CN102489328A - 一种碳载吡啶氮修饰化钴酞菁催化剂及其制备方法和应用 - Google Patents
一种碳载吡啶氮修饰化钴酞菁催化剂及其制备方法和应用 Download PDFInfo
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- CN102489328A CN102489328A CN2011103971954A CN201110397195A CN102489328A CN 102489328 A CN102489328 A CN 102489328A CN 2011103971954 A CN2011103971954 A CN 2011103971954A CN 201110397195 A CN201110397195 A CN 201110397195A CN 102489328 A CN102489328 A CN 102489328A
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- pyridine
- carbon
- catalyst
- cobalt phthalocyanine
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- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 52
- MPMSMUBQXQALQI-UHFFFAOYSA-N cobalt phthalocyanine Chemical class [Co+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 MPMSMUBQXQALQI-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 99
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims abstract description 50
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims abstract description 25
- DLGYNVMUCSTYDQ-UHFFFAOYSA-N azane;pyridine Chemical compound N.C1=CC=NC=C1 DLGYNVMUCSTYDQ-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000000446 fuel Substances 0.000 claims abstract description 20
- 230000009467 reduction Effects 0.000 claims abstract description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012298 atmosphere Substances 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 238000001035 drying Methods 0.000 claims abstract description 4
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 4
- 239000012018 catalyst precursor Substances 0.000 claims abstract description 3
- 230000003197 catalytic effect Effects 0.000 claims description 26
- 239000003795 chemical substances by application Substances 0.000 claims description 23
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- BSKHPKMHTQYZBB-UHFFFAOYSA-N 2-methylpyridine Chemical group CC1=CC=CC=N1 BSKHPKMHTQYZBB-UHFFFAOYSA-N 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 7
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- 229920000557 Nafion® Polymers 0.000 claims description 6
- SIOXPEMLGUPBBT-UHFFFAOYSA-N Picolinic acid Natural products OC(=O)C1=CC=CC=N1 SIOXPEMLGUPBBT-UHFFFAOYSA-N 0.000 claims description 6
- VXKWYPOMXBVZSJ-UHFFFAOYSA-N tetramethyltin Chemical compound C[Sn](C)(C)C VXKWYPOMXBVZSJ-UHFFFAOYSA-N 0.000 claims description 6
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 3
- 238000011068 loading method Methods 0.000 claims description 3
- 239000012528 membrane Substances 0.000 claims description 3
- 238000012546 transfer Methods 0.000 claims description 3
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 239000002134 carbon nanofiber Substances 0.000 claims description 2
- 239000004567 concrete Substances 0.000 claims description 2
- 239000012467 final product Substances 0.000 claims description 2
- 239000007789 gas Substances 0.000 claims description 2
- 229910021389 graphene Inorganic materials 0.000 claims description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 2
- 239000002091 nanocage Substances 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- LLYXJBROWQDVMI-UHFFFAOYSA-N 2-chloro-4-nitrotoluene Chemical compound CC1=CC=C([N+]([O-])=O)C=C1Cl LLYXJBROWQDVMI-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 150000003222 pyridines Chemical class 0.000 abstract description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract description 2
- 229910001882 dioxygen Inorganic materials 0.000 abstract description 2
- 229910000510 noble metal Inorganic materials 0.000 abstract description 2
- 239000003575 carbonaceous material Substances 0.000 abstract 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
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- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 32
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- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 11
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- 238000005516 engineering process Methods 0.000 description 3
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
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- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 150000002678 macrocyclic compounds Chemical class 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000010970 precious metal Substances 0.000 description 2
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- 101500000959 Bacillus anthracis Protective antigen PA-20 Proteins 0.000 description 1
- 102100026038 Lens fiber membrane intrinsic protein Human genes 0.000 description 1
- 101710115990 Lens fiber membrane intrinsic protein Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
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- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000005518 polymer electrolyte Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- -1 transition metal macrocyclic compound Chemical class 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
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- Inert Electrodes (AREA)
Abstract
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CN201110397195.4A CN102489328B (zh) | 2011-12-02 | 2011-12-02 | 一种碳载吡啶氮修饰化钴酞菁催化剂及其制备方法和应用 |
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CN102489328A true CN102489328A (zh) | 2012-06-13 |
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Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102850360A (zh) * | 2012-09-20 | 2013-01-02 | 首都师范大学 | 静电组装制备石墨烯/金属酞菁类化合物复合材料的方法 |
CN103586063A (zh) * | 2013-10-30 | 2014-02-19 | 东华大学 | 碳负载四磺酸基铜酞菁四钠盐燃料电池催化剂及其制备 |
CN103985885A (zh) * | 2014-05-30 | 2014-08-13 | 长春理工大学 | 一种吡啶基钴酞菁-钴复合物/石墨烯复合材料及其制备方法 |
CN104759259A (zh) * | 2015-04-02 | 2015-07-08 | 河北科技大学 | 一种负载金属酞菁吸附剂及其制备方法和用途 |
CN104891822A (zh) * | 2015-05-25 | 2015-09-09 | 黑龙江大学 | 一种磺酸基酞菁镍-氧化石墨烯复合薄膜材料及制备方法 |
CN104925784A (zh) * | 2014-03-18 | 2015-09-23 | 中国科学院大连化学物理研究所 | 一种石墨烯内嵌单分散金属原子的制备方法 |
WO2018132937A1 (en) * | 2017-01-17 | 2018-07-26 | South University Of Science And Technology Of China | Use of metal phthalocyanine/nanocarbon hybrid catalysts for efficient electrochemical reduction of co2 |
CN109529906A (zh) * | 2018-12-25 | 2019-03-29 | 西安近代化学研究所 | 一种合成1,1,2,3,3,3-六氟丙基甲醚的催化剂及其制备方法 |
CN109675602A (zh) * | 2018-12-25 | 2019-04-26 | 西安近代化学研究所 | 一种负载型钴-氮掺杂碳催化剂及其制备方法和应用 |
CN110652993A (zh) * | 2019-09-30 | 2020-01-07 | 成都理工大学 | 一种钴氮杂石墨烯基催化剂催化氨硼烷产氢性能的研究 |
CN115836071A (zh) * | 2020-12-24 | 2023-03-21 | Azul能源株式会社 | 金属络合物或其加合物、包含金属络合物或其加合物的催化剂及其制造方法、包含催化剂的液态组合物或电极、具备电极的空气电池或燃料电池 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101884937A (zh) * | 2010-08-17 | 2010-11-17 | 天津久聚能源科技发展有限公司 | 碳载钴酞菁催化材料的制备方法 |
-
2011
- 2011-12-02 CN CN201110397195.4A patent/CN102489328B/zh not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101884937A (zh) * | 2010-08-17 | 2010-11-17 | 天津久聚能源科技发展有限公司 | 碳载钴酞菁催化材料的制备方法 |
Non-Patent Citations (3)
Title |
---|
KRISTYANA TASHKOVA: "Co(II) Phthalocyanine Complex with Pyridine Bonded to Silica and Its Interaction with Oxygen", 《INORGANICA CHIMICA ACTA》, vol. 84, 31 December 1984 (1984-12-31), pages 31 - 34 * |
徐莉 等: "CoPy/C催化剂应用碱性介质氧还原催化的电化学性能", 《物理化学学报》, vol. 27, no. 10, 18 August 2011 (2011-08-18) * |
李嘉斌等: "负载酞菁钴气体扩散电极对氧的催化还原", 《化学与生物工程》, vol. 24, no. 7, 31 December 2007 (2007-12-31), pages 16 - 18 * |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102850360A (zh) * | 2012-09-20 | 2013-01-02 | 首都师范大学 | 静电组装制备石墨烯/金属酞菁类化合物复合材料的方法 |
CN103586063A (zh) * | 2013-10-30 | 2014-02-19 | 东华大学 | 碳负载四磺酸基铜酞菁四钠盐燃料电池催化剂及其制备 |
CN103586063B (zh) * | 2013-10-30 | 2016-01-06 | 东华大学 | 碳负载四磺酸基铜酞菁四钠盐燃料电池催化剂及其制备 |
CN104925784A (zh) * | 2014-03-18 | 2015-09-23 | 中国科学院大连化学物理研究所 | 一种石墨烯内嵌单分散金属原子的制备方法 |
CN103985885A (zh) * | 2014-05-30 | 2014-08-13 | 长春理工大学 | 一种吡啶基钴酞菁-钴复合物/石墨烯复合材料及其制备方法 |
CN103985885B (zh) * | 2014-05-30 | 2016-04-06 | 长春理工大学 | 一种吡啶基钴酞菁-钴复合物/石墨烯复合材料及其制备方法 |
CN104759259B (zh) * | 2015-04-02 | 2018-03-16 | 河北科技大学 | 一种负载金属酞菁吸附剂及其制备方法和用途 |
CN104759259A (zh) * | 2015-04-02 | 2015-07-08 | 河北科技大学 | 一种负载金属酞菁吸附剂及其制备方法和用途 |
CN104891822A (zh) * | 2015-05-25 | 2015-09-09 | 黑龙江大学 | 一种磺酸基酞菁镍-氧化石墨烯复合薄膜材料及制备方法 |
WO2018132937A1 (en) * | 2017-01-17 | 2018-07-26 | South University Of Science And Technology Of China | Use of metal phthalocyanine/nanocarbon hybrid catalysts for efficient electrochemical reduction of co2 |
CN109529906A (zh) * | 2018-12-25 | 2019-03-29 | 西安近代化学研究所 | 一种合成1,1,2,3,3,3-六氟丙基甲醚的催化剂及其制备方法 |
CN109675602A (zh) * | 2018-12-25 | 2019-04-26 | 西安近代化学研究所 | 一种负载型钴-氮掺杂碳催化剂及其制备方法和应用 |
CN109529906B (zh) * | 2018-12-25 | 2021-06-15 | 西安近代化学研究所 | 一种合成1,1,2,3,3,3-六氟丙基甲醚的催化剂及其制备方法 |
CN109675602B (zh) * | 2018-12-25 | 2021-12-21 | 西安近代化学研究所 | 一种负载型钴-氮掺杂碳催化剂及其制备方法和应用 |
CN110652993A (zh) * | 2019-09-30 | 2020-01-07 | 成都理工大学 | 一种钴氮杂石墨烯基催化剂催化氨硼烷产氢性能的研究 |
CN115836071A (zh) * | 2020-12-24 | 2023-03-21 | Azul能源株式会社 | 金属络合物或其加合物、包含金属络合物或其加合物的催化剂及其制造方法、包含催化剂的液态组合物或电极、具备电极的空气电池或燃料电池 |
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Inventor after: Qiao Jinli Inventor after: Dai Xianfeng Inventor after: Xu Li Inventor after: Qian Yiwei Inventor after: Ding Lei Inventor after: Qing Cuan Inventor after: Shi Jingjing Inventor after: Xu Pan Inventor after: Fan Mengyang Inventor before: Qiao Jinli Inventor before: Dai Xianfeng Inventor before: Ding Lei Inventor before: Xu Li Inventor before: Qian Yiwei |
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Free format text: CORRECT: INVENTOR; FROM: QIAO JINLI DAI XIANFENG DING LEI XU LI QIAN YIWEI TO: QIAO JINLI DAI XIANFENG XU LI QIAN YIWEI DING LEI QING XIN SHI JINGJING XU PAN FAN MENGYANG |
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Granted publication date: 20160106 Termination date: 20201202 |
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