CN106360960B - A kind of fibroin collagen bristle formula and preparation technology - Google Patents

Abstract

The invention discloses a kind of fibroin collagen bristle to be formulated by weight, including following component：Thermoplastic polyester particle, 50 grams to 60 grams；Fibroin collagen solution, 30 grams to 40 grams；Nano-magnetic powder, 5 grams to 10 grams；Coral nano powder, 5 grams to 8 grams；Nano pearl powder, 1 gram to 3 grams.The cosmetic brush of the present invention its have conspicuousness the reduction pitch-dark degree of skin of face effect, the present invention can penetrate to the skin amino acid surface, so play moisturizing, moisten, conditioning, the effect of enhancing gloss and elasticity.

Description

A kind of fibroin collagen bristle formula and preparation technology

Technical field

The present invention relates to bristle preparation technology, cosmetic brush technical field, more particularly to a kind of fibroin collagen bristle to match somebody with somebody Side and preparation technology.

Background technology

The bristle of professional color make-up brushing tool is generally divided into animal wool and two kinds of hair of synthesis.Natural animal felt has complete hair scale Piece, therefore hair quality is soft, eats powder degree saturation, uniform in color can be made docile, and do not stimulate skin.

Scientific investigations showed that contain substantial amounts of azelon and the ammonia of abundant fibroin and 18 kinds of needed by human body in silk Base acid activity composition, fibroin have good compatibility with tissue, and silk amino acid silk gum composition has nourishes rough skin, anti-mistake Quick, enhancement Skin Cell vigor, eliminate dermal melanin, skin makeup, skin care and other effects.Silk-fibroin also has moisture absorption, insulation and right Absorption of ultraviolet etc. acts on.

The common bristle of existing cosmetic brush generally use and preparation technology are made, and it does not contain fibroin collagen, Health-care effect is poor, and the problems demand solves.

The content of the invention

A kind of fibroin collagen bristle formula is provided it is an object of the invention to overcome the deficiency of above-mentioned prior art, The bristle of the present invention can be effectively protected the moisture in cuticula rich in skin care element, silk-fibroins such as silk-fibroins, and its regain can Up to more than 15%, so as to play a part of Glycerin, skin is set to keep gloss, delicacy and elasticity for a long time, and have well Whitening effect.

To achieve the above object, the present invention provides a kind of fibroin collagen bristle formula, by weight, including it is as follows Component：

Thermoplastic polyester particle, 50 grams to 60 grams；

Fibroin collagen solution, 30 grams to 40 grams；

Nano-magnetic powder, 5 grams to 10 grams；

Coral nano powder, 5 grams to 8 grams；

Nano pearl powder, 1 gram to 3 grams.

Preferably, by weight, also comprise the following components：Hyaluronic acid, 1 gram to 5 grams.

Preferably, by weight, also comprise the following components：Chinese herbal medicine extract dry powder with whitening effect, 0.2 gram To 0.5 gram.

Preferably, by weight, also comprise the following components：Natural perfume material, 0.1 gram to 0.2 gram.

Preferably, by weight, also comprise the following components：Polynucleotide extract dry powder, 0.01 gram to 0.03 gram.

Preferably, by weight, also comprise the following components：Soft agent, 2 grams to 10 grams.

Preferably, by weight, the thermoplastic polyester particle is PBT particles；The fibroin collagen solution is Silk-fibroin finishing agent SEW3260 solution.

The present invention also provides a kind of preparation technology of nano-antibacterial bristle, comprises the following steps：

S801, by weight ratio, PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder are added into mixer；Add Enter 30% fibroin collagen solution；Drying, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；

S802, cut into chunks according to customization size, burn a mao peak using sodium hydroxide, then cleaned using organic acid；

S803, is put into the dyeing of dye vat equipment, and adding 30% fibroin collagen solution after fixation passes through high temperature dye vat liter Temperature is incubated 30 minutes to 80 to 110 degree；

S804, clean, be dehydrated again, being dried into the baking 100 minutes of 110 degree of baking box.

Preferably, comprise the following steps：

S801, by weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, in Herb extracts dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30% fibroin collagen egg White solution, mix 50 minutes；Drying 2 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；

S802, cut into chunks according to customization size, burn a mao peak using sodium hydroxide, then cleaned using organic acid, then Subtract material process equipment with laser and further repair a mao peak；

S803, is put into the dyeing of dye vat equipment, and adding 30% fibroin collagen solution after fixation passes through high temperature dye vat liter Temperature is incubated 30 minutes to 80 to 110 degree；

S804, clean, be dehydrated again, being dried into the baking 100 minutes of 110 degree of baking box.

The beneficial effects of the invention are as follows：

1st, preparation technology of the invention is simple, cheap, and the present invention uses silk-fibroin finishing agent SEW3260, and it is applicable In the skin care arrangement suitable for cotton, hair, silk, fiber crops, chemical ＆ blended fabric and ready-made clothes.Clothes after its modification, summer dress Absorbing fast-drying, softness are smooth；Because silk-fibroin, amino acid are similar to human body skin composition, clothing is done with skin compatibility, is had Moisturizing, the effect for moistening, nursing one's health, strengthening gloss and elasticity.It is used for when by this finishing agent in bristle, can be with during bristle Amino acid etc. is penetrated into skin surface, and then plays moisturizing, the effect for moistening, nursing one's health, strengthening gloss and elasticity.What is used During, with the abrasion of bristle, the end face of bristle is gradually moved, and discharges content so as to there is microcapsules damaged always Thing.

2nd, proved by statistics, the possibility that its whitening effect of cosmetic brush of the invention has more than 99% is higher than generalization Adornment brush, whitening effect are superior.

3rd, it is all filling material, made by traditional handicraft that cosmetic brush, which uses bristle, in the market, with the development of society, Pursuit of the mankind to quality of the life, the attention to safety, we pass through the research and development of 2 years, invent nano microbeam bristle, will Suitable for fields such as cosmetic brush, wig makeups instrument, accessories.The present invention is widely used in medical treatment, and prove it is safe and efficient, to skin It is nonirritant, it is nontoxic, without allergic reaction.

Brief description of the drawings

Fig. 1 is the initial condition data figure that the present invention tests；

Fig. 2 is the experiment effect figure of one embodiment of the invention, and abscissa represents group, and 1 to 4 group represents hairbrush D respectively Group, hairbrush A groups, hairbrush B groups, hairbrush C groups；Ordinate represents the pitch-dark degree of skin, anaplasia of the pitch-dark degree from 0 to 10 Change；

Fig. 3 is that face pilot region divides schematic diagram in experimental design of the present invention；

Reference：A areas 10；B areas 20；C areas 30；D areas 40.

Embodiment

Embodiment one：Formula and preparation technology

	Prescription A（Gram）	Prescription B（Gram）	Prescription C（Gram）
				PBT particles	50	55	60
Nanometer silver antimicrobial liquid	30	35	40
				Nano-magnetic powder	5	8	10
Coral nano powder	5	6	8
				Nano pearl powder	1	2	3
Hyaluronic acid	1	3	5
				Chinese herbal medicine extract dry powder with whitening effect	0.2	0.3	0.5
Natural perfume material	0.1	0.15	0.2
				Polynucleotide extract dry powder	0.01	0.02	0.03
Soft agent	2	5	10

Preparation technology is as follows：S801, by weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, nano-pearl Powder, hyaluronic acid, Chinese herbal medicine extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30% fibroin collagen solution, mix 50 minutes；Drying 2 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；S802, according to Customization size is cut into chunks, and is burnt a mao peak using sodium hydroxide, is then cleaned using organic acid, then subtracts material process equipment with laser Further repair hair peak；S803, is put into the dyeing of dye vat equipment, and adding 30% fibroin collagen solution after fixation passes through height Warm dye vat is warming up to 80 to 110 degree insulation 30 minutes；S804, clean, be dehydrated again, being dried into the baking 100 minutes of 110 degree of baking box It is dry.Wherein, organic acid is citric acid.Fibroin collagen solution represents for mass concentration.

Embodiment two：Antibacterial effect experimental design and experimental result

Fig. 1 and Fig. 2 are referred to, 80 volunteers is randomly choosed, is divided into tetra- groups of A, B, C, D, each group includes 20 members. The face of each volunteer is divided into four regions, is divided into A areas 10, B areas 20, C areas 30, D areas 40.A areas 10 are prepared using prescription A Cosmetic brush, the cosmetic brush that B areas 20 are prepared using prescription B；The cosmetic brush that C areas 30 are prepared using prescription C.Use cosmetic brush daily To each volunteer's brush face（Do not brush cosmetics）, brush 5 minutes every time.Continue 15 days, after the 15th day terminates, with Visia skins Skin detector detects the pitch-dark degree of skin.

The pitch-dark degree under initial conditions is recorded below：

	Hairbrush D groups	Hairbrush A groups	Hairbrush B groups	Hairbrush C groups
					1	9.75	9.59	9.53	9.90
2	9.86	9.59	9.51	9.76
					3	9.70	9.87	9.94	9.87
4	9.73	9.74	9.81	9.54
					5	9.82	9.65	9.84	9.52
6	9.70	9.86	9.67	9.93
					7	9.92	9.82	9.88	9.68
8	9.63	9.77	9.77	9.71
					9	9.69	9.86	9.69	9.84
10	9.51	9.52	9.92	9.52
					11	9.69	9.88	9.83	9.91
12	9.85	9.79	9.64	9.72
					13	9.62	9.89	9.75	9.58
14	9.76	9.85	9.78	9.72
					15	9.87	9.76	9.83	9.59
16	9.65	9.86	9.94	9.93
					17	9.71	9.78	9.92	9.77
18	9.58	9.60	9.55	9.64
					19	9.54	9.70	9.87	9.92
20	9.54	9.58	9.63	9.69
					Maximum	9.92	9.89	9.94	9.93
Minimum value	9.51	9.52	9.51	9.52
					Average value	9.71	9.75	9.77	9.74
Standard deviation	0.114119772	0.116311489	0.135272814	0.138909891

Experimental data after 15 days

	D groups	A groups	B groups	C groups
					1	9.59	5.17	4.85	1.62
2	9.52	6.33	4.55	2.81
					3	9.68	6.48	5.10	1.68
4	9.79	5.75	4.75	2.79
					5	9.57	5.24	4.16	1.46
6	9.62	5.56	4.38	2.86
					7	9.76	6.74	5.44	2.07
8	9.60	5.25	4.88	2.73
					9	9.67	6.19	5.09	2.72
10	9.84	5.15	4.50	1.58
					11	9.79	5.55	4.65	1.41
12	9.66	6.74	4.65	1.49
					13	9.54	6.70	5.02	1.69
14	9.81	6.05	4.64	2.27
					15	9.84	6.04	5.17	1.16
16	9.78	6.23	5.05	1.58
					17	9.80	5.11	4.96	1.60
18	9.82	6.49	5.41	1.98
					19	9.77	5.66	4.62	1.61
20	9.58	5.40	4.12	2.87
					Maximum	9.84	6.74	5.44	2.87
Minimum value	9.52	5.11	4.12	1.16
					Average value	9.70	5.89	4.80	2.00
Standard deviation	0.107252	0.561041	0.357145	0.570618328

Example IV：Statistics conclusion

From Fig. 1 it can be found that the pitch-dark degree for 80 volunteer its skin of face chosen is more uniform, meet experiment It is required that.

From Fig. 2 it can be found that by experiment, control group（D groups）Its pitch-dark degree does not change substantially, but experimental group（A Group, B groups, C groups）Reduction by a relatively large margin is all presented in its pitch-dark degree, and the reduction amplitude of C groups is maximum.

In addition, carry out statistical test（T is examined）：

1. the front and rear T of control group D groups is examined, P=0.435239986>0.05, illustrate the possibility for having 95%, before and after experiment The two does not have the difference of conspicuousness, and pitch-dark degree does not change；

2. the front and rear T of experimental group A groups experiment is examined, P=1.32831E-18<0.01, illustrate the possibility for having 99%, A groups are in fact Testing pitch-dark degree of front and rear phase has significant difference, and cosmetic brush A has the whitening effect of conspicuousness；

2. the front and rear T of experimental group B groups experiment is examined, P=1.13683E-27<0.01, illustrate the possibility for having 99%, B groups are in fact Testing pitch-dark degree of front and rear phase has significant difference, and cosmetic brush B has the whitening effect of conspicuousness；

3. the front and rear T of experimental group C groups experiment is examined, P=4.25423E-25<0.01, illustrate the possibility for having 99%, C groups are in fact Testing pitch-dark degree of front and rear phase has significant difference, and cosmetic brush C has the whitening effect of conspicuousness；

4. experimental group C and experimental group A, the T after experiment is examined, P=5.86175E-23<0.01, illustrate to have 99% can Energy property, C groups, the pitch-dark degree of A groups have significant difference, and cosmetic brush C compares the whitening effect with conspicuousness than cosmetic brush A.

In summary, on statistical significance, cosmetic brush of the invention its have the reduction skin of face of conspicuousness pitch-dark The effect of degree, that is to say, that it has the whitening effect of conspicuousness, and on statistical significance, its conclusion has more than 99% possibility Property is effective.In addition, the cosmetic brush of the present invention also has anti-aging, antiplaque and other effects.

Although embodiments of the invention have been shown and described above, it is to be understood that above-described embodiment is example Property, it is impossible to limitation of the present invention is interpreted as, one of ordinary skill in the art is not departing from the principle and objective of the present invention In the case of above-described embodiment can be changed within the scope of the invention, change, replace and modification.

Claims (2)

1. a kind of preparation technology of nano-antibacterial bristle, it is characterised in that comprise the following steps：

S801, by weight ratio, PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder are added into mixer；Add 30% fibroin collagen solution；Drying, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；

S802, cut into chunks according to customization size, burn a mao peak using sodium hydroxide, then cleaned using organic acid；

S803, is put into the dyeing of dye vat equipment, and add 30% fibroin collagen solution after fixation is heated up by high temperature dye vat To 80 to 110 degree insulation 30 minutes；

S804, clean, be dehydrated again, being dried into the baking 100 minutes of 110 degree of baking box.

2. the preparation technology of a kind of nano-antibacterial bristle according to claim 1, it is characterised in that comprise the following steps：

S801, by weight ratio, by PBT particles, nano-magnetic powder, coral nano powder, Nano pearl powder, hyaluronic acid, Chinese herbal medicine Extract dry powder, natural perfume material, polynucleotide extract dry powder, soft agent add mixer；Add 30% fibroin collagen Solution, mix 50 minutes；Drying 2 hours, by reeling off raw silk from cocoons, equipment high temperature merges wire drawing；

S802, cut into chunks according to customization size, burn a mao peak using sodium hydroxide, then cleaned using organic acid, then with sharp Light subtracts material process equipment and further repairs a mao peak；

S803, is put into the dyeing of dye vat equipment, and add 30% fibroin collagen solution after fixation is heated up by high temperature dye vat To 80 to 110 degree insulation 30 minutes；

S804, clean, be dehydrated again, being dried into the baking 100 minutes of 110 degree of baking box.