CN102503142A - Dry particles for crystal polishing tiles sintered at one step and application thereof - Google Patents
Dry particles for crystal polishing tiles sintered at one step and application thereof Download PDFInfo
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- CN102503142A CN102503142A CN2011103205349A CN201110320534A CN102503142A CN 102503142 A CN102503142 A CN 102503142A CN 2011103205349 A CN2011103205349 A CN 2011103205349A CN 201110320534 A CN201110320534 A CN 201110320534A CN 102503142 A CN102503142 A CN 102503142A
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Abstract
The invention discloses dry particles for crystal polishing tiles sintered at one step, which comprise at least one kind in three kinds of dry particles of high potassium, high barium and high zinc; and the invention also discloses a method for preparing the crystal polishing tiles by using the dry particles. The dry particles disclosed by the invention have high original melting temperature, small high-temperature viscosity and favorable grain size distribution; the favorable air exhaust of a blank body can be ensured, and air bubbles can also be removed as far as possible at high temperature; and according to favorable compatibility between the three systems, the components of the dry particles of the three systems not only can be independently used but also can be used in a matching way according to actual conditions. The crystal polishing tiles prepared by using the dry particles for the crystal polishing tiles, which are disclosed by the invention, are sintered at one step, the process of high-temperature bisque sintering can be omitted, the energy consumption is greatly lowered, the pollution is effectively reduced, the production cost can be lowered by about 15 percent, and the production benefit is greatly enhanced. The crystal polishing tiles obtained by production have high transparency of glazed faces and little air bubbles.
Description
Technical field
The present invention relates to the brilliant brick of a kind of throwing and use dry granular, and use this dry granular to prepare the method for throwing brilliant brick.
Background technology
It is the NEW TYPE OF COMPOSITE sheet material that sytull is compounded in brick brick modelled after an antique surface one deck 1-4mm that imitative stone is thrown brilliant brick; It integrates glass, pottery, stone material advantage; Merge glass smelting technology, ceramic tile shaping and crystallization and thermal treatment, polishing, cutting technique in one, sytull piece pellet shop is applied on the ceramic tile base substrate formed compact product structure, clean mark, glittering and translucent through crystallizing and sintering; Stereoscopic sensation is strong, has the sensation as the beautiful matter.
The preparation that at present imitative stone is thrown brilliant brick mainly is to adopt the secondary burning technology, behind the stamp through the high temperature biscuiting after the base substrate upper berth apply one deck glass ceramics frit dry granular, twice firing at low temperatures.Secondary is fired and is thrown brilliant brick fully; Because base substrate will pass through the high temperature biscuiting earlier, through the low temperature biscuiting, the process for producing bricks of more once painting enamel metal ware is loaded down with trivial details again; Energy consumption is bigger, and defectives such as the pattern of burning till of substep makes that microlite exists that fastness to rubbing is low, hardness is low, base substrate and microcrystalline coating conjugation difference.How to capture that its surface porosity is many, wear resisting property is low, thermal stability is poor, how to enhance productivity and cut down the consumption of energy, have great importance.
Along with world population increases and Economic development, the resource consumption and the disposal of pollutants of building and operation thereof economize on resources, protect environment, realize building and natural harmony coexistence, are the common issues that the whole world faces.In the face of earth natural resource constantly utilize and non-renewable objective problem, be a big bottleneck on the ceramic boundary of puzzlement.The traditional ceramics industry is very high to the degree of complying with of the resource and the energy, and ceramic industry will really become energy resource and practice thrift friendly type industry, energy-saving and emission-reduction, and consumption reduction is sharp useless etc., and the aspect also shoulders heavy responsibilities.
Summary of the invention
The object of the present invention is to provide a kind of once-firing to throw brilliant brick and use dry granular, and use this dry granular to prepare the method for throwing brilliant brick.
The technical scheme that the present invention adopted is:
A kind of once-firing is thrown brilliant brick and is used dry granular, by at least a composition the in following high potassium, high barium, three kinds of dry granulars of high zinc, wherein:
High potassium dry granular is by Al
2O
315～21 parts, SiO
253～60 parts, K
26～8 parts of O, Na
21～5 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～6 part of BaO, Li
20～1 part of composition of O;
High barium dry granular is by Al
2O
312～15 parts, SiO
238～50 parts, K
20.5～3 part of O, Na
20.5～3 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～4 part of ZnO, B
2O
30～3,20～40 parts of BaO, Li
20～1 part of composition of O;
High zinc dry granular is by Al
2O
39～19 parts, SiO
253～64 parts, K
21～3 part of O, Na
20.1～3 part of O, 5～11 parts of CaO, 0.1～2 part of MgO, 5～15 parts of ZnO, B
2O
30～2 part, 0～6 part of BaO, Li
20～1 part of composition of O.
Preferably, the granularity of above-mentioned dry granular is 10 ~ 80 orders.
Preferably, said high potassium dry granular is by Al
2O
315～20 parts, SiO
253～59 parts, K
26～8 parts of O, Na
21～3 part of O, 8～11 parts of CaO, 0.1～3 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～5 part of BaO, Li
20～1 part of composition of O.
Preferably, said high barium dry granular is by Al
2O
312～15 parts, SiO
240～50 parts, K
20.5～2.5 part of O, Na
20.5～2.5 part of O, 7.5～12.5 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 22～40 parts of BaO, Li
20～1 part of composition of O.
Preferably, said high zinc dry granular is by Al
2O
310～19 parts, SiO
254～62 parts, K
21～3 part of O, Na
20.1～3 part of O, 6～11 parts of CaO, 0.1～2 part of MgO, 6～15 parts of ZnO, 0～6 part of BaO, B
2O
30～2, Li
20～1 part of composition of O.
A kind of once-firing is thrown the preparation method of brilliant brick, is included in the above-mentioned dry granular of brick surface cloth one deck, and the thickness of dry granular is 1 ~ 4mm, burns till at 1150 ℃ ~ 1230 ℃ next time, obtains throwing brilliant brick product.
Preferably, the firing time of the brilliant brick product of above-mentioned throwing is 60 ~ 150 minutes.
Beneficial effect of the present invention is:
The frit initial melting temperature height that dry granular of the present invention is used helps the base substrate oxidation, and granularity is suitable, both can guarantee that the base substrate exhaust was good, the eliminating bubble that can at high temperature try one's best again.Good consistency between formula system makes the dry granular composition of three systems all can use, and both can use separately, also can use according to the practical situation collocation.
Use the brilliant brick of throwing that dry granular of the present invention makes, once-firing can save high temperature biscuiting process, greatly reduces energy consumption, has reduced pollution effectively, and it is nearly 15% to reduce production costs, and has improved productivity effect greatly.The brilliant brick of the throwing that production obtains, the glaze transparency is high, and bubble is few.
The brilliant brick of the throwing of the inventive method preparation, the high temperature once-firing, the brilliant brick product of the throwing of the equal lower temperature twice firing of wear resistance and resistance to acids and bases has significantly raising, and once-firing, less energy consumption, technology is simple.
Description of drawings
Fig. 1 is that embodiments of the invention are fired the brilliant brick of the throwing that obtains and Comparative Examples and fired the contrast of the brilliant brick of throwing that obtains (a be embodiment 1, and the bright spot on it is the hot spot that reflects; B is embodiment 4, and the bright spot on it is the hot spot of reflection; C is embodiment 7; D is embodiment 8; E is a Comparative Examples 1, and the bright spot on it is the hot spot of reflection; F is a Comparative Examples 2).
Embodiment
A kind of once-firing is thrown brilliant brick and is used dry granular, by at least a composition the in following high potassium, high barium, three kinds of dry granulars of high zinc, wherein:
High potassium dry granular is by Al
2O
315～21 parts, SiO
253～60 parts, K
26～8 parts of O, Na
21～5 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～6 part of BaO, Li
20～1 part of composition of O;
High barium dry granular is by Al
2O
312～15 parts, SiO
238～50 parts, K
20.5～3 part of O, Na
20.5～3 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～4 part of ZnO, B
2O
30～3,20～40 parts of BaO, Li
20～1 part of composition of O;
High zinc dry granular is by Al
2O
39～19 parts, SiO
253～64 parts, K
21～3 part of O, Na
20.1～3 part of O, 5～11 parts of CaO, 0.1～2 part of MgO, 5～15 parts of ZnO, B
2O
30～2 part, 0～6 part of BaO, Li
20～1 part of composition of O.
Preferably, the granularity of above-mentioned dry granular is 10 ~ 80 orders.
Preferably, said high potassium dry granular is by Al
2O
315～20 parts, SiO
253～59 parts, K
26～8 parts of O, Na
21～3 part of O, 8～11 parts of CaO, 0.1～3 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～5 part of BaO, Li
20～1 part of composition of O.
Preferably, said high barium dry granular is by Al
2O
312～15 parts, SiO
240～50 parts, K
20.5～2.5 part of O, Na
20.5～2.5 part of O, 7.5～12.5 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 22～40 parts of BaO, Li
20～1 part of composition of O.
Preferably, said high zinc dry granular is by Al
2O
310～19 parts, SiO
254～62 parts, K
21～3 part of O, Na
20.1～3 part of O, 6～11 parts of CaO, 0.1～2 part of MgO, 6～15 parts of ZnO, 0～6 part of BaO, B
2O
30～2, Li
20～1 part of composition of O.
A kind of once-firing is thrown the preparation method of brilliant brick, is included in the above-mentioned dry granular of brick surface cloth one deck, and the thickness of dry granular is 1 ~ 4mm, burns till at 1150 ℃ ~ 1230 ℃ next time, obtains throwing brilliant brick product.
Preferably, the firing time of the brilliant brick product of above-mentioned throwing is 60 ~ 150 minutes.
Below in conjunction with embodiment the present invention is further described, but is not limited thereto.
Once among the embodiment, if no special instructions, number average referred to massfraction in said minute.
The preparation method of dry granular is following: frit is according to prescription, and behind the batching mixing, warp is founded for 1450 ℃ ~ 1550 ℃, obtains the frit that dry granular is used after the shrend, and the frit particle is crushed to after oven dry
10 ~ 80 orders, obtain required product.
Embodiment 1
A kind of once-firing is thrown brilliant brick and is used dry granular, is made up of high potassium dry granular, and wherein, high potassium dry granular is by Al
2O
315 parts, SiO
253 parts, K
26 parts of O, Na
21 part of O, 13 parts of CaO, 4 parts of MgO, 0.5 part of ZnO, B
2O
33, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 2mm, 1150 ℃, burns till in 120 minutes.The outward appearance of products obtained therefrom is shown in Fig. 1 a.
Embodiment 2
A kind of once-firing is thrown brilliant brick and is used dry granular, is made up of high barium dry granular, and wherein high barium dry granular is by Al
2O
312 parts, SiO
238 parts, K
20.5 part of O, Na
20.5 part of O, 7 parts of CaO, 4 parts of MgO, 1 part of ZnO, 40 parts of BaO, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 3mm, 1200 ℃, burns till in 90 minutes.
Embodiment 3
A kind of once-firing is thrown brilliant brick and is used dry granular, is made up of high zinc dry granular, and wherein high zinc dry granular is by Al
2O
39 parts, SiO
253 parts, K
21 part of O, Na
21 part of O, 5 parts of CaO, 1 part of MgO, 15 parts of ZnO, B
2O
32 parts, 1 part of composition of BaO.
After the adobe compression moulding, the dry granular of cloth one deck embodiment 3 in the brick surface, thickness is 1mm, 1230 ℃, burns till in 60 minutes.
Embodiment 4
A kind of once-firing is thrown brilliant brick and is used dry granular, mixes by high potassium dry granular and high barium dry granular mass ratio by 1:4, wherein:
High potassium dry granular is by Al
2O
321 parts, SiO
260 parts, K
28 parts of O, Na
23 parts of O, 10 parts of CaO, 0.1 part of MgO, 3 parts of ZnO, 6 parts of compositions of BaO;
High barium dry granular is by Al
2O
315 parts, SiO
250 parts, K
23 parts of O, Na
23 parts of O, 13 parts of CaO, 4 parts of MgO, 4 parts of ZnO, B
2O
33,40 parts of BaO, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 4mm, 1200 ℃, burns till in 90 minutes.The outward appearance of products obtained therefrom is shown in Fig. 1 b.
Embodiment 5
A kind of once-firing is thrown brilliant brick and is used dry granular, mixes by high potassium dry granular and high zinc dry granular mass ratio by 1:1, wherein:
High potassium dry granular is by Al
2O
318 parts, SiO
255 parts, K
27 parts of O, Na
21 part of O, 7 parts of CaO, 3 parts of MgO, 2 parts of ZnO, B
2O
32 parts, 4 parts of compositions of BaO;
High zinc dry granular is by Al
2O
319 parts, SiO
264 parts, K
22 parts of O, Na
23 parts of O, 11 parts of CaO, 2 parts of MgO, 15 parts of ZnO, B
2O
36 parts, 2 parts of BaO, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 3mm, 1200 ℃, burns till in 90 minutes.
Embodiment 6
A kind of once-firing is thrown brilliant brick and is used dry granular, mixes by high barium dry granular and high zinc dry granular mass ratio by 2:3, wherein:
High barium dry granular is by Al
2O
314 parts, SiO
240 parts, K
22 parts of O, Na
20.5 part of O, 10 parts of CaO, 0.1 part of MgO, 2 parts of ZnO, B
2O
32,30 parts of compositions of BaO;
High zinc dry granular is by Al
2O
315 parts, SiO
255 parts, K
22 parts of O, Na
20.1 part of O, 8 parts of CaO, 1 part of MgO, 10 parts of ZnO, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 3mm, 1200 ℃, burns till in 90 minutes.
Embodiment 7
A kind of once-firing is thrown brilliant brick and is used dry granular, mixes by high potassium dry granular, high barium dry granular and high zinc dry granular mass ratio by 1:1:1, wherein:
High potassium dry granular is by Al
2O
320 parts, SiO
258 parts, K
28 parts of O, Na
22 parts of O, 8 parts of CaO, 1 part of MgO, 1 part of ZnO, B
2O
31 part, 1 part of composition of BaO;
High barium dry granular is by Al
2O
313 parts, SiO
245 parts, K
21 part of O, Na
22 parts of O, 12.5 parts of CaO, 2 parts of MgO, 0.5 part of ZnO, B
2O
31 part, 22 parts of BaO, Li
21 part of composition of O;
High zinc dry granular is by Al
2O
310 parts, SiO
262 parts, K
21 part of O, Na
22 parts of O, 6 parts of CaO, 1 part of MgO, 5 parts of ZnO, B
2O
33 parts, 1 part of BaO, Li
21 part of composition of O.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 3mm, 1230 ℃, burns till in 90 minutes.The outward appearance of products obtained therefrom is shown in Fig. 1 c.
Embodiment 8
A kind of once-firing is thrown brilliant brick and is used dry granular, mixes by high potassium dry granular, high barium dry granular and high zinc dry granular mass ratio by 1:2:4, wherein:
High potassium dry granular is by Al
2O
315 parts, SiO
259 parts, K
28 parts of O, Na
23 parts of O, 11 parts of CaO, 2 parts of MgO, 1 part of ZnO, B
2O
32 parts, 5 parts of BaO, Li
21 part of composition of O;
High barium dry granular is by Al
2O
312 parts, SiO
240 parts, K
22.5 parts of O, Na
22.5 parts of O, 7.5 parts of CaO, 3 parts of MgO, 3 parts of ZnO, B
2O
32 parts, 35 parts of BaO, Li
21.5 parts of compositions of O;
High zinc dry granular is by Al
2O
312 parts, SiO
258 parts, K
21.5 parts of O, Na
21.5 parts of O, 7 parts of CaO, 1.5 parts of MgO, 6 parts of ZnO, B
2O
34 parts, 1.5 parts of compositions of BaO.
After the adobe compression moulding, the above-mentioned dry granular of cloth one deck in the brick surface, thickness is 3mm, 1230 ℃, burns till in 90 minutes.The outward appearance of products obtained therefrom is shown in Fig. 1 d.
Comparative Examples 1
The dry granular of embodiment 1 is broken into 80 ~ 200 orders, under similarity condition, fires, products obtained therefrom is shown in Fig. 1 e.
Comparative Examples 2
The brilliant brick of a kind of throwing is used dry granular, by Al
2O
313 parts, SiO
260 parts, K
20.5 part of O, 14 parts of CaO, Na
25 parts of O, 1 part of MgO, 0.5 part of ZnO, 2 parts of BaO, B
2O
31 part, Li
22 parts of compositions of O.
Above-mentioned dry granular is broken into 10 ~ 80 orders, with the same condition of embodiment under fire, the outward appearance of products obtained therefrom is shown in Fig. 1 f.
Visible from Fig. 1, to utilize once-firing of the present invention to throw brilliant brick and fire with dry granular that to obtain throwing brilliant brick structure fine and close, transparency is high, and the pattern of brick is high-visible, and glossiness is good, and bubble is few, greatly reduces production energy consumption, and environmental protection is attractive in appearance; And that Comparative Examples 1 is fired the brilliant brick transparency of the throwing that obtains is relatively low, and it is clear that the pattern of brick is smudgy, and low in glossiness; Comparative Examples 2 is fired the brilliant brick of the throwing top layer that obtains the cut bubble can occur, influences quality product.
This shows that the brilliant brick of the throwing of the application of the invention use dry granular, can save the sintering procedure of a kiln of biscuiting, the throwing crystalline substance brick that makes greatly reduces energy consumption, has reduced pollution effectively, and it is nearly 15% to reduce production costs, and has improved productivity effect greatly.The brilliant brick of the throwing that production obtains, the glaze transparency is high, and bubble is few.
Claims (7)
1. an once-firing is thrown brilliant brick and is used dry granular, by at least a composition the in following high potassium, high barium, three kinds of dry granulars of high zinc, wherein:
High potassium dry granular is by Al
2O
315～21 parts, SiO
253～60 parts, K
26～8 parts of O, Na
21～5 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～6 part of BaO, Li
20～1 part of composition of O;
High barium dry granular is by Al
2O
312～15 parts, SiO
238～50 parts, K
20.5～3 part of O, Na
20.5～3 part of O, 7～13 parts of CaO, 0.1～4 part of MgO, 0.5～4 part of ZnO, B
2O
30～3,20～40 parts of BaO, Li
20～1 part of composition of O;
High zinc dry granular is by Al
2O
39～19 parts, SiO
253～64 parts, K
21～3 part of O, Na
20.1～3 part of O, 5～11 parts of CaO, 0.1～2 part of MgO, 5～15 parts of ZnO, B
2O
30～2 part, 0～6 part of BaO, Li
20～1 part of composition of O.
2. throw brilliant brick according to the said a kind of once-firing of claim 1 and use dry granular, it is characterized in that, the granularity of said dry granular is 10 ~ 80 orders.
3. throw brilliant brick according to the said a kind of once-firing of claim 1 and use dry granular, it is characterized in that, said high potassium dry granular is by Al
2O
315～20 parts, SiO
253～59 parts, K
26～8 parts of O, Na
21～3 part of O, 8～11 parts of CaO, 0.1～3 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 0～5 part of BaO, Li
20～1 part of composition of O.
4. throw brilliant brick according to the said a kind of once-firing of claim 1 and use dry granular, it is characterized in that, said high barium dry granular is by Al
2O
312～15 parts, SiO
240～50 parts, K
20.5～2.5 part of O, Na
20.5～2.5 part of O, 7.5～12.5 parts of CaO, 0.1～4 part of MgO, 0.5～3 part of ZnO, B
2O
30～3 part, 22～40 parts of BaO, Li
20～1 part of composition of O.
5. throw brilliant brick according to the said a kind of once-firing of claim 1 and use dry granular, it is characterized in that, said high zinc dry granular is by Al
2O
310～19 parts, SiO
254～62 parts, K
21～3 part of O, Na
20.1～3 part of O, 6～11 parts of CaO, 0.1～2 part of MgO, 6～15 parts of ZnO, 0～6 part of BaO, B
2O
30～2, Li
20～1 part of composition of O.
6. an once-firing is thrown the preparation method of brilliant brick, is included in brick surface each described dry granular of cloth one deck claim 1 ~ 5, and the thickness of dry granular is 1 ~ 4mm, burns till at 1150 ℃ ~ 1230 ℃ next time, obtains throwing brilliant brick product.
7. throw the preparation method of brilliant brick according to the said a kind of once-firing of claim 6, it is characterized in that the firing time of the brilliant brick product of said throwing is 60 ~ 150 minutes.
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| CN103359943A (en) * | 2013-08-05 | 2013-10-23 | 广东高微晶科技有限公司 | Polymorphic microcrystalline glass ceramic composite board and preparation method thereof |
| CN103359943B (en) * | 2013-08-05 | 2016-03-02 | 广东高微晶科技有限公司 | Polymorphous glass-ceramic clad plate and preparation method thereof |
| CN104446657A (en) * | 2014-10-31 | 2015-03-25 | 佛山市高明区海帝陶瓷原料有限公司 | Dry granular additive for full polishing of ceramic tiles and preparation method of dry granular additive |
| CN104446657B (en) * | 2014-10-31 | 2016-01-20 | 佛山市高明区海帝陶瓷原料有限公司 | A kind of for ceramic tile dry granular additive entirely throwing glaze and preparation method thereof |
| CN105776864A (en) * | 2016-03-17 | 2016-07-20 | 鹰牌陶瓷实业（河源）有限公司 | High-transparency frit and preparation method thereof |
| CN105776864B (en) * | 2016-03-17 | 2018-09-07 | 鹰牌陶瓷实业（河源）有限公司 | A kind of frit of the high grade of transparency and preparation method thereof |
| CN108069732A (en) * | 2017-11-29 | 2018-05-25 | 广东道氏技术股份有限公司 | A kind of metal hole stone dry granular and preparation method thereof |
| CN108069732B (en) * | 2017-11-29 | 2020-10-27 | 广东道氏技术股份有限公司 | Metal travertine dry particles and preparation method thereof |
| CN109665871A (en) * | 2018-12-27 | 2019-04-23 | 佛山欧神诺陶瓷有限公司 | It is a kind of to improve the process for throwing brilliant ceramic brick surface wear-resisting property |
| CN110317051A (en) * | 2019-08-02 | 2019-10-11 | 佛山市陶莹新型材料有限公司 | A kind of diamond dry granular and its processing method |
| CN114920587A (en) * | 2022-06-17 | 2022-08-19 | 江西唯美陶瓷有限公司 | Ultra-low gloss fine sand smooth thin rock plate and preparation method thereof |
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