CN106360959B - A kind of nano-antibacterial bristle composition and preparation process - Google Patents
A kind of nano-antibacterial bristle composition and preparation process Download PDFInfo
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- CN106360959B CN106360959B CN201610772584.3A CN201610772584A CN106360959B CN 106360959 B CN106360959 B CN 106360959B CN 201610772584 A CN201610772584 A CN 201610772584A CN 106360959 B CN106360959 B CN 106360959B
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- antibacterial
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Classifications
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- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/006—Antimicrobial, disinfectant bristles, handle, bristle-carrier or packaging
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/02—Bristles details
- A46D1/0207—Bristles characterised by the choice of material, e.g. metal
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
- A46D1/045—Cleaning, e.g. washing, drying
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/04—Preparing bristles
- A46D1/06—Machines or apparatus for cutting bristles
Abstract
The invention discloses a kind of nano-antibacterial bristle compositions, by weight, including following component thermoplastic polyester granulate, 20 grams to 60 grams；Nanometer silver antimicrobial liquid, 20 grams to 30 grams；Couplant, 1 gram to 10 grams；Nano-magnetic powder, 1 gram to 5 grams；Coral nano powder, 1 gram to 2 grams；Nano pearl powder, 1 gram to 3 grams.The preparation process of the present invention is simple, cheap, is proved by statistics, and antibacterial effect of the invention has 99% or more possibility to be higher than the antibacterial effects of normal bristles, and anti-microbial property is superior；The nano-antibacterial bristle silver ion active constituent of the present invention, is widely used in medical treatment, and proves safe and efficient, and nontoxic, without allergic reaction to no skin irritation, low concentration can be obtained the antibacterial effect of high-efficiency broad spectrum.
Description
Technical field
The present invention relates to the combinations of bristle preparation process, prescription, antimicrobial technology field more particularly to a kind of nano-antibacterial bristle
Object and preparation process.
Background technology
Scientific investigations showed that nano silver has good antibacterial functions, and it uses use with good biocompatibility
In the sterilizing of toiletry, antibacterial processing.
The used bristle of cosmetic brush is all filling material, made by traditional handicraft currently on the market, and antibacterial ability is weaker, right
Skin has certain irritation, and safety is poor, which solves.
Invention content
A kind of nano-antibacterial bristle composition is provided it is an object of the invention to overcome the deficiency of the above-mentioned prior art, this
Invention carries out the anti-microbial property of the cilium of enhancing hairbrush using nano silver technology, and antibacterial effect is outstanding, has spectrum antibacterial effect
Fruit reduces the population density and type of the microorganism on hairbrush, clean and hygienic, very useful convenience.
To achieve the above object, the present invention provides a kind of nano-antibacterial bristle composition, by weight, including such as the following group
Point：
Thermoplastic polyester particle, 20 grams to 60 grams；
Nanometer silver antimicrobial liquid, 20 grams to 30 grams；
Couplant, 1 gram to 10 grams；
Nano-magnetic powder, 1 gram to 5 grams；
Coral nano powder, 1 gram to 2 grams；
Nano pearl powder, 1 gram to 3 grams.
Preferably, by weight, it also comprises the following components：Hyaluronic acid, 1 gram to 2 grams.
Preferably, by weight, it also comprises the following components：Chinese herbal medicine extract dry powder with whitening effect, 0.2 gram
To 0.5 gram.
Preferably, by weight, it also comprises the following components：Natural perfume material, 0.1 gram to 0.2 gram.
Preferably, by weight, it also comprises the following components：Polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
Preferably, by weight, it also comprises the following components：Soft agent, 1 gram to 10 grams.
Preferably, by weight, the thermoplastic polyester particle is PBT particles.
The present invention also provides a kind of preparation processes of nano-antibacterial bristle composition, include the following steps：
By weight ratio mixer is added in PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder by S801；Add
Enter 30% nanometer silver antimicrobial liquid；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；
S802 cuts into chunks according to customization size, a mao peak is burnt using sodium hydroxide, then organic acid utilized to clean；
S803 is put into the dyeing of dye vat equipment, and 30% nanometer silver antimicrobial liquid is added after fixation and 30% couplant passes through
High temperature dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；
S804 is cleaned, is dehydrated, being dried into the baking 100 minutes of 110 degree of oven again.
Preferably, include the following steps：
S801, by weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, in
Mixer is added in herb extracts dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；30% nanometer silver antimicrobial is added
Liquid, mixing 30 minutes；Drying 1 hour, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；
S802 cuts into chunks according to customization size, a mao peak is burnt using sodium hydroxide, then organic acid utilized to clean, then
Subtract material process equipment with laser and further modifies hair peak；
S803 is put into the dyeing of dye vat equipment, and 30% nanometer silver antimicrobial liquid is added after fixation and 30% couplant passes through
High temperature dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；
S804 is cleaned, is dehydrated, being dried into the baking 100 minutes of 110 degree of oven again.
The beneficial effects of the invention are as follows：
1, preparation process of the invention is simple, and cheap, its antibacterial ability of the products such as hairbrush prepared by this technique goes out
Crowd, contributes to the clean hygiene of user, and avoids skin infection.
2, by the way that nano-magnetic powder is arranged, hairbrush of the invention also has the effect of magnetic therapy physical therapy to the skin of human body.Pass through
Coral nano powder is arranged the element of coral can to penetrate to the skin surface when using hairbrush；By the way that pearl powder is arranged,
Nano pearl powder can be stretched into Skin Cell.Play good whitening effect.By the way that Chinese herbal medicine extract dry powder is arranged, when
When the micro sweat of hairbrush and body surface contacts, medicinal herb components can be penetrated into skin, such as the Chinese herbal medicine with whitening composition
Component.By the way that natural perfume material is added, bristle of the invention has good fragrant breath.It, can by mixing polynucleotide extract
In use, to supplement a certain amount of polynucleotide material for skin, play good health-care effect.
3, proved by statistics, antibacterial effect of the invention have 99% or more possibility be higher than normal bristles antibacterial
Effect, anti-microbial property are superior.
4, the used bristle of cosmetic brush is all filling material, made by traditional handicraft currently on the market, with the development of society,
Pursuit of the mankind to quality of the life, the attention to safety, we pass through research and development in 2 years, have devised nano-antibacterial bristle, will
Suitable for fields such as cosmetic brush, wig makeups tool, accessories.
The present invention nano-antibacterial bristle silver ion active constituent, be widely used in medical treatment, and prove it is safe and efficient, to skin
Skin is nonirritant, nontoxic, without allergic reaction, nano-antibacterial bristle sophistication, makes wherein silver ion diameter much smaller than receiving
Rice elargol state particle, since particle is atomic small, surface area is larger, has superpower bactericidal activity and stronger tissue infiltration
Property, low concentration can be obtained the antibacterial effect of high-efficiency broad spectrum.
Description of the drawings
Fig. 1 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group respectively represents hairbrush D
Group, hairbrush A groups, hairbrush B groups, hairbrush C groups；Ordinate represents microorganism concn rank, and 10 grades represent highest.
Specific implementation mode
Embodiment one：Formula and preparation process
| Prescription A（Gram） | Prescription B（Gram） | Prescription C（Gram） | |
| PBT particles | 30 | 40 | 60 |
| Nanometer silver antimicrobial liquid | 20 | 25 | 30 |
| Nano-magnetic powder | 1 | 3 | 5 |
| Coral nano powder | 1 | 1.5 | 2 |
| Nano pearl powder | 1 | 2 | 3 |
| Hyaluronic acid | 1 | 1.5 | 2 |
| Chinese herbal medicine extract dry powder with whitening effect | 0.2 | 0.3 | 0.5 |
| Natural perfume material | 0.1 | 0.15 | 0.2 |
| Polynucleotide extract dry powder | 0.01 | 0.02 | 0.03 |
| Soft agent | 1 | 5 | 10 |
| Couplant | 1 | 5 | 10 |
Preparation process is as follows：By weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder, transparent
Mixer is added in matter acid, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；Addition 30% is received
The silver-colored antimicrobial fluid of rice, mixing 30 minutes；Drying 1 hour, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；S802 is cut according to customization size
At section, a mao peak is burnt using sodium hydroxide, then organic acid is utilized to clean, then subtracts material process equipment with laser and further modify
Mao Feng；S803 is put into the dyeing of dye vat equipment, and 30% nanometer silver antimicrobial liquid is added after fixation and 30% couplant passes through high temperature
Dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；S804 is cleaned, is dehydrated, being dried into the baking 100 minutes of 110 degree of oven again
It is dry.Wherein, organic acid is citric acid.Nanometer silver antimicrobial liquid indicates for mass concentration.
Embodiment two：Antibacterial effect experimental design
Take microorganism nature culture（Containing human body surface, such as the multiple-microorganism of facial surface）；Prepare various trainings
Support the suspension of object；Hairbrush A, hairbrush B, hairbrush C are prepared respectively with component A, component B, component C, and are selected commercially available general
Logical hairbrush D, it is ensured that the specification of four kinds of hairbrush is identical.Certain time is impregnated in suspension with hairbrush, such as 30 minutes, 60 minutes,
180 minutes.Hairbrush is taken out, is cleaned with slow tap water.It dries, then, hairbrush is carried out to ultrasound in the container for determining volume
Wave cleans（Cleaning solution constant volume）, after cleaning, the liquid in extracting container is counted with cell counting board under the microscope
Number, the number of cell is classified, is divided into 1 to 10 grade, 1 grade of density is minimum, 10 grades of density highests.Every group of hairbrush selects 20 hairs
It brushes, totally four groups, totally 80 hairbrush.10 grades of concentration are defined as the cell concentration after suspension directly dilution.With point otherwise, directly
The expression microorganism residual quantity of sight.
Embodiment three：Experimental result
| Hairbrush D groups | Hairbrush A groups | Hairbrush B groups | Hairbrush C groups | |
| 1 | 9.40 | 6.12 | 5.19 | 2.55 |
| 2 | 9.23 | 6.74 | 4.95 | 1.81 |
| 3 | 9.84 | 5.29 | 4.81 | 1.59 |
| 4 | 9.37 | 6.74 | 5.08 | 2.96 |
| 5 | 9.25 | 5.61 | 4.08 | 1.39 |
| 6 | 9.80 | 6.48 | 5.37 | 2.75 |
| 7 | 9.27 | 6.13 | 4.78 | 2.62 |
| 8 | 9.54 | 6.79 | 4.71 | 1.78 |
| 9 | 9.80 | 5.98 | 4.80 | 2.21 |
| 10 | 9.69 | 5.08 | 4.97 | 2.54 |
| 11 | 9.19 | 6.68 | 4.47 | 2.93 |
| 12 | 9.24 | 6.66 | 5.30 | 2.12 |
| 13 | 9.04 | 5.21 | 4.38 | 2.51 |
| 14 | 9.73 | 6.13 | 4.56 | 1.30 |
| 15 | 9.65 | 6.08 | 5.15 | 2.66 |
| 16 | 9.48 | 6.46 | 4.97 | 1.80 |
| 17 | 9.30 | 5.02 | 4.08 | 1.58 |
| 18 | 9.45 | 5.42 | 4.87 | 1.62 |
| 19 | 9.81 | 6.36 | 4.72 | 2.50 |
| 20 | 9.44 | 5.84 | 4.28 | 1.33 |
| Maximum value | 9.84 | 6.79 | 5.37 | 2.96 |
| Minimum value | 9.04 | 5.02 | 4.08 | 1.30 |
| Average value | 9.48 | 6.04 | 4.78 | 2.13 |
| Standard deviation | 0.237904 | 0.577372 | 0.365827 | 0.544068 |
Above-mentioned experimental result is the experimental data obtained in the experimental design of embodiment two, and soaking time uses 30 points
Clock.
Example IV：Statistics conclusion
Referring to Fig. 1, Fig. 1 is data processing figure, from Fig. 1, it has also been discovered that 1 to 4 groups（That is D groups, A groups, B groups, C
Group）, average value reduces successively（Bacteria containing amount is horizontal）.
In addition, carrying out statistical test（T is examined）, P=3.27214E-19 between A groups and D groups<0.01, illustrate A groups with
D groups have significant difference, that is to say, that in statistics, its antibacterial ability of the hairbrush of A groups and the antibacterial ability of D groups have 99%
Possibility there is significant difference, wherein D groups are control group, and the antibacterial ability of A groups is significantly better than the antibacterial ability of D groups.
T inspections, P=7.736E-32 are carried out between B groups and D groups<Progress T inspections between 0.01, C group and D, P=
1.57857E-28<0.01, illustrate that the antibacterial ability of B groups, the antibacterial ability of C groups and D groups has 99% possibility to have significantly
The difference of property, B groups, C groups antibacterial ability be significantly better than the antibacterial ability of D groups.
Although the embodiments of the present invention has been shown and described above, it is to be understood that above-described embodiment is example
Property, it is not considered as limiting the invention, those skilled in the art are not departing from the principle of the present invention and objective
In the case of can make changes, modifications, alterations, and variations to the above described embodiments within the scope of the invention.
Claims (8)
1. a kind of nano-antibacterial bristle composition, which is characterized in that by weight, including following component：
Thermoplastic polyester particle, 20 grams to 60 grams；
Nanometer silver antimicrobial liquid, 20 grams to 30 grams；
Couplant, 1 gram to 10 grams；
Nano-magnetic powder, 1 gram to 5 grams；
Coral nano powder, 1 gram to 2 grams；
Nano pearl powder, 1 gram to 3 grams；
The thermoplastic polyester particle is PBT particles；
By weight ratio, mixer is added in PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder；Addition 30% is received
The silver-colored antimicrobial fluid of rice；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；It is cut into chunks according to customization size, is burnt using sodium hydroxide
Then Mao Feng utilizes organic acid to clean；It is put into the dyeing of dye vat equipment, 30% nanometer silver antimicrobial liquid and 30% is added after fixation
Couplant is warming up to 80 to 110 degree heat preservation 30 minutes by high temperature dye vat；It cleans, be dehydrated again, being toasted into 110 degree of oven
It dries within 100 minutes.
2. nano-antibacterial bristle composition according to claim 1, which is characterized in that further include as follows by weight
Component：Hyaluronic acid, 1 gram to 2 grams.
3. nano-antibacterial bristle composition according to claim 2, which is characterized in that further include as follows by weight
Component：Chinese herbal medicine extract dry powder with whitening effect, 0.2 gram to 0.5 gram.
4. nano-antibacterial bristle composition according to claim 3, which is characterized in that further include as follows by weight
Component：Natural perfume material, 0.1 gram to 0.2 gram.
5. nano-antibacterial bristle composition according to claim 4, which is characterized in that further include as follows by weight
Component：Polynucleotide extract dry powder, 0.01 gram to 0.03 gram.
6. nano-antibacterial bristle composition according to claim 5, which is characterized in that further include as follows by weight
Component：Soft agent, 1 gram to 10 grams.
7. a kind of preparation process of nano-antibacterial bristle composition according to claim 6, which is characterized in that including as follows
Step：
By weight ratio mixer is added in PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder by S801；It is added
30% nanometer silver antimicrobial liquid；Drying, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；
S802 cuts into chunks according to customization size, a mao peak is burnt using sodium hydroxide, then organic acid utilized to clean；
S803 is put into the dyeing of dye vat equipment, and 30% nanometer silver antimicrobial liquid is added after fixation and 30% couplant passes through high temperature
Dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；
S804 is cleaned, is dehydrated, being dried into the baking 100 minutes of 110 degree of oven again.
8. a kind of preparation process of nano-antibacterial bristle composition according to claim 7, which is characterized in that including as follows
Step：
S801, by weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, Chinese herbal medicine
Mixer is added in extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent；30% nanometer silver antimicrobial liquid is added,
Mixing 30 minutes；Drying 1 hour, passes through equipment high temperature fusion wire drawing of reeling off raw silk from cocoons；
S802 cuts into chunks according to customization size, a mao peak is burnt using sodium hydroxide, then organic acid utilized to clean, then with sharp
Light subtracts material process equipment and further modifies hair peak；
S803 is put into the dyeing of dye vat equipment, and 30% nanometer silver antimicrobial liquid is added after fixation and 30% couplant passes through high temperature
Dye vat is warming up to 80 to 110 degree heat preservation 30 minutes；
S804 is cleaned, is dehydrated, being dried into the baking 100 minutes of 110 degree of oven again.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610772584.3A CN106360959B (en) | 2016-08-31 | 2016-08-31 | A kind of nano-antibacterial bristle composition and preparation process |
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| CN201610772584.3A CN106360959B (en) | 2016-08-31 | 2016-08-31 | A kind of nano-antibacterial bristle composition and preparation process |
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| CN106360959A CN106360959A (en) | 2017-02-01 |
| CN106360959B true CN106360959B (en) | 2018-07-20 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018112812A1 (en) * | 2016-12-22 | 2018-06-28 | 东莞市正和日用制品有限公司 | Antibacterial nanobristle formula and preparation process |
| CN107557899A (en) * | 2017-09-26 | 2018-01-09 | 枣庄正和制刷有限公司 | A kind of preparation technology of nylon flush for rolling brush |
| CN108577167A (en) * | 2018-05-31 | 2018-09-28 | 代明 | A kind of anti-bacterial bristles containing nano silver |
| CN108903226A (en) * | 2018-05-31 | 2018-11-30 | 代明 | A kind of anti-bacterial bristles containing silver zinc copper germanium Nanoalloy |
| CN110055612A (en) * | 2019-03-22 | 2019-07-26 | 中山尚洋科技股份有限公司 | A kind of negative ion far-infrared antimicrobial nylon hair, cosmetic brush bristles and cosmetic brush |
| CN109943905B (en) * | 2019-03-22 | 2021-10-08 | 代明 | Artificial wool containing plant nano powder |
| CN110158187A (en) * | 2019-05-24 | 2019-08-23 | 浦江卓尔雅化妆用具有限公司 | Cosmetic brush bristles composition and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP5275714B2 (en) * | 2008-04-28 | 2013-08-28 | 富士ケミカル株式会社 | Antibacterial cosmetic brush and method for producing the same |
| CN101602883A (en) * | 2009-06-19 | 2009-12-16 | 深圳英纳利毛刷制品有限公司 | A kind of antimicrobial silver liquid composition and cosmetic brush bristles |
| CN205492981U (en) * | 2016-03-14 | 2016-08-24 | 湖北瑞特威日化有限公司 | Tooth -cleaners with novel polymer nano -silver antibacterial brush hair |
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