams to 10 grams；
Nano-magnetic powder, 3 grams to 5 grams；
Corallium Japonicum Kishinouye nano powder, 3 grams to 5 grams；
Nanometer Margarita powder, 2 grams to 4 grams.
Preferably, by weight, also comprise the following components: hyaluronic acid, 1 gram to 3 grams.
Preferably, by weight, also comprise the following components: there is the Chinese herbal medicine extract dry powder of whitening effect, 0.2 gram
To 0.5 gram.
Preferably, by weight, also comprise the following components: natural perfume material, 0.1 gram to 0.2 gram.
Preferably, by weight, also comprise the following components: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
Preferably, by weight, also comprise the following components: soft agent, 2 grams to 10 grams.
Preferably, by weight, described thermoplastic polyester granule is pbt granule；Described nanometer vitamine capsule solution
It is the solution of vitamin nano capsule vce5788.
The present invention also provides a kind of preparation technology of nano-antibacterial bristle, comprises the steps:
S801, by weight ratio, pbt granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder is added mixer；Add
30% nanometer vitamine capsule solution；Dry, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；
S802, cuts into chunks according to customization size, burns a mao peak using sodium hydroxide, then utilizes organic acid to clean；
S803, puts into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution and cross-linking agent passes through high temperature after fixation
Dye vat is warmed up to 80 to 110 degree insulation 30 minutes；
S804, cleaning, dehydration, 110 degree of bakings of entrance baking box again are dried for 100 minutes.
Preferably, comprise the steps:
S801, by weight ratio, by pbt granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, hyaluronic acid, Chinese herbal medicine
Extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30% nanometer vitamine capsule
Solution, mixes 40 minutes；Dry 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；
S802, cuts into chunks according to customization size, burns a mao peak using sodium hydroxide, then utilizes organic acid to clean, then with swashing
Light subtracts material process equipment and repairs a mao peak further；
S803, puts into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution and cross-linking agent passes through high temperature after fixation
Dye vat is warmed up to 80 to 110 degree insulation 30 minutes；
S804, cleaning, dehydration, 110 degree of bakings of entrance baking box again are dried for 100 minutes.
The invention has the beneficial effects as follows:
1st, the preparation process is simple of the present invention, cheap, the product such as cosmetic brush prepared by this technique its spread out rich in microorganism
Biological (or vitamin c), vitamin e(tocopherol), these vitamin make skin health and high resilience and gloss, to human body
Skin have good protective effect, have the effects such as whitening, slow down aging.The present invention has excellent moisture absorption and performance of keeping humidity,
Regain, up to more than 15%, has hydroscopic fast-drying and anlistatig effect.The cosmetic brush of the present invention have good comfortableness and
Taking is little to skin irritation.
2nd, present invention employs vitamin nano capsule, specially vitamin nano capsule vce5788, it is microorganism c
The full capsule type Nano capsule of derivant and vitamin e is it is adaptable to the arrangement of cotton, hair, silk, fiber crops, chemical ＆ blended fabric and ready-made clothes.Arrange
After fabric stress afterwards, microcapsule is impaired, and microorganism c derivant and microorganism e overflow, and by skin absorbed themselves, play skin protection
Skin care, the function of preventing skin from corrugating etc..As no external force acts on, microcapsule is not then damaged, and effect persists, and never disappears
Lose.After this capsule of nano uses in bristle, when using cosmetic brush in skin surface brush, the microcapsule in bristle, especially
Be bristle ends microcapsule be subject to the external force such as frictional force and pressure and start breakage, microcapsule breakage after, its inclusions is opened
Begin to discharge, in the middle of the cell of skin surface.Skin Cell absorbs vitamin, thus supplementing the micro- of skin surface cell
Biology, because vitamin c, e have antioxidation, can eliminate intracellular Superoxide radical anion, thus have prolonging
Slow aging, postpones good beauty treatment, the health-care effecies such as mottle formation.During using, with the abrasion of bristle, bristle
End face gradually moves, and discharges content such that it is able to there be microcapsule damaged always.
3rd, prove through statistics, its whitening effect of the cosmetic brush of the present invention have more than 99% probability be higher than generalization
Adornment brush, whitening effect is superior.
4th, cosmetic brush institute is all made by filling material, traditional handicraft using bristle in the market, with social development,
The pursuit to quality of the life for the mankind, the attention to safety, we, through the research and development of 2 years, invent nano microbeam bristle, will
It is applied to the fields such as cosmetic brush, wig makeups instrument, accessory.The present invention is widely used in medical treatment, and proves safe and efficient, to skin
Nonirritant, nontoxic, no anaphylaxiss.
Brief description
Fig. 1 is the initial condition data figure of present invention experiment；
Fig. 2 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group represents hairbrush d group, hair respectively
Brush a group, hairbrush b group, hairbrush c group；Vertical coordinate represents the pitch-dark degree of skin, and pitch-dark degree changes between 0 to 10；
Fig. 3 is that in experimental design of the present invention, face pilot region divides schematic diagram;
Reference:
A area 10；
B area 20；
C area 30；
D area 40.
Specific embodiment
Embodiment one: formula and preparation technology
| A(gram of prescription) | B(gram of prescription) | C(gram of prescription) | |
| Pbt granule | 40 | 50 | 60 |
| Nanometer silver antimicrobial liquid | 25 | 28 | 30 |
| Nano-magnetic powder | 3 | 4 | 5 |
| Corallium Japonicum Kishinouye nano powder | 3 | 4 | 5 |
| Nanometer Margarita powder | 2 | 3 | 4 |
| Hyaluronic acid | 1 | 2 | 3 |
| There is the Chinese herbal medicine extract dry powder of whitening effect | 0.2 | 0.3 | 0.5 |
| Natural perfume material | 0.1 | 0.15 | 0.2 |
| Polynucleotide extract dry powder | 0.01 | 0.02 | 0.03 |
| Soft agent | 2 | 5 | 10 |
| Cross-linking agent | 5 | 8 | 10 |
Preparation technology is as follows: s801, by weight ratio, by pbt granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, thoroughly
Bright matter acid, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30%
Nanometer vitamine capsule solution, mixes 40 minutes；Dry 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；S802, according to
Customization size is cut into chunks, and burns a mao peak using sodium hydroxide, then utilizes organic acid to clean, then subtracts material process equipment with laser
Repair hair peak further；S803, puts into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution and friendship after fixation
Connection agent is warmed up to 80 to 110 degree insulation 30 minutes by high temperature dye vat；S804, cleaning, dehydration, 110 degree of bakings of entrance baking box again
Dry within roasting 100 minutes.Wherein, organic acid is citric acid.Nanometer vitamine capsule solution represents for mass concentration.
Embodiment two: antibacterial effect experimental design and experimental result
Refer to Fig. 1 and Fig. 2, randomly choose 80 volunteers, be divided into tetra- groups of a, b, c, d, each group comprises 20 members.Will be every
The face of individual volunteer is divided into four regions, is divided into a area 10, b area 20, c area 30, d area 40.A area 10 uses the change of prescription a preparation
Adornment brush, b area 20 uses the cosmetic brush of prescription b preparation；C area 30 uses the cosmetic brush of prescription c preparation.Adopt cosmetic brush daily to every
Individual volunteer's brush face (not brushing cosmetics), brushes 5 minutes every time.Continue 15 days, after the 15th day terminates, with the inspection of visia skin
Survey the pitch-dark degree that instrument detects skin.
Pitch-dark degree under record initial conditions below:
| D group | A group | B group | C group | |
| 1 | 9.81 | 9.55 | 9.82 | 9.65 |
| 2 | 9.66 | 9.57 | 9.83 | 9.86 |
| 3 | 9.88 | 9.86 | 9.58 | 9.58 |
| 4 | 9.90 | 9.52 | 9.92 | 9.57 |
| 5 | 9.77 | 9.89 | 9.77 | 9.85 |
| 6 | 9.72 | 9.60 | 9.84 | 9.60 |
| 7 | 9.55 | 9.78 | 9.93 | 9.80 |
| 8 | 9.75 | 9.58 | 9.75 | 9.95 |
| 9 | 9.83 | 9.86 | 9.54 | 9.62 |
| 10 | 9.94 | 9.56 | 9.54 | 9.67 |
| 11 | 9.84 | 9.62 | 9.51 | 9.77 |
| 12 | 9.66 | 9.61 | 9.58 | 9.91 |
| 13 | 9.79 | 9.62 | 9.64 | 9.63 |
| 14 | 9.90 | 9.78 | 9.79 | 9.69 |
| 15 | 9.67 | 9.88 | 9.79 | 9.66 |
| 16 | 9.86 | 9.53 | 9.90 | 9.83 |
| 17 | 9.64 | 9.79 | 9.95 | 9.75 |
| 18 | 9.81 | 9.68 | 9.63 | 9.81 |
| 19 | 9.80 | 9.75 | 9.75 | 9.76 |
| 20 | 9.92 | 9.74 | 9.94 | 9.68 |
| Maximum | 9.94 | 9.89 | 9.95 | 9.95 |
| Minima | 9.55 | 9.52 | 9.51 | 9.57 |
| Meansigma methodss | 9.79 | 9.69 | 9.75 | 9.73 |
| Standard deviation | 0.104551279 | 0.1253122 | 0.142993886 | 0.109351 |
Experimental data after 15 days
| D group | A group | B group | C group | |
| 1 | 9.84 | 6.55 | 4.42 | 2.52 |
| 2 | 9.84 | 6.41 | 5.23 | 2.25 |
| 3 | 9.84 | 5.77 | 4.13 | 2.35 |
| 4 | 9.84 | 6.68 | 4.76 | 1.52 |
| 5 | 9.91 | 6.48 | 5.05 | 2.02 |
| 6 | 9.93 | 5.01 | 4.39 | 2.56 |
| 7 | 9.84 | 6.78 | 4.97 | 1.39 |
| 8 | 9.81 | 5.27 | 4.78 | 2.60 |
| 9 | 9.82 | 6.78 | 5.18 | 2.01 |
| 10 | 9.93 | 6.02 | 5.30 | 1.75 |
| 11 | 9.82 | 5.72 | 5.34 | 2.36 |
| 12 | 9.85 | 5.28 | 4.38 | 1.17 |
| 13 | 9.82 | 5.48 | 4.77 | 1.70 |
| 14 | 9.82 | 5.31 | 4.77 | 2.23 |
| 15 | 9.82 | 6.40 | 4.24 | 2.43 |
| 16 | 9.83 | 6.00 | 5.27 | 1.31 |
| 17 | 9.81 | 6.45 | 5.22 | 2.15 |
| 18 | 9.84 | 6.01 | 4.46 | 2.21 |
| 19 | 9.94 | 5.33 | 4.66 | 2.45 |
| 20 | 9.85 | 6.27 | 4.06 | 2.37 |
| Maximum | 9.94 | 6.78 | 5.34 | 2.60 |
| Minima | 9.81 | 5.01 | 4.06 | 1.17 |
| Meansigma methodss | 9.85 | 6.00 | 4.77 | 2.07 |
| Standard deviation | 0.040743 | 0.556228567 | 0.404696 | 0.431581 |
Example IV: statistics conclusion
From Fig. 1 it is found that the pitch-dark degree of 80 its skin of face of volunteer chosen is more uniform, meet wanting of experiment
Ask.
It is found that through experiment, matched group (d group) its pitch-dark degree is not changed in substantially from Fig. 2, but experimental group (a
Group, b group, c group) its pitch-dark degree all assumes reduction by a relatively large margin, and the reduction amplitude of c group is maximum.
Additionally, carrying out statistical test (t inspection):
First, the t inspection before and after the experiment of experimental group a group, p=4.31357e-20 < 0.01, illustrate 99% probability, a group is tested
Phase pitch-dark degree has significant difference in front and back, and cosmetic brush a has the whitening effect of significance；
2nd, the t inspection before and after the experiment of experimental group b group, p=7.9546e-25 < 0.01, illustrates 99% probability, before the experiment of b group
Later stage pitch-dark degree has significant difference, and cosmetic brush b has the whitening effect of significance；
3rd, the t inspection before and after the experiment of experimental group c group, p=2.65403e-27 < 0.01, illustrate 99% probability, c group is tested
Phase pitch-dark degree has significant difference in front and back, and cosmetic brush c has the whitening effect of significance；
4th, experimental group c and experimental group a, the t inspection after experiment, p=2.46199e-24 < 0.01,99% possibility is described
Property, c group, the pitch-dark degree of a group have significant difference, and cosmetic brush c compares the whitening effect with significance than cosmetic brush a.
In sum, on statistical significance, the cosmetic brush of the present invention its to have the reduction skin of face of significance pitch-dark
That is to say, that it has the whitening effect of significance, on statistical significance, its conclusion has more than 99% possibility to the effect of degree
Property is effective.Additionally, the cosmetic brush of the present invention also has defying age, antiplaque and other effects.
Although embodiments of the invention have been shown and described above it is to be understood that above-described embodiment is example
Property it is impossible to be interpreted as limitation of the present invention, those of ordinary skill in the art is in the principle without departing from the present invention and objective
In the case of above-described embodiment can be changed within the scope of the invention, change, replace and modification.
Claims (9)
1. a kind of nanometer vitamin bristle formula it is characterised in that by weight, including following component:
Thermoplastic polyester granule, 40 grams to 60 grams；
Nanometer vitamine capsule solution, 25 grams to 30 grams；
Cross-linking agent, 5 grams to 10 grams；
Nano-magnetic powder, 3 grams to 5 grams；
Corallium Japonicum Kishinouye nano powder, 3 grams to 5 grams；
Nanometer Margarita powder, 2 grams to 4 grams.
2. according to claim 1 nanometer of vitamin bristle formula it is characterised in that by weight, also includes as follows
Component: hyaluronic acid, 1 gram to 3 grams.
3. according to claim 2 nanometer of vitamin bristle formula it is characterised in that by weight, also includes as follows
Component: there is the Chinese herbal medicine extract dry powder of whitening effect, 0.2 gram to 0.5 gram.
4. according to claim 3 nanometer of vitamin bristle formula it is characterised in that by weight, also includes as follows
Component: natural perfume material, 0.1 gram to 0.2 gram.
5. according to claim 3 nanometer of vitamin bristle formula it is characterised in that by weight, also includes as follows
Component: polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
6. according to claim 3 nanometer of vitamin bristle formula it is characterised in that by weight, also includes as follows
Component: soft agent, 2 grams to 10 grams.
7. the nanometer vitamin bristle formula according to any one of claim 1 to 6 it is characterised in that by weight, institute
Stating thermoplastic polyester granule is pbt granule；Described nanometer vitamine capsule solution is the molten of vitamin nano capsule vce5788
Liquid.
8. a kind of preparation technology of nano-antibacterial bristle is it is characterised in that comprise the steps:
S801, by weight ratio, pbt granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder is added mixer；Add
30% nanometer vitamine capsule solution；Dry, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；
S802, cuts into chunks according to customization size, burns a mao peak using sodium hydroxide, then utilizes organic acid to clean；
S803, puts into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution and cross-linking agent passes through high temperature after fixation
Dye vat is warmed up to 80 to 110 degree insulation 30 minutes；
S804, cleaning, dehydration, 110 degree of bakings of entrance baking box again are dried for 100 minutes.
9. a kind of preparation technology of nano-antibacterial bristle according to claim 8 is it is characterised in that comprise the steps:
S801, by weight ratio, by pbt granule, nano-magnetic powder, Corallium Japonicum Kishinouye nano powder, nanometer Margarita powder, hyaluronic acid, Chinese herbal medicine
Extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30% nanometer vitamine capsule
Solution, mixes 40 minutes；Dry 1.5 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；
S802, cuts into chunks according to customization size, burns a mao peak using sodium hydroxide, then utilizes organic acid to clean, then with swashing
Light subtracts material process equipment and repairs a mao peak further；
S803, puts into the dyeing of dye vat equipment, adds 30% nanometer of vitamine capsule solution and cross-linking agent passes through high temperature after fixation
Dye vat is warmed up to 80 to 110 degree insulation 30 minutes；
S804, cleaning, dehydration, 110 degree of bakings of entrance baking box again are dried for 100 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610774981.4A CN106333481B (en) | 2016-08-31 | 2016-08-31 | A kind of nanometer of vitamin bristle and preparation process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610774981.4A CN106333481B (en) | 2016-08-31 | 2016-08-31 | A kind of nanometer of vitamin bristle and preparation process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106333481A true CN106333481A (en) | 2017-01-18 |
| CN106333481B CN106333481B (en) | 2019-04-02 |
Family
ID=57822803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610774981.4A Expired - Fee Related CN106333481B (en) | 2016-08-31 | 2016-08-31 | A kind of nanometer of vitamin bristle and preparation process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106333481B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018112813A1 (en) * | 2016-12-22 | 2018-06-28 | 东莞市正和日用制品有限公司 | Vitamin nanobristle formula and preparation process |
| CN110158182A (en) * | 2018-02-26 | 2019-08-23 | 沧州成浩化妆用具有限公司 | A kind of novel artificial hair of the cosmetic brush with antibacterial functions |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1113973A (en) * | 1994-06-24 | 1995-12-27 | 温一林 | Producing method for antibiotic health tooth-brush |
| JP2009285445A (en) * | 2008-04-28 | 2009-12-10 | Fuji Chemical Kk | Anti-bacterial make-up brush and method of manufacturing brush bristle |
| CN102462151A (en) * | 2010-11-05 | 2012-05-23 | Hct亚洲有限公司 | Brush with magnetic filaments |
| CN104367247A (en) * | 2014-05-04 | 2015-02-25 | 爱丽丝·常 | Face and body brush with thin and conical bristles, mixture compositions and massage face |
| CN105686328A (en) * | 2009-07-31 | 2016-06-22 | 高露洁-棕榄公司 | High cleaning dentifrice compositions |
-
2016
- 2016-08-31 CN CN201610774981.4A patent/CN106333481B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1113973A (en) * | 1994-06-24 | 1995-12-27 | 温一林 | Producing method for antibiotic health tooth-brush |
| JP2009285445A (en) * | 2008-04-28 | 2009-12-10 | Fuji Chemical Kk | Anti-bacterial make-up brush and method of manufacturing brush bristle |
| CN105686328A (en) * | 2009-07-31 | 2016-06-22 | 高露洁-棕榄公司 | High cleaning dentifrice compositions |
| CN102462151A (en) * | 2010-11-05 | 2012-05-23 | Hct亚洲有限公司 | Brush with magnetic filaments |
| CN104367247A (en) * | 2014-05-04 | 2015-02-25 | 爱丽丝·常 | Face and body brush with thin and conical bristles, mixture compositions and massage face |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018112813A1 (en) * | 2016-12-22 | 2018-06-28 | 东莞市正和日用制品有限公司 | Vitamin nanobristle formula and preparation process |
| CN110158182A (en) * | 2018-02-26 | 2019-08-23 | 沧州成浩化妆用具有限公司 | A kind of novel artificial hair of the cosmetic brush with antibacterial functions |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106333481B (en) | 2019-04-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106360959B (en) | A kind of nano-antibacterial bristle composition and preparation process | |
| CN106165965B (en) | A kind of nano-negative ion bristle and preparation process | |
| CN105168038B (en) | Golden flower flower clay mask and preparation method thereof | |
| CN107308057B (en) | Nontoxic hair softening cream capable of softening and nourishing hair and preparation method thereof | |
| CN107714559A (en) | One kind is without anti-corrosion deep water supplement skin care item | |
| CN102440937A (en) | Healthcare wet tissue with antimicrobial and anti-acne functions | |
| US20200397689A1 (en) | Compositions and methods for hair and scalp treatment | |
| JP2009073773A (en) | Composition for hair-scalp and hair treatment, color treatment, pore-cleaning agent, shampoo and soap comprising the same composition for hair-scalp | |
| CN107714515A (en) | A kind of eye shadow cream of quick colour generation | |
| CN106893650A (en) | A kind of zeolite perfumed soap and preparation method thereof | |
| CN102440938A (en) | Pure plant moisturizing facial cleanser | |
| CN107375095A (en) | A kind of whitening, moisturizing essence and preparation method thereof | |
| US20180169000A1 (en) | Dying agent using natural henna | |
| KR101089879B1 (en) | Tape of protecting ultraviolet rays | |
| CN106333481A (en) | Formula of nanometer vitamin brush bristle and preparation technology | |
| CN107854403A (en) | A kind of clean moisture surge treatment formula | |
| KR20090099110A (en) | Functional cream including nano silver | |
| KR101539688B1 (en) | Cosmetic effective in improving skin photoaging containing oleoresin capsicum and manufacturing method thereof | |
| CN107569441A (en) | A kind of antiallergic lightening compositions and its application | |
| KR20070068881A (en) | Composition for hairdye using natural plant materials | |
| KR101650304B1 (en) | Clay composition for sheer type pack and sheer type clay mask pack using the same | |
| CN107184430A (en) | A kind of Haircare composition of not silicate-containing oil and preparation method thereof | |
| CN106360960B (en) | A kind of fibroin collagen bristle formula and preparation technology | |
| CN104490613B (en) | A kind of microcapsule-type rouge | |
| CN105832638B (en) | Whitening pearl facial mask beautifying liquid with deep water supplement moisture-keeping functions and its preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190402 |